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Structural Evolution of UHMWPE Fibers during Prestretching Far and Near Melting Temperature: An In Situ Synchrotron Radiation Small‐ and Wide‐Angle X‐Ray Scattering Study 下载免费PDF全文
Combining a homemade extension apparatus and the in situ synchrotron radiation small‐ and wide‐angle X‐ray scattering methods for measurement, the structural evolutions of gel‐spun ultrahigh molecular weight polyethylene (UHMWPE) fibers during prestretching at temperatures of 25 and 100 °C are investigated, respectively. Lamellar rotation toward the stretching direction occurs before strain hardening, while the folded‐chain crystal destruction and extended‐chain fibril formation processes occur in the strain hardening zone at 25 °C. While at 100 °C, stretching induced crystal melting before the stress plateau region and formation of fibrous crystals at the onset of the stress plateau are observed. Further stretching results in shear displacement of crystal blocks and, finally, destruction of the folded‐chain crystals and formation of extended‐chain fibrils. Prestretching UHMWPE fibers at 100 °C within a certain strain range can produce highly oriented fibrous crystals, which may provide an ideal precursor structure for the poststretching process. 相似文献
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为了提高光纤光栅测量应变的测量范围与测量精度,该文对基片式光纤光栅传感器应变传递理论及其有限元分析应力分布进行了阐述,并对光纤光栅应变传感器的制作工艺进行了探索。封装工艺与普通基片式光纤光栅传感器的不同是在制作时加载确定的预紧力,用等强度梁对预应力基片式光纤光栅传感器进行测试并标定,得到传感器灵敏度为0.88pm/με,线性度为0.996,传递效率为74%。并在MTS拉伸试验机上进行预紧力基片式光纤光栅传感器、裸光纤光栅传感器与电阻应变计压缩对比实验研究,实验表明,预拉伸制作工艺提高了光纤光栅测量压缩应变的线性度与测量范围。 相似文献
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P. H. Wang 《应用聚合物科学杂志》1998,67(7):1185-1190
Polyacrylonitrile (PAN) fibers of a special grade have been modified by a method of prestretching with various stretching ratios from negative to positive before the onset of stabilization. The effect of such pretreatments on the thermorhelogical and thermal behaviors of PAN fibers was followed by free shrinkage experiments and differential scanning calorimetry (DSC) analyses. It was found that prestretching had a significant influence on the physical shrinkage of PAN fibers. DSC results of PAN fibers showed dependence not only on atmospheric conditions but also on the extent of prestretching. © 1998 John Wiley & Sons, Inc. J Appl Polym Sci 67:1185–1190, 1998 相似文献
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阐述了5MN铝板预拉伸机测控系统的总体设计方案,硬件的组成、软件设计方法;通过预拉伸方法,有效的消除7050超厚铝合金因淬火引起的残余应力。 相似文献
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通过金相、扫描电镜、拉伸和断裂韧性试验等分析测试手段,研究了固溶处理温度及预拉伸变形量对2197铝锂合金板材组织和性能的影响。结果表明,2197铝锂合金在490~580℃温度范围内固溶再时效后,其强度随固溶处理温度的升高先增大后减小,强度峰值出现在540℃。当固溶处理温度高于565℃时,合金出现了再结晶现象。但是,合金在490~580℃固溶处理过程中均未出现明显的过烧现象。固溶处理后进行预拉伸变形可以有效提高合金的强度。综合考虑合金的强韧匹配,2197合金板材较优的固溶和预拉伸变形量分别为540℃×1.5 h和2%~5%。 相似文献
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