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本实验以水为溶剂提落叶松中的二氢槲皮素,主要考察提取温度、时间、料液比等因素对提取率的影响,以三种单因素设计正交实验,实验表明,温度具有显著性(p<0.05),最终确立提取工艺的最佳条件是:以水加热回流提取,温度为90℃,时间40min,料液比为1:12,提取3次,提取率达到85%以上.探讨乙醇沉淀法、大孔树脂吸附法、聚酰胺树脂吸附法三种纯化方法对二氢槲皮素粗提物纯化的效果.由结果可知,三种方法均能达到一定的纯化效果,其中聚酰胺树脂的纯化效果最佳,将醇沉与大孔吸附树脂相结合,可以作为一种新的纯化二氧槲皮素的方法进行深入研究. 相似文献
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探索了从刺玫蔷薇茎中提取二氢槲皮素的工艺条件,考察了乙醇提取及盐酸水解过程中各条件对二氢槲皮素提取率的影响.通过单因素实验确定其最佳条件:原料粒度为100~120目、提取温度为80℃、乙醇溶液浓度为60%、料液比为1∶15、提取时间为3h及盐酸溶液与原料用量比值为3∶1、盐酸浓度为3mol/L、水解时间为2h、水解温度为90℃,在此条件下二氢槲皮索的提取率为90.79%. 相似文献
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为简化二氢槲皮素提取工艺,降低能耗与成本,提高提取效率,促进二氢槲皮素的综合应用,本研究采用黑龙江省的兴安落叶松为原料,运用超高压辅助胶束提取技术提取落叶松中二氢槲皮素,测定落叶松树根、树干等不同部位的二氢槲皮素总含量。以此总含量为基础,对提取胶束进行筛选,采用响应面试验对提取工艺进行优化,考察了料液比、提取压力、提取次数及胶束浓度4种不同因素对二氢槲皮素提取率的影响,并与微波提取、超声提取、回流提取等不同提取工艺进行能耗与CO2排放比较。结果表明,最终确定提取胶束为茶皂素,最佳提取工艺条件为:茶皂素浓度8%,料液比1:11.5,提取压力157 MPa,提取次数3次,保压时间5min,在此最佳条件下重复进行3次实验,二氢槲皮素实际提取率可达84.35%±1.20%,与预测值84.98%基本一致。与其他提取方法相比超高压辅助胶束提取率最高,单位原料的能耗和CO2排放量均为最低,分别为1.71×10-4 kW·h·g-1,1.34×10-4 kg/g。综上,利用超高压辅助胶束绿色溶... 相似文献
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Textural Properties of Cold-set Gels Induced from Heat-denatured Whey Protein Isolates 总被引:2,自引:0,他引:2
A 9% whey protein (WP) isolate solution at pH 7.0 was heat-denatured at 80°C for 30 min. Size-exclusion HPLC showed that native WP formed soluble aggregates after heat-treatment. Additions of CaCl2 (10–40 mM), NaCl (50–400 mM) or glucono-delta-lactone (GDL, 0.4–2.0%, w/v) or hydrolysis by a protease from Bacillus licheniformis caused gelation of the denatured solution at 45°C. Textural parameters, hardness, adhesiveness, and cohesiveness of the gels so formed changed markedly with concentration of added salts or pH by added GDL. Maximum gel hardness occurred at 200 mM NaCl or pH 4.7. Increasing CaCl2 concentration continuously increased gel hardness. Generally, GDL-induced gels were harder than salt-induced gels, and much harder than the protease-induced gel. 相似文献
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Anne Theobald Catherine Simoneau Philippe Hannaert Patrizia Roncari Anna Roncari Thomas Rudolph Elke Anklam 《Food Additives & Contaminants》2000,17(10):881-887
The levels of bisphenol-F-diglycidyl ether (BFDGE) were quantified as part of a European survey on the migration of residues of epoxy resins into oil from canned fish. The contents of BFDGE in cans, lids and fish collected from all 15 Member States of the European Union and Switzerland were analysed in 382 samples. Cans and lids were separately extracted with acetonitrile. The extraction from fish was carried out with hexane followed by re-extraction with acetonitrile. The analysis was performed by reverse phase HPL C with fluorescence detection. BFDGE could be detected in 12% of the fish, 24% of the cans and 18% of the lids. Only 3% of the fish contained BFDGE in concentrations considerably above 1mg/kg. In addition to the presented data, a comparison was made with the levels of BADGE (bisphenol-A-diglycidyl ether)analysed in the same products in the context of a previous study. 相似文献
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A. Boenke 《Food Additives & Contaminants》2001,18(12):1135-1140
The European Commission's, Quality of Life Research Programme, Key Action 1—Health, Food & Nutrition is mission-oriented and aims, amongst other things, at providing a healthy, safe and high-quality food supply leading to reinforced consumer confidence in the safety of European food. Its objectives also include the enhancing of the competitiveness of the European food supply. Key Action 1 is currently supporting a number of different types of European collaborative projects in the area of risk analysis. The objectives of these projects range from the development and validation of prevention strategies including the reduction of consumers risks; development and validation of new modelling approaches; harmonization of risk assessment principles, methodologies, and terminology; standardization of methods and