液相介质对水平气液间歇流动的压降影响

研究了水平管内不同液相介质(水、油和不同浓度的CMC溶液)对气液两相间歇流动压降的影响. 实验管道为内径50 mm的透明有机玻璃管,从入口到分离器长约30 m,实验段由2个长3 m的水平管组成. 共记录了320组不同表观流速下的压降信号：油相0.17~1.85 m/s,水相0.17~2.48 m/s,CMC溶液0.17~1.42 m/s,气相0.06~3.40 m/s. 结果表明,液相为牛顿流体(油或水)的气液流动,随着表观气相流速的增大,压降呈增加趋势;非牛顿幂率流体(不同浓度的CMC溶液)的管道流动,当流动指数低于一定值时,压降随气相流量的增加呈降低趋势,并且低于单液相流动的压降. Lockhart-Martinelli模型过高地预测了气-非牛顿幂率流体两相的压降.     

Drop properties and pressure fluctuations in liquid–liquid–solid fluidized-bed reactors

Characteristics of size, rising velocity and distribution of liquid drops were investigated in an immiscible liquid–liquid–solid fluidized-bed reactor whose diameter was 0.102 and 2.5 m in height. In addition, pressure fluctuations were measured and analyzed by adopting the theory of chaos, to discuss the relation between the properties of liquid drops and the resultant flow behavior of three (liquid–liquid–solid) phase in the reactor. Effects of velocities of dispersed (0–0.04 m s⁻¹) and continuous (0.02–0.14 m s⁻¹) liquid phases and fluidized particle size (1, 2.1, 3 or 6 mm) on the liquid drop properties and pressure fluctuations in the reactor were determined. The resultant flow behavior of liquid drops became more irregular and complicated with increasing the velocity of dispersed or continuous liquid phase, but less complicated with increasing fluidized particle size, in the beds of 1.0 or 2.1 mm glass beads. In the beds of 3.0 or 6.0 mm glass beads, the effects of continuous phase velocity was marginal. The resultant flow behavior of liquid drops was dependent strongly upon the drop size and its distribution. The drop size increased with increasing dispersed phase velocity, but decreased with increasing particle size. The drop size tended to increase with approaching to the center or increasing the height from the distributor. The size and rising velocity of liquid drops and correlation dimension of pressure fluctuations have been well correlated in terms of operating variables.     

宁东灵武矿区煤粉密相输送管道压降研究

采用Barth气力输送理论,通过实验在质量流率1 550—1 700 kg/h的输送范围内,研究了宁东灵武矿区煤粉密相输送的压降和表观气速的关系。结果表明:随着表观气速的增加,水平管道和竖直管道的压降都是先降低后升高,但竖直段的压降变化速度比水平段变化快,水平段的经济气速(4 m/s)小于竖直段的经济气速(7 m/s)。通过计算值与实验值比较,发现理论计算值与实验值偏差在30%以内,说明基于Barth附加压降法对宁东灵武矿区煤粉密相气力输送管阻力特性的计算具有较好的适应性。     

工业级水平管粉煤气力输送的最小压降速度和稳定性

采用压缩空气作为输送介质,在工业级水平管(内径50 mm)上开展了粉煤密相气力输送实验研究。在实验获得最小压降速度基础上,通过电容层析成像系统观察到,随着表观气速降低而存在分层流、沙丘流、移动床流以及栓塞流4种流型。不同流型压力信号的概率密度分布和功率谱密度分析表明,压力信号的波动特征与流型紧密联系;由于流动形态的变化,存在由稳定输送过渡到不稳定输送的临界气速,且该速度小于最小压降速度。     

大输量多相混输管路气液两相流实验研究

为了研究大输量条件下多相混输管路的流动特性,以水和空气为实验介质,在长江大学多相流实验平台上进行了水平状态的高气液量两相流模拟实验研究。实验采用内径为60 mm、长9.4 m的透明有机玻璃管,并利用高速摄像仪记录实验过程中的流型。通过对实验流型进行整理,将水平管内的气液两相流流型划分为分层流、泡状流、段塞流和环状流,并与典型的Mandhane流型图进行对比分析。另外,对实验范围内的几种典型流型下的压降梯度变化规律进行了研究,泡状流区域压降梯度随气流速的增大而减小,段塞流区域压降梯度随气流速的增大而缓慢增大,环状流区域压降梯度随气流速的增加而继续增大。     

