环形粉末预制坯压制规律研究

研究了环形粉末预制坯压制过程中压力和密度变化规律。通过力学分析建立了环形粉末预制坯压制力学模型，导出了6种压制方式下压制力沿预制坯高度分布规律，建立了统一的压制力分布计算公式，并计算了环形粉末预制坯下端面的最小压制力。基于黄培云粉末压制理论，导出了环形粉末预制坯相对密度沿高度分布计算公式，以及环形粉末预制坯上下端面密度的比值。     

金属粉末体压制成形过程模型的研究

通过对“６．３ＭＮ粉末成形液压机”的研制，对金属粉末体压制过程的数学模型和有限元模型进行了研究，对其密度、应力、应变分布进行了分析。建立并推导了刚塑性有限元材料体积可压缩性法中参数ｇ与粉末体相对密度ρ之间的关系式，用来动态模拟粉末体压制过程。为粉末体压制过程的模拟提供了一种新思路。该方法也可用于烧结后粉末体压制模拟。     

粉末低电压电磁压制实验研究

将低电压电磁成形方法用于粉末材料压制 ,采用间接加工方式对铝、铜、锡粉进行了压制实验 ,在成功压制出高密度粉末制品的基础上 ,分析了电压、电容、摩擦、压制次数、粉末粒度等因素对制品压实密度的影响。实验结果表明 ,对不同粉末材料 ,在保证一定加载速率和放电能量的前提下 ,降低电压和增加电容 ,有利于提高粉末制品压实密度及其均匀性 ;电压越高 ,摩擦能量消耗率越大 ;当设备放电能量有限时 ,多次压制是获得致密均匀、高密度粉末制品的有效途径     

电磁成形技术在粉末成形中的应用

介绍了电磁成形技术、粉末挤压成形方法以及电磁成形技术在粉末成形中的应用.用电磁成形技术压制粉末材料是获得高密度、高性能粉末冶金制品的一种有效方法,是低成本制造高密度陶瓷零件的新途径.     

金属粉末压制成形理论与工艺进展

描述了粉末压制成形过程中颗粒的移动和变形,并用方程定量描述了压坯密度和压制压力的关系.针对粉末冶金行业近年来出现的提高产品致密化的新途径,描述了温压技术、流动温压技术、粉末电磁压制技术、高速压制技术和电场活化烧结技术的原理、特点和应用情况.     

铝青铜基粉末冶金摩擦材料压制工艺研究

采用实验研究的方法分析不同工艺条件,包括粉末混和、压制压力、压制方法、复压、热复压等对铝青铜基粉末冶金摩擦材料压坯性能的影响.结果表明,压制压力和润滑条件是影响压坯密度的关键因素:双向压制所得压坯质量优于单向压制;提高压制温度有利于提高压坯密度;复压工艺可有效提高压坯的密度和烧结质量.     

连续体塑性力学方法描述粉末金属压制过程

介绍了建立描述粉末金属压制过程数学模型的难点，详细论述了目前运用较多的基于连续体力学的建模方法，即粉末烧结体塑性力学方法和土性力学方法。分析、比较两种方法的优劣，并对建模工作提出了展玫地性意见。     

铝粉末模压成型有限元模拟

基于金属粉末材料的塑性变形理论及Shima-Oyane屈服函数,采用体积可压缩有限元法和Marc有限元软件对纯铝粉末单向及双向模压过程进行了三维有限元模拟,探讨了粉末材料在两种模压过程中的变形特征和流动规律.模拟结果表明,同等载荷条件下,双向压制与单向压制相比,能够获得密度更高及更均匀的压坯,但两者都存在局部高密度区和低密度区;随着压力载荷的增加,平均相对密度快速增加,然后趋于饱和.模拟结果对压制工艺的制定有指导意义.     

粉体压制过程密度变化机理及影响因素模拟分析

采用MSC.MARC有限元模拟软件对轴套粉体压制成形过程中粉末的位移走向和粉末位移对生坯相对密度的影响进行研究。同时,研究了不同模壁润滑条件以及不同厚度高度比对生坯密度分布的影响。结果表明,粉体成形过程中模壁摩擦导致的位移滞后效应决定了生坯最终的相对密度分布状况;粉末的位移变化规律与生坯的密度分布相似。随着模壁润滑条件的改善和高度厚度比的增加,生坯的密度分布均匀性得到提高;尤其是采用特殊润滑时,生坯密度均匀性得到了明显的改善。这些为研究粉体压制致密化过程提供了理论参考依据。     

MCrAlY熔覆粉末单向冷压成形过程的数值分析及验证

利用大型有限元软件MSC.MARC对MCrAlY熔覆粉末单向冷压成形过程进行了数值模拟分析.建立了粉末片压制成形过程的二维有限元模型,确定了MCrAlY熔覆粉末的材料模型、单向冷压成形过程的初始条件和边界条件,获得了粉末单向冷压过程中沿其高度和直径方向位移的变化规律.提出将粉末片最大相对密度作为其理论相对密度,获得了粉末片孔隙度、致密度、相对密度及其高度随压制力的变化关系.基于Matlab对压制后的粉末片进行图像处理,获得了粉末片的实际高度和粉末片上下表面的相对密度,验证了有限元仿真模型的合理性和可靠性.     

