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精制L-乳酸的分子蒸馏工艺研究 总被引:12,自引:0,他引:12
分子蒸馏技术是一种在高真空条件下进行的连续蒸馏过程,适合于分离高沸点、热敏性及具有生物活性的混合物。今研究了用分子蒸馏技术对L-乳酸进行精制的工艺条件;实验过程中粗乳酸原料不需要进行其它脱水及脱色方法处理,只需通过两次分子蒸馏,即可得到高纯度的L-乳酸。考察了分子蒸馏工艺操作过程的蒸馏温度、进料速率、刮膜器转速等因素对L-乳酸收率及纯度的影响。发现适宜的分离工艺是:操作压力0.1Pa,蒸发温度55~75℃,进料速率90mLh-1,刮膜器转速110~130rmin-1,其中蒸发温度和进料速率是影响产品L-乳酸纯度的最重要的因素。 相似文献
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From the measurement of liquid flow field on a large plate by a hot-film anemometer, three different regions on the large plate were presented, including a liquid circulation area near the inlet down-comer, a region with very slow moving or stagnant liquid on the side of the tray and an active flow region at the center of the plate. According to the contribution of the three regions, the tray efficiency for large plates was proposed. The prediction plate efficiency by the present model are compared with the experimental data in the literature and those calculated by other models. It is shown that the present model is more accurate for prediction of efficiency of large plates, and the calculation is simpler. 相似文献
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This paper proposes a modified operation mode of batch extractive distillation with two reboilers.The separation of ethanol and water using as ethylene glycol is well done to validate the feasibility of this mode.The pilot-plant experimental data under the identical operational conditions between the regular mode and the modified mode are in particular discussed.The studied results prove more practical advantages of the modified mode over the regular mode such as easier operation control,more flexibility and higher separation efficiency etc.So it supplies certain guidance for the industrial application of batch extractive distillation process. 相似文献
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