Hydrodynamics and droplet size distribution of liquid–liquid flow in a packed bed reactor with orifice plates

A packed bed reactor with orifice plates (PBR@OP) was designed by adding orifice plates periodically in packed beds. Hydrodynamics and droplet size distribution in PBR@OP were experimentally investigated using fatty acid methyl esters (FAME)/water as the model liquid–liquid system. In PBR@OP, the flow pattern was close to plug flow. Droplets with Sauter mean diameter (d₃₂) of 150–550 μm were generated. The pressure drop of orifice, flow velocity and plate spacing were key parameters to control the droplet size. The reactor performance was evaluated by analyzing a FAME epoxidation process. At the same d₃₂ and residence time, the length and total pressure drop of PBR@OP were about 1/3 and 1/4 of those of PBR without orifice plates, respectively. Furthermore, a semi-empirical correlation describing the d₃₂ change in PBR@OP was developed, revealing a relative mean deviation of 8.64%. PBR@OP presents a cost-effective option for the intensification of liquid–liquid medium rate reactions.     

油水混合物在水平管中的二相流动特性研究

对内径40mm的钢管和有机玻璃管内油水二相水平流动时的流型、摩擦压降特性进行了详细的实验研究,结果表明:油包水向水包油的转变发生在含水体积分数约0. 4时。随含水体积分数的增大,油水二相流的摩擦压降先是急剧减小,其后在含水体积分数大于0. 4时压降变化趋于平缓。油水二相流的摩擦压降受含水体积分数、管壁润湿特性、管壁粗糙度以及混合物流速的影响,当二相流体处于水包油状态时,钢管内的摩擦压降比有机玻璃管内的大;而当处于油包水时,有机玻璃管内的摩擦压降则比钢管内的摩擦压降大。     

水平管内水环输送模拟稠油减阻特性

基于自主设计加工并搭建的水环输送稠油减阻模拟管路系统,采用500^#白油模拟稠油,试验研究了稠油在水环作用下的水平管流阻力特性,分析了油相表观流速（0.3～1.0m/s）、水相表观流速（0.11～0.72m/s）及入口含水率（0.13～0.49）对水润滑管流流型特征及减阻效果的影响。结果表明：环状水膜可有效隔离并润滑油壁界面,油-水两相流流型总体上呈稳定的偏心环状流结构;水环输送可大幅降低管道输送过程中的压降,其压降值仅为相同油流量下纯油输送压降的1/55～1/27;当入口含水率为0.13～0.27时,水环输送的效能显著,输油效率均高于40;油相表观流速和入口含水率的增加会增大单位管长压降,降低水环输送的减阻效果和输油效能。     

水平渐变管内油水两相流模拟研究

为优化油气集输管道局部管道结构,采用计算流体力学软件对水平渐变管内油水两相流进行数值模拟,对比不同含水率、不同入口流速条件下两相流流型,分析油水两相流在管道内的压力分布规律。结果表明,渐变管内油水两相流流型为水包油流型,管壁主要为油相润湿;渐缩管压力随流向位移持续下降,渐扩管先下降后上升再下降;整体压降速率与含水率成反比,与入口流速成正比。研究结果可以为优化稠油集输管网管道结构、降低管道流动能耗等油水混输问题提供参考。     

Gas–liquid two-phase flow division at a micro-T-junction

The phase distribution of a gas–liquid flow through a 1 mm T junction has been studied. Gas superficial velocities of 2.5 and 4.9 m/s and liquid superficial velocities 0.09–0.42 m/s were investigated. Increasing the liquid superficial velocity was shown to decrease the liquid taken off at the side arm. Increasing the gas superficial velocity was found to affect the phase split by increasing the fractional liquid taken off. It was noticed that pressure has no influence in the phase split when it was increased from 0.13 to 0.18 MPa. From examination of data from different pipe sizes, it was seen that the 1 mm T-junction shared similar split characteristics as those observed for larger diameter junctions. Finally, the gas–liquid flow pattern through the junction was observed to be slug for a range of gas and liquid superficial velocities.     

