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Olivine-type LiFePO4/C composite cathode materials were synthesized by a solid-state reaction method in an inert atmosphere. The glucose was added as conductive precursors before the formation of the crystalline phase. The effects of glucose content on the properties of as-synthesized cathode materials were investigated. The crystal structure and the electrochemical performance were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), laser particle-size distribution measurement and electrochemical performance testing. The material has a single crystal olivine structure with grain-sizes ca. 100-200 nm. SEM micrographs and the corresponding energy dispersive spectrometer (EDS) data confirm that the carbon particulates produced by glucose pyrogenation are uniformly dispersed among the LiFePO4 grains, ensuring a good electronic contact. Impedance spectroscopy was used to investigate the ohmic and kinetic contributions to the cell performance. It is found that increasing the carbon content leads to a reduction of the cell impedance due to the reduction of the charge transfer resistance. The galvanostatically charge and discharge tests show that the material obtained by adding 10% C (by mass) gives a maximum discharge capacity of 140.8mA·h·g^-1 at the same rate (C/10). The material also displays a more stable cycle-life than the others. 相似文献
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北京南站冷热电三联供系统探讨 总被引:2,自引:0,他引:2
介绍了北京南站冷热电三联供系统设计,包括方案选择、负荷计算、系统配置、运行策略、节能分析等。认为使用燃气内燃机比燃气轮机更具优势,建议在电力并网前提下采用以电定热原则确定系统设备容量配置。 相似文献
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Olivine-type LiFePO_4/C composite cathode materials were synthesized by a solid-state reaction method in an inert atmosphere.The glucose was added as conductive precursors before the formation of the crystalline phase.The effects of glucose content on the properties of as-synthesized cathode materials were investigated.The crystal structure and the electrochemical performance were characterized by X-ray diffraction(XRD),scanning electron microscopy(SEM),laser particle-size distribution measurement and electrochemical performance testing. The material has a single crystal olivine structure with grain-sizes ca.100-200 nm.SEM micrographs and the corresponding energy dispersive spectrometer(EDS)data confirm that the carbon particulates produced by glucose pyrogenation are uniformly dispersed among the LiFePO_4 grains,ensuring a good electronic contact.Impedance spectroscopy was used to investigate the ohmic and kinetic contributions to the cell performance.It is found that increasing the carbon content leads to a reduction of the cell impedance due to the reduction of the charge transfer resistance.The galvanostatically charge and discharge tests show that the material obtained by adding 10% C(by mass)gives a maximum discharge capacity of 140. 8mA.h.g~(-1) at the same rate(C/10) .The material also displays a more stable cycle-life than the others. 相似文献
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通过CFD模拟计算给出了北京南站高架层环形车道夏季最不利条件下各区域的空气品质.结合国家标准<环境空气质量标准>和香港环保署颁布的<半封闭式公共交通换乘站地区空气污染控制>要求,分析了环形车道内的污染物浓度分布,认为其空气品质基本满足安全卫生要求.根据模拟计算给出了新风取风口的设置位置. 相似文献
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新型空气过滤器检测系统 总被引:2,自引:0,他引:2
提出一套将高效过滤器检测系统与一般通风用空气过滤器检测系统合二为一的过滤器性能检测系统的方案,效率检测采用计径计数法,并按此方案搭建了实验装置。经实验,该测试系统及检测结果均符合过滤器测试要求,可实现自动化检测,检测更方便,测试结果更可靠。 相似文献