莱芜黑猪肉中烟酸含量的测定

采用高效液相色谱法测定莱芜黑猪肉中烟酸的含量,并对提取方法及色谱条件等方面进行了改进,以Kromasil C_(18)柱为分离柱,甲醇–0.05mol/L磷酸二氢钾缓冲液(体积比5∶95)为流动相,柱温30℃,紫外检测器在波长261nm条件下检测,可以在4min左右完成分析。烟酸在1.0～25.0mg/L范围内有良好的线性关系(R=0.9998),相对标准偏差为0.62%(n=6),平均加标回收率为98.4%,检出限为2.0×10~(-4)g/kg,为准确测定莱芜黑猪肉中的烟酸含量提供了一种简便快捷的检测方法。     

小像元红外探测器读出电路设计研究

介绍了基于SMIC 0.18 μm 3.3 V工艺设计研究的第一款小像元红外探测器读出电路,间距10 μm,规模1024×1024。文章详细介绍了像素输入级以及列级、输出级运放的设计,为提高线性摆伏,设计选用了低阈值NMOS管nmvt 33,仿真分析证明低阈值管nmvt 33的噪声性能优于普通管n 33；版图设计对关键信号线和敏感点采取隔离处理措施,对像元间串扰进行了仿真分析,有效控制了信号串扰。电路经测试使用各项功能正常,最大电荷处理能力达到4.3 Me-,动态范围≥65 dB,读出速率达到10 MHz,性能指标满足设计要求。     

塔北地区储层敏感性综合预测

综合分析地质、地震及测井资料，可以准确地预测储层的敏感性。以地质分析及敏感性实验资料为基础，以测井资料为标定手段，以地震信息为横向预测导向，综合处理各种信息，从而实现对区域储层的敏感性预测。其中，利用测井资料预测储层敏感性是关键，须采用多参数相关系数法进行单井储层敏感性分析。以塔北地区侏罗系为例，综合各类信息进行了储层敏感性处理，分析结果表明，该区储层速敏弱，水敏、盐敏、碱敏和酸敏程度中等，与其储层敏感性实验结果基本吻合。     

文脉中的环节建筑

环节建筑产生于建筑与城市的内在联系之中，它将“文脉”的含义拓展到基地、城市公共空间体系和城市职能等领域。阐述了环节建筑的基本概念，在此基础上分析了环节建筑在上述三个领域中所扮演的角色及其相互关系。     

珠窝大坝金属结构实全检测与评估

介绍闸门和启闭机安全检测项目与方法,并根据珠窝大坝金属结构安全检测与计算的主要成果,对其设备安全状况进行评估,提出评估结论及建议.检测与评估成果可作为该工程维修加固或更新改造的设计依据,检测与评估方法亦可供其它工程参考借鉴.     

Effects of modeling means on properties of monitoring models of spot welding quality

Analyzing and modeling the relation between monitoring information during welding and quality information of the joints is the foundation of monitoring resistance spot welding quality. According to the means of modeling, the known models can be divided into three large categories: single linear regression models, multiple linear regression models and multiple non-linear models. By modeling the relations between dynamic resistance information and welding quality parameters with different means, this paper analyzes effects of modeling means on performances of monitoring models of resistance spot welding quality. From the test results, the following conclusions can be drawn: By comparison with two other kinds of models, artificial neural network (ANN) model can describe non-linear and high coupling relationship between monitoring information and quality information more reasonably, improve performance of monitoring model remarkably, and make the estimated values of welding quality parameters more accurate and reliable.     

Effects of modeling means on properties of monitoring models o spot welding quality

Analyzing and modeling the relation between monitoring information during welding and quality information of the joints is the foundation of monitoring resistance spot welding quality.According to the means of modeling,the known models can be divided into three large categories:single linear regression models,multiple linear regression models and multiple nonlinear models.By modeling the relations between dynamic resistance information and welding quality parameters with different means,this paper analyzes effects of modeling means on performances of monitoring models of resistance spot welding quality. From the test results,the following conclustons can be drawn:By comparison with two other kinds of models,artificial neural network(ANN) model can describe non-linear and high coupling relationship between monitoring information and quality information more reasonably,improve performance of monitoring model remarkably,and make the estimated values of welding quality parameters more accurate and reliable.     

Spin Dependent Hopping in Ti Doped La0.67 Ca0.33 MnO3

A systematic investigation of the magnetic and transport properties of Ti doped La0.67Ca0.33MnO3 was reported. The Ti substitution for Mn ions results in a reduction in ferromagnetism and conductivity. The metal-insulator transition temperature is close to Curie temperature which decreases from 274 to 82 K as x increases from 0 to 0.17. The most important effect of Ti doping is to introduce spin clusters in the samples due to the distortion of local lattice and the inhomogeneous magnetic structure induced primarily by the random distribution of Mn ions. A maximum magnetoresistance ratio as large as 90% in 1 T at 122 K was obtained for the sample with x =0. 055, which is four times larger than that obtained for LCMO sample at 272 K. There is a remarkable field-history dependent MR in the cooling process for the doped samples while such phenomenon disappears in the warming run. The resistivity follows well the variable range hopping behavior in paramagnetic state. Both the size effect and spin dependent hopping of carriers between the spin clusters should be considered in this system.     

钢筋混凝土受弯构件全约束优化设计

本文根据结构优化问题的特点，运用Ｋｕｈｕ－Ｔｕｃｋｅｒ最佳性条件，给出了满足现行ＧＢＪ１０－８９《混凝土结构设计规范》规定的钢筋混凝土受弯构件全约束优化设计方法。