An experimental study of energy-saving pneumatic conveying system in a horizontal pipeline with dune model

In order to reduce power consumption and conveying velocity, a pneumatic conveying system where a dune model is mounted in a pipeline is proposed in this paper. The experimental study focuses on the effect of the mounted dune model in the horizontal pneumatic conveying system in terms of pressure drop, power consumption and conveying velocity. The test pipeline consisted of a horizontal smooth acrylic tube with an inside diameter of 80 mm and a length of about 5 m. Polyethylene spherical particles with a density of 952 kg/m³ and diameters of 2.3 and 3.3 mm are used as conveying materials. The mean air velocity is varied from 9 to 16 m/s, and the solid mass flow rate is from 0.25 to 0.45 kg/s. Firstly, the effect of the dune model location on pneumatic conveying is experimentally studied. It is found that in the lower air velocity range, the pressure drop of the pneumatic conveying with a mounted dune model is lower than that of a conventional pneumatic conveying system. A lower conveying velocity and energy-saving conveying can be realized by installing a dune model in the conveying pipe. Especially the case of fixing the dune model on the bottom of the pipe at the inlet of particle feed is more effective. The particle flow patterns also show that the dune model reduces the deposition of particles. Then, the effect of different surface materials of the dune model is examined. By using a surface material of the dune model with a large coefficient of restitution, the pressure drop of conveying large particles is the lowest. When conveying relatively small particles, however, the pressure drop becomes the lowest by a small coefficient of restitution. The maximum reduction rates of the minimum velocity and power consumption by the dune model are about 19% and 34%, respectively.     

Experimental studies on phase inversion in a small diameter horizontal pipe

The present work describes phase inversion during kerosene–water flow through a 0.012 m diameter horizontal pipe. The phenomenon has been identified using three techniques namely the optical probe technique, pressure drop measurements and an isokinetic sampling technique. Since repeated experiments have reveled dispersed flow to occur at high mixture velocities (>1 m/s), the studies have been conducted for mixer velocity ranging from 1 m/s to 2.5 m/s. The observations have shown that the transition from oil-in-water to water-in-oil dispersion occurs via an emulsified homogenous mixture at high mixture velocities while several different flow patterns mark the transition at lower flow rates of the two phases.     

The effect of gas injection on the flow of immiscible liquids in horizontal pipes

The flow of two immiscible liquids and the influence of an additional inserted gas phase in horizontal pipes is investigated. The experiments are carried out in a transparent horizontal pipe with an inner diameter of 59 mm and a total length of 48 m. Experimental results are presented for the flow regimes of the two phase and three phase flow of oil, water and gas mixtures. The effect of phase inversion on the pressure drop is measured. The experimental results obtained for the three phase flow of oil, water and air indicate that drag reduction is possible by injecting gas in laminar flowing mixtures of oil and water. In the aerated slug flow regime of oil, water and air a water dominated and an oil dominated flow system can be distinguished. The pressure drop of the three phase flow system is of the magnitude as the pressure drop of the two phase flow of gas and the dominating liquid phase.     

CFD modeling and validation for two-phase medium viscosity oil-air flow in horizontal pipes

This study presents the results of a Computational Fluid Dynamics (CFD) simulation of two-phase medium viscosity oil-air flow in a 50.8?mm internal diameter horizontal pipe. Void fraction and pressure gradient predictions were validated using experimental data for four different oil viscosities (0.039, 0.06, 0.108 and 0.166?Pa s) and different flow rates varying from 0.1 to 2.9?m/s for the gas phase and from 0.01 to 2.95?m/s for the liquid phase, where four flow patterns were predicted (stratified, dispersed bubble, bubble elongated and slug flow). The obtained results of void fraction and pressure gradient presented a mean relative error of 30.04 and 21.38%, respectively. Furthermore, the CFD results were compared against 66 empirical correlations and predictions from OLGA. It was found that between the three studied methods (CFD, OLGA and empirical correlations) the CFD model outperformed the other two methods regarding the predicted flow patterns, pressure gradients and void fractions on most cases.     

水包油型乳化液油滴的管内节流破碎行为与机理

实验研究了水包油型乳化液油滴在管内节流元件处的破碎行为,分析了破碎机理. 结果表明,液滴破碎主要发生在节流元件内壁及下游附近,其概率是施于液滴上湍流应力与液滴表面能之比的递增函数,是流体韦伯数及节流元件两侧最大压差的递增函数;在湍流状态(Re>4000)下,液滴充分振荡且受到较大的水流惯性力和速度梯度剪切力,更易破碎;由苏丹红IV染色的正庚烷体系界面张力由非染色时的47 mN/m降到23.6 mN/m,黏性力对液滴破碎的影响程度下降,受流速、压差等影响的惯性力起决定性作用,液滴破碎程度更大;流速决定流体对分散相油滴的湍流剪切破碎力,流速增大则油滴粒径破裂程度加大,而流速取决于流量和节流比;注入染色正庚烷油相体积增大(0.5~5 mL),削弱了节流元件的液滴破碎作用,两相流体系倾向于形成更大直径的液滴,中位径一般为20~35 mm.     

