离子交换树脂对长春花中文多灵、长春质碱和长春碱的富集研究

通过D-113、110、D-151、NKC-9、001x7、D-072、D-062离子交换树脂对长春花中文多灵、长春质碱和长春碱的静态吸附容量、吸附率和解吸率等指标的考察,筛选出最佳树脂为D-151.对文多灵、长春质碱和长春碱的吸附容量分别为118.2mg/mL、102.2mg/mL和2.6mg/mL,并进一步考察其富集长春花3种生物碱的吸附和解吸附性能,确定了最佳的工艺条件和参数.吸附:上样溶液浓度为0.41mg生药/mL, pH为6.0,流速为3mL/min;解吸附:洗脱剂为20%乙醇除杂,90%乙醇(含2%氨水)洗脱.结果表明,经D-151离子交换树脂富集的长春花总生物碱中文多灵、长春质碱和长春碱的含量分别提高到34.53%、22.31%和5.86%,比传统溶剂萃取方法分别提高了2.34、3.49和2.07倍,回收率均在90%以上,D-151离子交换树脂可以用来富集长春花中的生物碱成分.     

长径比对侵彻阻力的影响

基于经典空腔膨胀理论、Forrestal阻力修正模型和加速度阻力模型研究了战斗部侵彻强度靶过程中长径比对于侵彻阻力的影响,通过对不同长径比条件下战斗部侵彻余速的计算,分析了长径比对阻力项系数的影响,讨论了3种理论的适用范围。结果表明:当战斗部长径比小于3时,加速度阻力项系数变化对侵彻过程影响较大;当长径比大于5时,3个模型的计算结果趋于一致,均适用于工程计算。     

一种可实现收发一体连续扫描的微透镜阵列

设计了一种可实现收发一体连续扫描的微透镜阵列,该三片式微透镜阵列以加入场镜的开普勒望远结构为原型,通过微透镜阵列之间的微小横向位移进行接收视场的选择与发射光线的同步偏转,完成扫描光学系统对大视场区域的光束收发。设计约束望远镜的视觉放大率为1,即入射和出射端口的微单元通光孔径相等,从而实现收发共用且不会造成能量损失和串扰。利用ZEMAX光学设计软件,采用发射、接收端口单独设计然后拼接的方法搭建模型。微透镜阵列工作中心波长为1 064 nm,凝视视场为±1.06°,扫描视场为±10°,单元规格为1 mm×1 mm,且只需移动一片即可实现双向扫描,具有体积小、扫描角度大、灵敏度高等优点。     

TOPOPIC对强流束流在周期FODO结构中的传输研究

粒子云网格(Particle In cell,PIC) 方法是研究带电粒子在加速器中运动的关键工具之一。基于PIC 算法,开发了模拟强流条件下的束流动力学模拟程序TOPOPIC(Trace of Particle Orbit with PIC method),并且利用TOPOPIC,研究了束流在四极铁周期结构(FODO) 中的传输问题。结果表明,在强流条件下空间电荷效应显著地影响了束流的整体行为和单粒子的运动轨迹。最后比较了TOPOPIC 程序和通用的BEAMPATH 程序在相同条件下的计算结果,可以看到两个程序给出的模拟结果吻合得非常好,这表明TOPOPIC程序的计算结果是合理、可靠的。The Particle in cell (PIC) method is one of the key techniques in the research of charged particles in accelerators. Based on the PIC method, a new beam simulation code for high intensity beam named TOPOPIC (Trace of particle orbit with PIC method) has been developed. With the code TOPOPIC,the beam behavior during passing through the periodic quadrupole (FODO) structure has been studied. The results show that the nonlinear space charge affects the single particle behavior and beam envelope a lot. At last, the PIC code BEAMPATH is used for benchmark, the results given by TOPOPIC and BEAMPATH show good agreements,which means the code TOPOPIC is reliable.     

具有内核伸出段的套管构件点接触力学模型研究

针对轴向压力作用下具有内核伸出段的套管构件,理论研究了初弯曲内核与柔性套筒的点接触变形过程.采用小挠度二阶平衡微分方程,推导了内核处于点接触状态时套管构件的挠度、剪力、弯矩、接触力等物理量的计算公式.理论的对比结果表明:1)内核伸出段会显著增大套管构件的弯曲轴向位移,降低套管构件的非线性轴向刚度;2)内核伸出段使内核与套筒端部的接触反力有显著的增加,随着轴向压力的增大,该接触反力的增加更大;3)内核伸出段使内核的剪力、弯矩均有显著的提高,尤其在内核与套筒抗弯刚度比值较大时,弯矩的提高更显著.该文的研究可为套管构件及内核与套筒端部连接的设计提供依据.     