systems used for the safety evaluation of transgenic food; providing of tools for the evaluation of human viral contamination of shellfish and quality control; new methodologies for assessing the potential of unintended effects of genetically modified (genetically modified) foods; development of a risk assessment model for Cryptosporidium parvum related to the food and water industries; to the development of a communication platform for genetically modified organism, producers, retailers, regulatory authorities and consumer groups to improve safety assessment procedures, risk management strategies and risk communication; development and validation of new methods for safety testing of transgenic food; evaluation of the safety and efficacy of iron supplementation in pregnant women; evaluation of the potential cancer-preventing activity of pro- and pre-biotic ('synbiotic') combinations in human volunteers. An overview of these projects is presented here. 相似文献
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为研究低温带皮菜籽粕微粉的不同粒级部分的功能特性,以经低温脱脂的带皮菜籽粕为原料,经微粉碎后筛分成212~425μm、150~212μm和106~150μm的3个不同粒级的微粉样品,检测这些样品的吸水性、吸油性、乳化性和乳化稳定性、蛋白质体外消化率。结果表明:1 3个不同粒级的微粉样品之间的粗纤维含量存在显著差异,表明三者的结构组成成分有一定差异。23个微粉样品的乳化活性和乳化稳定性随粒度级别的减小而显著增加(P0.01)。33个微粉样品的蛋白质体外消化率随粒度级别的减小而显著增加(P0.01)。4不同粒级带皮菜籽粕微粉样品的吸水性与吸油性受其结构组成物质不同和粒度的双重影响,与粒度的相关性不明显。 相似文献
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Microbiology of food taints 总被引:2,自引:0,他引:2
Fresh and processed foods are often spoilt by the presence of undesirable flavours and odours caused by microbial action. The aim of this paper is to review the current knowledge of microbiologically induced taints that occur in a wide range of foodstuffs, including meats, poultry, fish, crustaceans, milk, dairy products, fruits, vegetables, cereals and cereal products. Examples have been chosen where the compounds responsible for the taint have been identified and sufficient data obtained to demonstrate the involvement of microorganisms. However, in some cases the full identity of the causative organism may not have been elucidated. The types of microorganisms covered by this review include bacteria, fungi, yeasts, actinomycetes and cyanobacteria. Although cyanobacteria do not in general infect foods, their presence in aqueous systems and water supplies can lead to off-flavours in aquatic organisms and processed foodstuffs. Several examples of each of these processes are discussed. Wherever possible, the likely biosynthetic pathway used by the microorganism to produce the offending compound in a foodstuff is indicated. 相似文献
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Polymers intended for food contact use have been analysed for organic residues which could be attributed to a range of substances employed as polymerization aids (e.g. initiators and catalysts). A wide range of polymers was extracted with solvents and the extracts analysed by gas chromatography-mass spectrometry (GC-MS). The overwhelming majority of substances identified were not derived from aids to polymerization but were oligomers, additives and adventitious contaminants. However, a small number of substances were identified as initiator residues. These included tetramethylsuccinonitrile (TMSN) which was observed in two polymers and it derived from recombination of two azobisisobutyronitrile (AIBN) initiator radicals. Methyl benzoate, benzoic acid, biphenyl and phenyl benzoate were detected in one poly(methyl methacrylate) sample and in two polyvinylchlorides and they are thought to be derived from benzoyl peroxide initiator. TMSN was subsequently targeted for analysis of poly-(methyl methacrylate) plastics using proton nuclear magnetic resonance spectrometry (1 相似文献
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Jesus Simal-Gandara Miguel Sarria-Vidal Rinus Rijk 《Food Additives & Contaminants》2000,17(9):815-819
