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排序方式: 共有162条查询结果,搜索用时 468 毫秒
1.
Michael Bratychak Mihailo Bratychak Witold Brostow Olena Shyshchak 《Materials Research Innovations》2002,6(1):24-30
Oligomers containing peroxy groups have been synthesized on the basis of epoxides reacting with tert–butylhydroperoxide in the presence of boron trifluoride etherate. Dependence of reaction rates upon the quantity of catalyst,
temperature and also nature of hydroperoxide has been investigated: A kinetic equation for the process has been formulated
and also a kinetic scheme for the reaction taking into account the presence of boron trifluoride etherate is proposed. Structures
of the synthesized peroxy oligomers have been confirmed by IR- and NMR-spectroscopy. The reaction initiating properties of
the oligomers so synthesized were studied using as the example the styrene polymerization reaction.
Electronic Publication 相似文献
2.
This paper presents the results of investigation of condensation stimulated (CSD) and thermal stimulated (TSD) diffusion in nanoscale film systems on the basis of Fe/Cr and Cu/Cr by Auger-electron spectroscopy method. The film systems were built in ultrahigh vacuum. Auger spectrum was traced during condensation after each increase in thickness of 0.5-1 nm or during film systems annealing from 300 to 683 K over 5 h. According to experimental data the concentration profiles were built and the effective coefficients of CSD and TSD were computed by several mathematical methods. The efficiency of these techniques in different cases was analyzed. The most accurate results were obtained with Weeple and Gauss error methods that take into account the thickness of the diffusant source. 相似文献
3.
Beladenta Amalia Marcela Fu Olena Tigova Montse Ballbè Yolanda Castellano Sean Semple Luke Clancy Constantine Vardavas Maria J. López Nuria Cortés Raúl Pérez-Ortuño José A. Pascual Esteve Fernández 《Indoor air》2021,31(5):1601-1613
Secondhand electronic cigarette (e-cigarette) aerosol (SHA) might impair indoor air quality and expose bystanders. This study aims to investigate exposure to SHA in controlled conditions of enclosed settings simulating real-world scenario. An experiment was performed in a car and in a room, in which SHA was generated during a 30-minute ad libitum use of an e-cigarette. The experiment was replicated on five consecutive days in each setting. We measured PM2.5, airborne nicotine concentrations, and biomarkers of exposure to SHA, such as nicotine metabolites, tobacco-specific nitrosamines, propylene glycol, and glycerol in bystanders’ saliva samples before, during, and after the exposure period. Self-reported health symptoms related to exposure to SHA were also recorded. The results showed that the highest median PM2.5 concentration was recorded during the exposure period, being 21 µg/m3 in the room setting and 16 µg/m3 in the car setting—about twofold increase compared to the baseline. Most concentrations of the airborne nicotine and all biomarkers were below the limit of quantification in both settings. Bystanders in both settings experienced some short-term irritation symptoms, expressed as dry throat, nose, eyes, and phlegm. In conclusion, short-term use of an e-cigarette in confined spaces increased indoor PM2.5 level and caused some irritation symptoms in bystanders. 相似文献
4.
L. A. Timofeeva S. S. Timofeev A. Y. Dyomin I. I. Fedchenko D. G. Voskoboynikov 《Journal of Friction and Wear》2018,39(3):227-231
The article has described a promising oxyalloying technique for the surface modification of machine parts made of iron–carbon alloys that operate under conditions of friction and wear. The new method has been implemented via the surface impregnation of steel and cast-iron parts with superheated steam of aqueous solutions of salts containing chemically active alloying elements. A multilayer coating formed on the surfaces of parts as a result of this treatment increases their performance characteristics, which has been confirmed by the integrated research. 相似文献
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Ajay Kumar Shukla Ryabov Dmitry Olena Volkova Piotr R. Scheller Brahma Deo 《Metallurgical and Materials Transactions B》2011,42(1):224-235
The melting of steel scrap in high temperature liquid iron melt is investigated by conducting cold model experiments of the
melting of ice sample of different geometries and sizes in an argon-stirred vessel containing water. The melting process of
ice samples is observed using a high-speed camera. Design of experiments is based on similarity criteria. The relationships
between non-dimensional groups related to heat transfer (Nu, Re, Pr, and Gr) are derived for different experimental conditions.
The results are compared with those reported in the literature. The heat transfer coefficient is estimated as a function of
mixing power and is found to be in good agreement with the calculated values obtained by using reported relationships in literature. 相似文献
8.
Thomas Fend Wilhelm Völker Rolf Miebach Olena Smirnova Daniel Gonsior Daniel Schöllgen Peter Rietbrock 《International Journal of Heat and Mass Transfer》2011,54(19-20):4175-4181
The results of experimental investigations of novel ceramic high-temperature heat exchangers (HTHE) and its main characteristics such as effectiveness and power load as a function of mass flow and the geometry of the channels are presented. Firstly, some information on the background and the manufacturing of the HTHE, which is based on honey comb structures made out of extruded silicon carbide, is given. The experimental tests have been carried out with air as a heat transfer medium at temperatures of up to 1000 °C. The experimental set-up is described in detail. The acquired characteristic temperature and effectiveness data for different inlet temperatures and mass flows are discussed. They have been compared with data from theoretical calculations as well as with characteristic data of typical counter flow heat exchangers. Additionally, thermal shock tests have been carried out for a qualitative testing of the mechanical strength. Finally, a conclusion and an outlook on further activities are given. 相似文献
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