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81.
82.
Biofuels are set to play an important role in the future strategy of automotive fuel suppliers, and therefore the study of using alcohols in spark ignition engines has become a necessity. A simple thermodynamic model was developed for calculating air–fuel mixture parameters for port injection engines fueled with gasoline–isobutanol blends, and theoretical results were compared to experimental values. For simulating the evaporation process, gasoline was considered a mixture of four components, with isobutanol added in different proportions. As all engine components are at ambient temperature during cold starts, mixture formation was considered an adiabatic process, with the fuel breaking up into droplets and evaporating, thus resulting in a temperature drop. A port injection engine fitted to a passenger car was used to validate the model for calculating air–fuel mixture parameters. 相似文献
83.
Lixia Cheng Zhipeng Xie Guanwei Liu 《Journal of the European Ceramic Society》2013,33(15-16):2971-2977
By adding a small amount of tungsten carbide (WC) as sintering aids, nearly fully dense TiC ceramics were obtained by spark plasma sintering at 1450–1600 °C. The results show that the densification temperature of TiC ceramic was significantly decreased with the addition of 3.5 wt% WC. Compared with the monolithic TiC, the densification temperature of TiC–3.5 wt% WC is lower by ~150 °C and no deterioration of mechanical properties is observed. The TiC composite sintered at 1600 °C exhibits full density, a Vickers hardness of 28.2 ± 1.2 MPa, a flexural strength of 599.5 ± 34.7 MPa and a fracture toughness of 6.3 ± 1.4 MPa m1/2. 相似文献
84.
Pramoda K. Nayak Hao-Tung Lin Man-Ping Chang Wei-Hsio Chen Jow-Lay Huang 《Journal of the European Ceramic Society》2013,33(15-16):3095-3100
We report the synthesis of a new class of Al2O3–WC nanocomposites for the first time by using metal–organic chemical vapor deposition process in a spouted bed followed by spark plasma sintering technique. The microstructure and mechanical properties of these prepared nanocomposites have been analyzed for various sintering parameters. From microstructure observation, it is found that the nanosized WC particles are dispersed within alumina matrix grains and intergrains. The microstructure of transgranular and step-wise fracture surface are found in these nanocomposites. The basic mechanical properties like density, hardness, and toughness also have been analyzed and the results are interpreted by correlating with that of corresponding microstructures. 相似文献
85.
《应用陶瓷进展》2013,112(4):251-256
AbstractDensification is an exothermic process according to the classical sintering theories; however, it has never been explored experimentally. In the present work, such heat release was successfully detected from nanosized BaTiO3 nanopowder compact, which was rapidly consolidated by spark plasma sintering. A reduction of total power consumption was observed immediately when rapid densification occurred. The effects of the deviation of overall electric resistance on total power consumption were analysed. The temperature at which a falling inflection point of the power supply was observed can be used as an indicator of the minimum temperature required for densification. This would be of help for defining the ‘kinetic window’ for processing of nanoceramics in sintering practice. 相似文献
86.
R. Ohser-Wiedemann U. MartinH.J. Seifert A. Müller 《International Journal of Refractory Metals and Hard Materials》2010
Pure molybdenum was sintered with SPS under various temperatures, external pressures and heating rates. The microstructure of the specimens representing the different sintering conditions was investigated by classical metallographic methods. The relative density, the microhardness and the chord length distribution were measured. Linear shrinkage, depending on time or temperature, was calculated from piston travel, which was recorded during sintering process. These results show that the main part of consolidation takes place during fast heating up. The densification behaviour is controlled mainly by sintering temperatures and applied pressure. The molybdenum powder was successfully consolidated by SPS in very short times. A relative density of 95% was reached by sintering temperatures of 1600 °C and external pressure of 67 MPa. 相似文献
87.
N. Taefi 《Cement and Concrete Research》2010,40(7):1114-1119
Measurement of the cement powder composition as a major building material is considered very important. In this paper the capabilities of Spark Induced Breakdown Spectroscopy (SIBS) as a new technique for analysis of cement powder are shown. The major and minor elements of cement such as Ca, Si, Fe, K, Mg, Al, Na, Ba, Ti, V, Pb, Mn and Sr are detected qualitatively. For quantitative measurement, calibration curves are prepared for elements Ca, Si, Mg, Al, Fe and K with limit of detection below 220 ppm. The critical problems such as how to achieve quantitative measurement and improve the detection limits are investigated. The potential and drawbacks of SIBS technique in comparison with XRF for analysis of powder products are discussed. 相似文献
88.
《应用陶瓷进展》2013,112(4):240-247
Abstract Abstract The structural and chemical stability of multiwall carbon nanotubes (MWNTs) in ceramic nanocomposites prepared by spark plasma sintering was studied. High resolution electron microscopy, X-ray diffraction and Raman spectroscopy were used to evaluate any degradation of the MWNTs. They were found to be well preserved in alumina after sintering up to 1900°C/100?MPa/3?min. In boron carbide, structural degradation of MWNTs started from ~1600°C when sintered for 20?min. Multiwall carbon nanotubes maintained their high aspect ratio and fibrous nature even after being sintered in boron carbide at 2000°C for 20?min. However, no Raman vibrations of MWNTs were observed for nanocomposites processed at temperatures <2000°C, which indicates that they were severely degraded. Structural preservation of MWNTs in ceramic nanocomposites depends on the ceramic matrix, sintering temperature and dwell time. Multiwall carbon nanotubes were not preserved for matrices that require high sintering temperatures (>1600°C) and longer processing times (>13?min). 相似文献
89.
90.
The heat of combustion of two distinctly synthesized stoichiometric tantalum-tungsten oxide energetic composites was investigated by bomb calorimetry. One composite was synthesized using a sol-gel (SG) derived method in which micrometric-scale tantalum is immobilized in a tungsten oxide three-dimensional nanostructured network structure. The second energetic composite was made from the mixing of micrometric-scale tantalum and commercially available (CA) nanometric tungsten oxide powders. The energetic composites were consolidated using the spark plasma sintering (SPS) technique under a 300 MPa pressure and at temperatures of 25, 400, and 500 °C. For samples consolidated at 25 °C, the density of the CA composite is 61.65 ± 1.07% in comparison to 56.41 ± 1.19% for the SG derived composite. In contrast, the resulting densities of the SG composite are higher than the CA composite for samples consolidated at 400 and 500 °C. The theoretical maximum density for the SG composite consolidated to 400 and 500 °C are 81.30 ± 0.58% and 84.42 ± 0.62%, respectively. The theoretical maximum density of the CA composite consolidated to 400 and 500 °C are 74.54 ± 0.80% and 77.90 ± 0.79%, respectively. X-ray diffraction analyses showed an increase of pre-reaction of the constituents with an increase in the consolidation temperature. The increase in pre-reaction results in lower stored energy content for samples consolidated to 400 and 500 °C in comparison to samples consolidated at 25 °C. 相似文献