Experiments were performed to characterize the kinetics of the permeation of different medium molecular weight model permeants: bisphenol A, warfarin and anthracene, from liquid paraffin, through a surrogate potential functional barrier (25 microns-thick orientated polypropylene--OPP) into the food simulants olive oil and 3% (w/v) acetic acid. The characterization of permeation kinetics generally observed the permeation models previously reported to explain the experimental permeation results obtained for a low molecular weight group of model permeants. In general, the model permeants exhibited behaviour consistent with their relative molecular weights with respect to (a) the time taken to attain steady-state permeation into the food simulant in which they were more soluble, (b) their subsequent steady-state permeation rates, and (c) their partition between liquid paraffin and the OPP membrane. 相似文献
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H. J. Van Den Top A. Boenke P. A. Burdaspal
J. Bustos
H. P. Van Egmond T. Legarda
A. Mesego A. Mouri o W. E. Paulsch C. Salgado 《Food Additives & Contaminants》2000,17(6):419-433
This paper describes the first part of a project undertaken to develop mussel reference materials for Paralytic Shellfish Poisoning (PSP) toxins. Two interlaboratory studies were undertaken to investigate the performance of the analytical methodology for several PSP toxins, in particular saxitoxin (STX) and decarbamoyl-saxitoxin (dc-STX) in lyophilized mussels, and to set criteria for the acceptance of results to be applied during the second part of the project: the certification exercise. In the first study, 18 laboratories were asked to measure STX and dc-STX in rehydrated lyophilized mussel material and to identify as many other PSP toxins as possible with a method of their choice. In the second interlaboratory study, 15 laboratories were additionally asked to determine quantitatively STX and dc-STX in rehydrated lyophilized mussel and in a saxitoxin-enriched mussel material. The first study revealed that three out of four postcolumn derivatization methods and one pre-column derivatization method sufficed in principle to determine STX and dc-STX. Most participants (13 of 18) obtained acceptable calibration curves and recoveries. Saxitoxin was hardly detected in the rehydrated lyophilized mussels and results obtained for dc-STX yielded a CV of 58% at a mass fraction of 1.86 mg/kg. Most participants (14 out of 18) identified gonyautoxin-5 (GTX-5) in a hydrolysed extract provided. The first study led to provisional criteria for linearity, recovery and separation. The second study revealed that 6 out of 15 laboratories were able to meet these criteria. Results obtained for dc-STX yielded a CV of 19% at a mass fraction of 3.49mg/kg. Results obtained for STX in the saxitoxin-enriched material yielded a CV of 19% at a mass fraction of 0.34mg/kg. Saxitoxin could not be detected in the PSP-positive material. Hydrolysis was useful to confirm the identity of GTX5 and provided indicative information about C1 and C2 toxins in the PSP-positive material. The methods used in the second interlaboratory study showed sufficiently consistent analysis results to undertake a certification exercise to assign certified values for STX and dc-STX in lyophilized mussel. 相似文献
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《造纸信息》2014,(8):75-75
In the English section of this issue, 〈China Paper Newsletters〉 will introduce "National Development and Reform Commission Issued Announcement for Selection of Major Preliminary Research Projects for the '13th Five-Year Plan'", "2013 Annual Report of China's Paper Industry", and news of projects and other policies. 相似文献
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《纺织机械》2014,(3)
正Nowadays,textile enterprises are all taking efforts in transformation and upgrading,like improving producing capacity and optimizing production structure to face market downturn.It claimed a higher request to the standard of textile equipments.In the upcoming of ITMA ASIA+CITME 2014exhibition,this magazine have interviewed several branch associations and a series of relative enterprises,to summarize industrial developing status 相似文献