| 双环戊二烯马来酸单酯的合成与表征 |
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| 引用本文： | 俎喜红,胡剑青,涂伟萍.双环戊二烯马来酸单酯的合成与表征[J].化学试剂,2007,29(11):667-669. |
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| 作者姓名： | 俎喜红 胡剑青 涂伟萍 |
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| 作者单位： | 华南理工大学,化工与能源学院,广东,广州,510640 |
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| 摘 要： | 通过顺丁烯二酸酐水解并与双环戊二烯发生酸催化加成反应,合成了标题化合物(DHCM),收率达90%,产品中w(DHCM)>85%。通过元素分析、红外光谱和GC-MS等对其结构进行了表征。
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| 关 键 词： | 双环戊二烯马来酸单酯 合成 双环戊二烯 顺丁烯二酸酐 |
| 文章编号： | 0258-3283（2007）11-0667-03 |
| 修稿时间： | 2007-05-24 |
Synthesis and characterization of dicyclopentadiene monomaleate |
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| ZU Xi-hong,HU Jian-qing,TU Wei-ping.Synthesis and characterization of dicyclopentadiene monomaleate[J].Chemical Reagents,2007,29(11):667-669. |
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| Authors: | ZU Xi-hong HU Jian-qing TU Wei-ping |
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| Affiliation: | Institute of Chemical and Energy Engineering,South China University of Technology,Guangzhou 510640,China |
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| Abstract: | Dicyclopentadiene monomaleate(DHCM),a new functional monomer,was prepared by hydrolysis of maleic anhydride(MA) followed by acid-catalyzed addition reaction with dicyclopentadiene(DCPD),and the yield of DHCM was up to 90% with its purity exceeding 85%.The molecular structure of product was characterized by EA,FT-IR spectroscopy and GC-MS,and the synthetic technology and performance of DHCM were also studied. |
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| Keywords: | dicyclopentadiene monomaleate synthesis dicyclopentadiene maleic anhydride |
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