Effects of Post-weld Heat Treatment on Microstructure,Mechanical Properties and the Role of Weld Reinforcement in 2219 Aluminum Alloy TIG-Welded Joints

In as-welded state, each region of 2219 aluminum alloy TIG-welded joint shows diff erent microstructure and microhardness due to the diff erent welding heat cycles and the resulting evolution of second phases. After the post-weld heat treatment, both the amount and the size of the eutectic structure or θ phases decreased. Correspondingly, both the Cu content in α-Al matrix and the microhardness increased to a similar level in each region of the joint, and the tensile strength of the entire joint was greatly improved. Post-weld heat treatment played the role of solid solution strengthening and aging strengthening. After the post-weld heat treatment, the weld performance became similar to other regions, but weld reinforcements lost their reinforcing eff ect on the weld and their existence was more of an adverse eff ect. The joint without weld reinforcements after the post-weld heat treatment had the optimal tensile properties, and the specimens randomly crack in the weld zone.     

The First Phase of the SRIF Industrialized Base in ＂West Area＂ Has Been Put into Operation

After nearly two years＇ tense construction, the first phase of industrialized base of Shenyang Research Institute of Foundry （SRIF）, located at the Tiexi Casting and Forging Industrial Park in the west of Tiexi District, has now been completed and formally put into operation.     

新型的治疗阿尔茨海默氏症药物(1-二甲基磷酰基-2,2,2-三氯)-乙基-1-醇烟酸醋对体外神经细胞的作用

目的: 观察本实验室合成的一种治疗阿尔茨海默氏症(AD)的药物(1-二甲基磷酰基-2, 2, 2 -三氯)-乙基^-1-醇烟酸醋(NMF),对体外培养的皮层神经细胞活性的影响以及对海人藻酸(KA)所致的神经损伤的保护作用。方法: 采用体外培养皮层神经元的方法,解剖分离 15 d胚胎小鼠皮层神经细胞, 接种于 96孔板,48 h 后加药并培养 72 h,以 MIT 法 观察 NMF 对小鼠皮层神经细胞活性的影响;同时将接种于 24 孔板的细胞预先给予 NMF,d 3 时加或不加KA处理后,以台盼蓝染色鉴别并计数死、活细胞,可得出细胞的存活率。结果: NMF 明显促进胎鼠皮层神经元活性,其中 NMF1、0. 1、10nmol·L^-1促进神经元活性增殖率分别高达 34.7%、37.4%、36. 7%, NMF 明显促进正常胎鼠皮层神经元存活卒,与对照组比较,10nmol·L^-1 NMF 对皮层神经元的存活率分别提高 39.3%、73.5%。 NMF能显著 对抗 KA 所致的神经元损伤,与 KA 损伤组相比, NMF0.1、10、10nmol·L^-1对损伤皮层神经元的保护率分别为 77.30%、80.10%、84.15%。结论: NMF 明 显促进胎鼠皮层神经元的洁性、提高正常皮层神经元,的存活卒,并能有效地保护KA所致的神经元损伤,提示 NMF 是一种很有潜力的治疗 AD 的药物。     

Theoretical Analysis for the Motion and Temperature of Melt Droplets in Spray Degassing Process

The motion of melt droplets in spray degassing process was analyzed theoretically. The height of the treatment tank in spray degassing process could be determined by the results of theoretical calculation of motion of melt droplets. To know whether the melt droplets would solidify during spraying process, the balance temperature of melt droplets was also theoretically analyzed. Then proof experiments for theoretical results about temperature of melt droplets were carried. In comparison, the experimental results were nearly similar to the calculation results.     

Growth Kinetics of Single Inclusion Particle in Molten Melts

On the basis of the single-particle framework, a new theory on inclusion growth in metallurgical melts is developed to study the kinetics of inclusion growth on account of reaction and collision. The studies show that the early growth of inclusion depends on reaction growth and Brawnian motion collision, and where the former is decisive, the late growth depends on turbulence collision and Stokes＇ collision, and where the former is dominant; collision growth is very quick during the smelting process, lessened in the refining process, but nearly negligible in the continuous casting process.     

