排序方式: 共有75条查询结果,搜索用时 31 毫秒
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采用有机金属裂解法在Pt/TiO2/SiO2/Si基板上制备M型钡铁氧体(Ba M)薄膜,并着重研究了螯合剂乙二胺四乙酸(EDTA)含量对Ba M薄膜结构、磁性和微波性能的影响。研究发现,当EDTA∶(Ba2++Fe3+)=1(摩尔比)时,Ba M薄膜形成较多的六角形状晶粒,而且磁性能和微波性能较佳,沿c轴生长的取向度高达0.91,饱和磁化强度Ms为302k A/m(μ0Ms=0.38T),在50GHz时铁磁共振线宽ΔH为22k A/m(277Oe)。这是因为适量的EDTA不仅在溶液挥发时能够阻止金属离子的分离和间歇性的沉淀,并且能够促进成形成均匀的前驱液,从而在前驱液分解时能促进形成Ba M,在经过热处理后易形成沿c轴取向、具有六角形状晶粒的Ba M薄膜。 相似文献
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以醛、酮为原料经羟醛缩合反应合成了具有一类含查尔酮结构的光敏性二胺:1-(3-氨基苯基)-3-(4-氨基苯基)-2-丙烯-1-酮与对-二(间氨基肉桂酰)苯.通过优化实验得到最佳的合成工艺为:醛、酮在温度为0℃下,以乙醇为溶剂,氢氧化钠为催化剂,进行羟醛缩合反应3h.收率可达到86%,经液相色谱分析其纯度分别为99.92%,99.91%,紫外可见最大吸收波长分别为349nm、361nm.所得方法操作简便,收率较高,原料易得.并用元素分析、核磁共振、红外光谱等手段对产物的结构进行了表征. 相似文献
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平面Z-型软磁铁氧体频率特性的研究 总被引:2,自引:0,他引:2
研究分析了Co2Z材料显微结构与磁性能的关系,在普通铁氧体工艺中引入预磁化处理方法,并适当控制二次再结晶现象,成功地研制出高性能的Co2Z型宽频材料,Z-型铁氧体材料的共振频率可达1.8GHz以上,截止频率在1GHz附近,起始磁导率在8-13之间,介电常数相对较低(ε'<30)。 相似文献
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Rare earth permanent magnets Sm(Co, Fe, Cu, Zr)z with outstanding performance and high-temperature thermal stability were fabricated. Optimized by Fe content and process, Sm(Co0.72Fe0.15Cu0.1Zr0.03)7.5 magnet with B1〉0.75 T and Hci〉1300 kA/m at 300 ℃ can be obtained. According to the performance data of Sm(Co0.72Fe0.15Cu0.1Zr0.03)7.5, the magnetic field along central axis Bz in periodic permanent magnet (PPM) focusing system was simulated using electromagnetic field analysis software Maxwell 2D/3D. The Bz exhibited typical cosine curve along central axis, and the peak value of Bz was high enough to meet the demand of PPM focusing system at room temperature even at 200±20 ℃. Additionally, a kind of simple cooling structure for PPM focusing system was designed by setting cooling pipe between polepieces. Simulated results showed that smooth cosine curve of Bz was successfully achieved with good control of the thickness of cooling pipe. 相似文献
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