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排序方式: 共有162条查询结果,搜索用时 15 毫秒
1.
Ahmadi Ameneh Sedaghat Tahereh Azadi Roya 《Journal of Inorganic and Organometallic Polymers and Materials》2021,31(10):4126-4140
Journal of Inorganic and Organometallic Polymers and Materials - 3-Chloropropyltrimethoxysilane (CPTMS) was grafted on the surface of silica coated Fe3O4 core (Fe3O4@MCM-41) and then condensed with... 相似文献
2.
Jalalzadeh-Esfahani Mehrnoosh Sedaghat Tahereh Beheshti Azizollah Azadi Roya 《Journal of Porous Materials》2022,29(4):1149-1164
Journal of Porous Materials - Benzimidazole functionalized mesoporous silica nanoparticles immobilized Pd(0)/Pd(II) has been proposed as an efficient catalyst for the one-pot preparation of biaryls... 相似文献
3.
Fire resistance of structural members is dependent on the thermal and mechanical properties of constituent materials and these properties vary as a function of temperature. Currently, there are limited standardized test procedures for evaluating thermal and mechanical properties of construction materials at elevated temperatures. This paper provides a review and assessment of test methods and procedures for evaluating high temperature thermal and mechanical properties of concrete. The drawbacks and variations in currently available test procedures and methods in standards are discussed. Recommendations on the most suitable methods and procedures for measuring thermal and mechanical properties at elevated temperature is presented. In addition, applicability of the proposed high temperature test methods and procedures is illustrated through a case study on conventional concrete specimens. Further, the need for developing standards by organizations such as American Society for Testing and Materials (ASTM), with standardized specifications and test procedures for measuring high temperature properties of construction materials, is laid out. 相似文献
4.
Adhesion plays an important role in the final properties of nanocomposites. This study explored the surface interaction of
cellulose nanocrystals (CNCs) and the effect of CNC sources on adhesion between individual CNCs and the Si tip of an AFM cantilever
using a force mapping technique called FMap. The adhesion between CNCs and a Si tip from five different sources has been studied:
cotton, Whatman filter paper, hemp, softwood chemical kraft pulp, and softwood-dissolving pulp (alistaple). Mica was used
as the background substrate to act as an internal standard. This study’s findings suggest that adhesion is not the same for
all CNCs. Transmission electron microscopy and atomic force microscopy were used to determine the size and shape of each CNC.
The experimental quantitative data showed that adhesion between CNCs and the Si tip has a close correlation with the diameter
of the CNCs. X-ray photoelectron spectroscopy confirmed the presence of sulfate groups on the surface of the CNCs and a correlation
between adhesion and surface chemistry of the CNCs was observed. 相似文献
5.
6.
Arrays of precisely positioned single crystal silicon nanopillars, nanoneedles, and nanoblades with minimum feature sizes as small as 30 nm are fabricated using entirely scalable top-down fabrication techniques. Using the same scalable technologies, devices consisting of electrically connected silicon nanopillars with multiple addressable electrodes for each nanostructure are realized. The arrays of nanopillars, nanoneedles, and nanoblades are shown to exhibit Raman signal enhancement on 1,2-benzenedithiol monolayers, opening a path to nanodevices that manipulate, position, detect and analyze molecules. 相似文献
7.
A new approach for nonenzymatic glucose sensing, based on a simple modification of epoxy-silver surfaces deposited on the tip of commercial copper electric wires, is presented. Palladium was galvanically displaced on the surface of the epoxy-silver surface in order to obtain metal nanoparticles that act as catalyst for the direct oxidation of glucose. Scanning electron microscopy revealed the formation of the metal nanoparticles. X-ray photoelectron spectroscopy confirmed the metallic nature of the formed nanostructures on the surface. Electrochemical characterization and calibration of the palladium-modified epoxy-silver electrode is reported, obtaining a linear range of 1–20 mM for the detection of glucose with low interference of ascorbic acid and uric acid. A simple 3-step coulometry was used as the detection technique. The developed sensing material is believed to be a great candidate for integration in small devices for clinical essays, due to the simplicity and cost effectiveness of the presented approach, compared to the state-of-the-art devices reported recently in the literature. Simplicity in the coulometry determinations makes these Pd-modified epoxy-silver sensors a good candidate for easy glucose determinations. 相似文献
8.
A galvanic displacement technique is used to coat silicon scanning force microscopy cantilevers with copper. The copper coating is characterized using X-ray photoelectron spectroscopy, scanning force microscopy, contact angle measurements, scanning electron microscopy and energy-dispersive X-ray spectroscopy. This coating technique results in uniform, reflective and conformal films and hence, no stress-induced bending of the cantilever is observed. To demonstrate the effectiveness of this approach for tribological studies, the coated cantilevers are chemically modified with alkanethiol monolayers in order to functionalize the cantilevers. The effect of changed surface energy are detected with adhesion measurements in water and ethanol. 相似文献
9.
Ian Laboriante Maxwell Fisch Amir Payamipour Fang Liu Carlo Carraro Roya Maboudian 《Tribology Letters》2011,44(1):13-17
The evolution of morphology, electrical properties, and chemical composition has been studied in cyclically contacting polycrystalline
silicon (polysilicon) surfaces coated with perfluoroalkylsilane self-assembled monolayer (SAM). The microinstrument used is
a MEMS cantilever that is repeatedly actuated out-of-plane to impact a landing pad and is then moved in-plane to enable nondestructive
in situ inspection of the impacted area. Analyses show that a device with a monolayer coating exhibits signs of surface degradation
after a much higher number of cycles than its uncoated counterpart. A sharp increase in contact resistance between the cantilever
and landing pad is observed at ~10 billion cycles for a coated device, versus ~25 million cycles for an uncoated device. Likewise,
the onset of grain fracture in the landing pad occurs at ~25 billion cycles for the SAM-coated device, versus ~3 billion cycles
for its uncoated counterpart. The effectiveness of the monolayer coating diminishes after more than 100 billion contact cycles
as the SAM layer is removed, and the polysilicon substrate becomes susceptible to adhesive wear. 相似文献
10.
We developed an alternative approach for measuring information and communication technology (ICT), applying Data Envelopment Analysis (DEA) using data from the International Telecommunications Union as a sample of 183 economies. We compared the ICT-Opportunity Index (ICT-OI) with our DEA-Opportunity Index (DEA-OI) and found a high correlation between the two. Our findings suggest that both indices are consistent in their measurement of digital opportunity, though differences still exist in different regions. Our new DEA-OI offers much more than the ICT-OI. Using our model, the target and peer groups for each country can be identified. 相似文献