An Easy Way to Quantify the Adhesion Energy of Nanostructured Cu/X(X=Cr,Ta,Mo,Nb,Zr) Multilayer Films Adherent to Polyimide Substrates

An approach based on film buckling under simple uniaxial tensile testing was utilized in this paper to quantitatively estimate the interfacial energy of the nanostructured multilayer films(NMFs) adherent to flexible substrates. The interfacial energies of polyimide-supported NMFs are determined to be *5.0 J/m2 for Cu/Cr, *4.1 J/m2 for Cu/Ta,*2.8 J/m2 for Cu/Mo, *1.1 J/m2 for Cu/Nb, and *1.2 J/m2 for Cu/Zr NMFs. Furthermore, a linear relationship between the adhesion energy and the interfacial shear strength is clearly demonstrated for the Cu-based NMFs, which is highly indicative of the applicability and reliability of the modified models.     

High-Speed Friction Stir Welding of SiC_p/Al–Mg–Si–Cu Composite

A 17 vol% SiCp/Al–Mg–Si–Cu composite plate with a thickness of 3 mm was successfully friction stir welded(FSWed) at a very high welding speed of 2000 mm/min for the first time. Microstructural observation indicated that the coarsening of the precipitates was greatly inhibited in the heat-affected zone of the FSW joint at high welding speed, due to the significantly reduced peak temperature and duration at high temperature. Therefore, prominent enhancement of the hardness was achieved at the lowest hardness zone of the FSW joint at this high welding speed, which was similar to that of the nugget zone. Furthermore, the ultimate tensile strength of the joint was as high as 369 MPa, which was much higher than that obtained at low welding speed of 100 mm/min(298 MPa). This study provides an effective method to weld aluminum matrix composite with superior quality and high welding efficiency.     

Three-Dimensional Growth of Coherent Ferrite in Austenite: A Molecular Dynamics Study

Coherent second phase often exhibits anisotropic morphology with specifi c orientations with respect to both the second and the matrix phases. As a key feature of microstructure, the morphology of the coherent particles is essential for understanding the second-phase strengthening eff ect in various industrial alloys. This letter reports anisotropic growth of coherent ferrite from austenite matrix in pure iron based on molecular dynamics simulation. We found that the ferrite grain tends to grow into an elongated plate-like shape, independent of its initial confi guration. The fi nal shape of the ferrite is closely related to the misfi t between the two phases, with the longest direction and the broad facet of the plate being, respectively, consistent with the best matching direction and the best matching plane calculated via the Burgers vector content(BVC) method. The strain energy calculation in the framework of Eshelby's inclusion theory verifi es that the simulated orientation of the coherent ferrite is energetically favorable. It is anticipated that the BVC method will be applicable in analysis of anisotropic growth and morphology of coherent second phase in other phase transformation systems.     

A STUDY OF TEMPERATURE-DEPENDENT VALENCE BOND STRUCTURE OF TITANIUM

On the basis of energy and shape method for the determination of the valence bond (VB) structures of crystal, the valence bond structure of titanium is redetermined at room temperature and calculated in the whole temperature range of 0-1943K. The outer shell electronic distribution of Ti is e_c~(2.9907) · (s_c~(0.4980) d_c~(2.4927)) ef1.0093 in crystal. The temperature dependences of the VB structures of hcp and bcc phases are the same. The VB structures of hcp and bcc phases monotonically increase or decrease with the increase in temperature, but show discontinuous changes at the phase-transformation temperature 1155K.     

Structural Optimization of Electromagnetic Swirling Flow in Nozzle of Slab Continuous Casting

During the slab continuous casting process, the flow field of molten steel in the mold plays a decisive role in the quality of the slab. In this paper, electromagnetic swirling flow in nozzle technology is proposed to control the flow field in mold.This technology can drive molten steel to rotate inside the submerged entry nozzle by electromagnetic force, thereby controlling the flow field. This research shows that it can reduce the impact of molten steel on the bottom of nozzle and partly reduce the negative pressure at the upper part of nozzle outlet which is even eliminated by optimizing the structure and angle of nozzle. The area of heat flux of the mold wall becomes larger, and the crest value of heat flux gets lower than that without swirling in nozzle and any nozzle optimization. The meniscus fluctuates smoothly, and the flow velocity at the top surface is within a reasonable range. The temperature field distribution in the mold is uniform which was beneficial to the growth of equiaxed crystal and decreased element segregation.