替代反应法测量锕系核(n,f)和(n,xn)截面

对于某些中子反应截面,在直接测量上存在困难。为了获得那些对核能发展极其重要的核数据,人们提出替代反应法,即利用带电粒子代替中子进行反应,从而实现中子反应截面间接测量的方法。现有替代反应一般采用非弹激发、转移等周边反应,涉及的角动量远比中子反应的大,需要理论修正,这造成了一定的困难。有鉴于此,提出利用轻带电离子的俘获反应作为替代反应,其复合核自旋与中子反应的相当,有效避免了自旋修正的困难。根据这个思路,采用236U的（α,f）和（α,2n）反应作为替代反应,成功提取了239Pu的（n,f）和（n,2n）反应截面,与ENDFB7评价库数据在误差范围内符合较好,表明了替代反应法的优越性,可以在核数据测量中推广应用。There are always difficulties in the direct measurement of reactions induced by neutron, in order to obtain the neutron induced nuclear reaction data which are extremely important for nuclear power development, the surrogate reaction method, which uses charged particles instead of neutron, was proposed. The existing surrogate reaction method generally chooses peripheral reaction as the surrogate reaction, such as inelastic scattering excitation or transfer reaction. As a result, the angular momentum involved is always far larger than the neutron induced reaction, which causes difficulties in the theoretical calculation. Because of this, we proposed to use light-ion capture reaction as the surrogate reaction, the compound nuclei spin is similar with that of the neutron induced reaction, so that the difficulties in spin correction can be effectively avoided. Based on this idea, the 239Pu(n, f) and (n, 2n) reaction cross sections were successfully extracted using 236U(α,f) and (α,2n) reactions as the surrogate reaction. The results coincide well with the data of ENDFB7 within the error range, which shows that the surrogate reaction method has its own superiority, and it can be applied in the measurement of nuclear data.     

单颗LED实现远距离均匀照明系统设计

针对现有的LED照明系统体积大、结构复杂、工作距离短的缺点,提出一种轻量化、均匀性好、能够实现远距离照明的单颗LED投影系统的设计方法。从照明设计理论出发,结合非成像设计和成像设计方法,设计了由单颗大功率LED、聚光镜、孔径光阑和投影物镜组成的投影照明系统。聚光镜对LED出射的光线进行匀化并会聚于照明面位置,投影物镜将照明面处的光斑投影到指定距离的接收面上。系统采用全透射式结构,便于加工和装调;单颗大功率LED作为光源能够有效减小系统体积和质量。实验结果表明:系统能在3 m~3 km范围内形成均匀度大于90%的照明,成像质量良好,投影面畸变小于5%,能满足远距离均匀照明投影的要求。     

氯硝西泮及其代谢产物7-氨基氯硝西泮的化学合成

以2-氰基-4-硝基苯胺为原料，经氧化偶联、酰胺化、亲核取代反应、分子内Wittig反应、还原反应等过程实现了7-氨基氯硝西泮的化学合成，在反应完成后可以直接过滤淋洗即可得到产物，无需其他纯化，操作简便。      

基于色散位移光纤的高宣布式窄带单光子源

文章利用脉冲激光抽运色散位移光纤,通过自发四波混频过程产生的关联光子对,实验演示了一种光通讯波段的窄带宣布式单光子源. 实验测得-3 dB带宽为1.1 nm单光子场的二阶关联函数g⁽²⁾(0)=0.09±0.01,宣布效率可达0.5以上. 这种单光子源在量子通信中有潜在的应用前景. 关键词： 宣布式单光子 光纤 自发四波混频 量子通信     

Dynamic behavior and complexity of modulated optical micro ring resonator

The dynamic behavior of an optical micro ring resonator (OMRR) with an amplitude modulator positioned in the micro ring is investigated quantitatively by adopting a recently introduced quantifier, the permutation entropy (PE). The effects of modulation depth are focused on, and the roles of input power are considered. The two-dimensional (2D) maps of PE showing dependence on both modulation depth and input power are presented as well. PE values nearly increase with modulation depth. On the other hand, the optimal value of input power is achieved when the PE reaches its maximum. Thus, PE can successfully quantify the dynamics of modulated OMRR. Selecting the parameters in the region with high PE values would contribute to the complexity-enhanced OMRR-based chaotic communication systems.