Pressure Drop in Liquid‐liquid Two Phase Horizontal Flow: Experiment and Prediction

The present study is aimed at an investigation of the pressure drop characteristics during the simultaneous flow of a kerosene‐water mixture through a horizontal pipe of 0.025 m diameter. Measurements of pressure gradient were made for different combinations of phase superficial velocities ranging from 0.03–2 m/s such that the regimes encountered were smooth stratified, wavy stratified, three layer flow, plug flow and oil dispersed in water, and water flow patterns. A model was developed, which considered the energy minimization and pressure equalization of both phases.     

气液螺旋环状流压降特性研究

考虑旋流衰减的影响，对气液螺旋环状流的压降特性进行研究并推导出了螺旋环状流压降预测模型。定义压降旋-直比系数为气液两相螺旋环状流和气液两相直流的压降之比，以此来表征旋流衰减对压降的影响。基于量纲分析的方法对压降旋-直比系数进行分析，推导出其表达式，压降旋-直比系数依赖于Lockhart-Martinelli 参数和气相Froude数变化。最终，得出了气液两相螺旋环状流的压降预测模型。在50 mm内径的水平管内对螺旋环状流的压降特性进行了实验研究，其中气相表观流速变化范围为10~16 m/s，体积含液率（LVF）变化范围为0.6%~4.8%。通过与实验数据进行对比，压降预测模型的相对误差在±15%以内，为工程应用提供了参考。     

Study on pressure drop characteristics of gas-liquid swirl annular flow

Considering the influence of swirl attenuation, the pressure drop characteristics of gas-liquid spiral annular flow are studied, and the pressure drop prediction model of spiral annular flow is deduced. The swirl-straight ratio of pressure drop is defined as the ratio of pressure drop of swirl flow to straight flow, used to characterize the effect of swirl decay on pressure drop. The expression of swirl-straight ratio of pressure drop is derived by the method of dimensional analysis, and it has a strongly dependence on Lockhart-Martinelli coefficient and gas phase Froude number. Finally, the prediction model of pressure drop for gas-liquid swirl annular flow is obtained. The pressure drop characteristics of the swirl annular flow are experimentally studied in a horizontal tube with an inner diameter of 50 mm. The range of the gas superficial velocity is 10—16 m/s and the range of the liquid volume fraction (LVF) is 0.6%—4.8%. Through comparison with experimental data, the relative error of the pressure drop prediction model is within ±15%, which provides a method reference for engineering applications.     

圆形微通道反应器内2-乙基四氢蒽氢醌氧化反应

以管径为900 μm的圆形微通道反应器内2-乙基四氢蒽氢醌(THEAQH2)的氧化反应为研究对象,研究了反应过程中气液两相的流动形态,考察了反应温度、反应压力、液体流速ULS、气液比rAS等因素对THEAQH2氧化反应的影响.研究表明,圆形微通道反应器内进行THEAQH2的氧化反应时可得到较高的气液两相接触比表面积;氧化反应随温度升高、压力增大和液体流速ULS的增加而显著加快;THEAQH2的氧化反应在圆形微通道反应器内进行可得到较高的过氧化氢时空收率YSTY (Space-Time Yield),在温度50℃、压力0.29 MPa、液体流速0.052 m/s时,YSTY可达1 790 kg/(m3·h),高出常规反应器1～2个数量级.     

An Analysis of Pressure Drop and Holdup for Liquid‐Liquid Upflow through Vertical Pipes

The present study has attempted to investigate pressure drop and holdup during simultaneous flow of two liquids through a vertical pipe. The liquids selected were kerosene and water. The measurements were made for phase velocities varying from 0.05–1.2 m/s for both liquids. The pressure drop was measured with a differential pressure transducer while the quick closing valve (QCV) technique was adopted for the measurement of liquid holdup. The measured holdup and pressure drop were analyzed with suitable theoretical models according to the existing flow patterns. The analysis reveals that the homogeneous model is suitable for dispersed bubbly flow whereas bubbly and churn‐turbulent flow pattern is better predicted by the drift flux model. On the other hand, the two fluid flow model accurately predicts the pressure drop in core annular flow.