滴定法测定饲料添加剂中硫酸亚铁含量的不确定度探讨

依据HG2935—2000饲料级一硫酸亚铁标准规定,对重铬酸钾滴定法测定硫酸亚铁含量的不确定进行了评定,建立了测量过程中各个分量的数学模型,并估算了各不确定度分量对总不确定度的影响。结果表明,在置信概率水平为95％时,硫酸亚铁含量测量结果报告为x=（80．34±0．48）％,k=2。该方法适用于硫酸亚铁含量的不确定评定,其中影响硫酸亚铁含量的不确定度主要来源是滴定体积所引入。     

Chaos from second-order PLL in presence of CW interference

The chaotic behaviour of a second-order phase-locked loop (PLL) in the presence of continuous wave (CW) interference is examined. The Lyapunov exponents and dimension of the system are calculated to confirm the chaotic phenomenon. A range of interfering signal power and frequency has been found where chaos could occur     

Biomass yield and energy analysis of soybean production in relation to fertilizer-NPK and organic manure

The study attempts to quantify the root biomass and density, nodulation, crop biomass and grain yield of soybean, to analyze crop growth and energy (renewable and non-renewable) inputs in relation to fertilizer-NPK and organic manure. Observations were recorded from soybean grown with no fertilizer, NPK and NPK + FYM (farmyard manure). The root biomass (BM_root) increased significantly with NPK + FYM compared to NPK and control. The trend of BM_root was best fitted with a third order polynomial. Root length density was higher in NPK + FYM. Biomass of stem, petiole and leaf were significantly greater in NPK + FYM than other treatments, relative contribution to total biomass at physiological maturity were stem 29%, petiole 9%, leaf 17% and pod 46%; quadratic regression models best represented the stem, petiole and leaf biomass data. A maximum LAI of 4.88, total biomass of 633 g m^?2 at maturity, CGR of 18.4 g m^?2 d^?1 were recorded in NPK + FYM. Grain yields increased by 72.5 and 98.5%, and stover yields by 56.0 and 94.8% in NPK and NPK + FYM, respectively over control. Though the total energy input in NPK + FYM was greater than those in NPK and control, the share of renewable energy was much higher with greater net energy output and non-renewable energy productivity in NPK + FYM than NPK. The use efficiency of non-renewable energy was also higher in NPF + FYM. Thus, a combination of NPK-fertilizer and organic manure (FYM) could be the viable nutrient management option for soybean production.     

土壤中铅铬铜铁锌锰钙的测定

报道使用全酸法消解土壤，并用同一消解液分剐测定土壤中的铅、铬、铜、铁、锌、锰、钙等金属元素。其中铅使用原子荧光光谱法测定，其他元素使用火焰原子吸收光谱法测定。方法准确、快速、简便，适用于环境土壤中多种元素的测定，结果满意。     

Phase detector for data-clock recovery circuit

A new type of phase detector which can be used in data-clock recovery circuits is reported. The main feature of the proposed phase detector is that it is free front data dependent jitter, which is the main problem with the Hogge phase detector