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目的 分离鉴定青叶胆 Swertia mileensis全草的酮类成分。方法 95 %乙醇浸提 ,经硅胶柱色谱分离纯化 ,UV,IR,MS,1 H和 1 3CNMR波谱方法确定化学结构。结果 分得 12个酮成分 ,分别为 1-羟基 - 2 ,3,4 ,5 -四甲氧基酮 (1- hydroxy- 2 ,3,4 ,5 - tetramethoxyxanthone, ) ;1-羟基 - 2 ,3,7-三甲氧基酮 (1- hydroxy- 2 ,3,7-trim ethoxyxanthone, ) ;1-羟基 - 2 ,3,5 ,7-四甲氧基酮 (1- hydroxy- 2 ,3,5 ,7- tetram ethoxyxanthone, ) ;1,5 -二羟基 - 2 ,3-二甲氧基酮 (1,5 - dihydroxy- 2 ,3- dimethoxyxanthone, ) ;1,5 -二羟基 - 2 ,3,7-三甲氧基酮 (1,5 - dihy-droxy- 2 ,3,7- trimethoxyxanthone, ) ;1-羟基 - 2 ,3,5 -三甲氧基酮 (1- hydroxy- 2 ,3,5 - trimethoxyxanthone, ) ;1,5 -二羟基 - 2 ,3,4 ,7-四甲氧基酮 (1,5 - dihydroxy- 2 ,3,4 ,7- tetramethoxyxanthone, ) ;1,8-二羟基 - 2 ,3,6 -三甲氧基酮 (1,8- dihydroxy- 2 ,3,6 - trimethoxyxanthone, ) ;1-羟基 - 2 ,3,4 ,7-四甲氧基酮 (1- hydroxy- 2 ,3,4 ,7- te-tramethoxyxanthone, ) ;1,2 ,3,5 -四甲氧基酮 (1,2 ,3,5 - tetromethoxyxanthone, ) ;1-羟基 - 2 ,3,4 ,6 -四甲氧基酮 (1- hydroxyl- 2 ,3,4 ,6 相似文献
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J.Wai-Kuo Shih Geoŗge Hess Paul M. Kaplan John L. Gerin 《Journal of virological methods》1980,1(1):47-59
Hepatitis B virions (Dane particles) were purified from the sera of chronic HBsAg carriers by consecutive rate-zonal and isopycnic centrifugations in sucrose gradients using HBsAg, HBcAg and endogenous DNA polymerase activities as specific markers. Purified Dane particles, radiolabelled with Na 125I by the chloramine-T procedure, had a higher buoyant density in CsCl (1.28 g/cm3) than unlabelled particles (1.26 g/cm3) and an estimated sedimentation coefficient of 280 s. 125I-Dane particles were fully precipitated by anti-HBs and not by anti-HBc sera. Heavy and light density core particles were purified from heavy and light density populations of Dane particles and radioiodinated. The iodinated polypeptides of Dane particles and HBcAg were compared with those of the iodinated 22-nm form of HBsAg by SDS-PAGE. Iodinated Dane particles contained seven polypeptides with molecular weights of 18,000, 23,000, 26,000, 34,000, 43,000, 48,000 and 115,000. Heavy and light core particles contained three polypeptides with molecular weights of 18,000, 25,000 and 37,000. 相似文献
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青叶胆酮类化合物的成分研究 总被引:1,自引:1,他引:1
目的 分离鉴定青叶胆 Swertia mileensis全草的酮类成分。方法 95 %乙醇浸提 ,经硅胶柱色谱分离纯化 ,UV,IR,MS,1 H和 1 3CNMR波谱方法确定化学结构。结果 分得 12个酮成分 ,分别为 1-羟基 - 2 ,3,4 ,5 -四甲氧基酮 (1- hydroxy- 2 ,3,4 ,5 - tetramethoxyxanthone, ) ;1-羟基 - 2 ,3,7-三甲氧基酮 (1- hydroxy- 2 ,3,7-trim ethoxyxanthone, ) ;1-羟基 - 2 ,3,5 ,7-四甲氧基酮 (1- hydroxy- 2 ,3,5 ,7- tetram ethoxyxanthone, ) ;1,5 -二羟基 - 2 ,3-二甲氧基酮 (1,5 - dihydroxy- 2 ,3- dimethoxyxanthone, ) ;1,5 -二羟基 - 2 ,3,7-三甲氧基酮 (1,5 - dihy-droxy- 2 ,3,7- trimethoxyxanthone, ) ;1-羟基 - 2 ,3,5 -三甲氧基酮 (1- hydroxy- 2 ,3,5 - trimethoxyxanthone, ) ;1,5 -二羟基 - 2 ,3,4 ,7-四甲氧基酮 (1,5 - dihydroxy- 2 ,3,4 ,7- tetramethoxyxanthone, ) ;1,8-二羟基 - 2 ,3,6 -三甲氧基酮 (1,8- dihydroxy- 2 ,3,6 - trimethoxyxanthone, ) ;1-羟基 - 2 ,3,4 ,7-四甲氧基酮 (1- hydroxy- 2 ,3,4 ,7- te-tramethoxyxanthone, ) ;1,2 ,3,5 -四甲氧基酮 (1,2 ,3,5 - tetromethoxyxanthone, ) ;1-羟基 - 2 ,3,4 ,6 -四甲氧基酮 (1- hydroxyl- 2 ,3,4 ,6 相似文献
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细梗紫菊中的化学成分 总被引:3,自引:0,他引:3
目的 对细梗紫菊Notoseris gracilipes全草的化学成分进行分离纯化、结构鉴定和抗菌活性测试。方法 以甲醇室温提取,采用各种色谱技术进行分离纯化。根据NMR等波谱数据鉴定结构。按常规方法进行抗菌活性的定性测定。结果 从细梗紫菊全草的甲醇提取物中分离鉴定出12个化合物,其中8个为倍半萜内酯:jacquilenin(Ⅰ),scorzoside(Ⅱ),ixerisosideD(Ⅲ),austricin(Ⅳ),notoserolideA(Ⅴ),crepidiasideB(Ⅶ)和lactusideB(Ⅷ)。另外4个化合物分别鉴定为6,7-二羟基香豆素(Ⅸ),野莴苣苷(Ⅹ),木犀草素-7-葡萄糖苷(Ⅺ)和胡萝卜苷(Ⅻ)。倍半萜内酯的抗菌实验表明化合物Ⅰ和Ⅱ对蜡状芽孢杆菌(Bacillu cereus AS.1.1688)的生长有抑制作用。结论 这些化合物均为首次从该植物中分离得到。 相似文献
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Ying-Chen Kuo Lin-Fen Hsieh 《Journal of manipulative and physiological therapeutics》2019,42(6):407-415
ObjectiveThe purpose of this study was to compare the diagnostic accuracy of lesion localization between Cyriax’s functional examination and ultrasonography in participants with and without shoulder pain.MethodsA total of 206 adults aged 20 years and older with or without shoulder pain were included. All participants received Cyriax’s functional examination by the first blinded physiatrist. Within a week, ultrasonography was performed by another blinded specialist. The diagnoses made by both methods, respectively, were compared finally. Sensitivity, specificity, and positive and negative predictive values were evaluated for the diagnosis of shoulder lesions between Cyriax’s functional examination and ultrasonography.ResultsThere was no significant difference between the 2 groups regarding age, sex, and body mass index. Moderate to high sensitivity (74.1%, 76.5%, and 66.7%) and high specificity (93.0%, 99.5%, and 99.0%) were in supraspinatus, subscapularis, and infraspinatus lesions, respectively. For the subacromial-subdeltoid bursitis, high sensitivity (90.4%) and moderate to high specificity (70.3%) was found. In contrast, low sensitivity (15.0%) and high specificity (100.0%) were found in the biceps lesions.ConclusionIn this study, we found that Cyriax’s functional examination had high sensitivity in detecting subacromial-subdeltoid bursitis and high specificity in rotator cuff lesion. 相似文献
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