Behavior of untreated and crosslinked cotton fibers. I. Contribution of maturity

The physical and structural properties of American Upland cottons of different maturities have been examined carefully in order to identify fiber parameters which make significant contributions to easy-care properties. The cottons studied possess widely different degrees of overall orientation as determined from birefringence measurements and also exhibit slightly different crease recovery angles. These cottons also respond differently to swelling in sodium hydroxide solution of different concentrations. The physical and mechanical properties of these cottons modified by formaldehyde crosslinking are also compared. The increase in crease recovery angles and the concomitant tensile losses vary from cotton to cotton but are not dependent on maturity or fineness. The stiffness of crosslinked fibers decreases rather than increases with increasing bound formaldehyde. A comparison of the changes in the mechanical properties of formaldehyde-crosslinked cottons differing widely in orientation suggests that cottons with very high orientation are not suitable for chemical modification to impart durable press properties.     

The effects of xanthan and guar gums on staling of gluten-free rice cakes baked in different ovens

The objective of this study was to determine the effects of different concentrations of xanthan and guar gums and their blends on staling of gluten-free rice cakes baked in microwave-infrared combination oven (MW–IR) and to compare the cakes with conventionally baked ones. Gums were added at concentrations of 0.3% and 1.0%. For preparation of gum blend, 0.5% xanthan gum was mixed with 0.5% guar gum. In order to understand the staling behaviour of cakes, cakes were stored at 22 ± 2 °C for 120 h. Xanthan-guar gum blend decreased hardness, weight loss, retrogradation enthalpy and the change in setback viscosity values of cakes during storage for both types of ovens as compared to control formulation. It was found that oven type was a significant factor in affecting staling parameters of gluten-free cakes.     

Analysis and Implementation of a Time-Interleaved ADC Array for a Software-Defined UWB Receiver

A software-defined radio (SDR) for ultrawideband (UWB) communication systems places several stringent requirements on the analog-to-digital converter (ADC). One alternative to using a single ADC is to sample the received signal with an array of lower speed ADCs that were driven by interleaved sampling clocks; however, mismatches among the ADCs will result in signal distortion. This paper makes three important contributions to overcoming this problem: 1) analytical quantification of the impact of ADC gain, offset, and timing mismatches on the performance of a time-interleaved sampling ADC array for UWB signals; 2) demonstration of the efficacy of using a pilot-based matched-filter architecture to mitigate the impact of timing mismatches in the presence of multipath; and 3) implementation of an 8-ADC time-interleaved UWB SDR testbed that operates at an effective sampling frequency of 6.4 GHz. In addition, our findings allow for the design specification of the number of pilots required to obtain a desired system performance. The simulation and measured performance results from this paper demonstrate that ADC mismatches can be controlled to within plusmn10%, yielding acceptable levels of distortion and bit-error-rate (BER) performance on the UWB SDR testbed. Both analytical and simulation results also demonstrate the efficacy of a pilot-based matched filter in mitigating the impact of timing mismatch errors, even in the presence of multipath.     

Conversion of Extracted Oil Cake Fibers into Bioethanol Including DDGS,Canola, Sunflower,Sesame, Soy,and Peanut for Integrated Biodiesel Processing

We have come up with a novel, integrated approach for making biodiesel by in-house producion of ethanol after fermentation of hexane extracted edible oil cake fiber. In addition, we have demonstrated how ethanol could be manufactured from commonly available oil cakes (such as canola, sunflower, sesame, soy, peanut) and dried distiller’s grains with solubles (DDGS). The edible oil cakes and DDGS were hexane extracted, ammonia fiber expansion pretreated, enzymatically hydrolysed and fermented to produce ethanol. From all the oil cakes tested in this work, DDGS and peanut oil cake showed the most promising results giving more than 180 g of glucose/kg of oil cake. These two feedstock’s were hydrolyzed at 15% solids loading and fermented by a native strain of Pichia stipitis. Most sugars were consumed during the first 24 h, with no pronounced inhibition of P. stipitis by the degradation products in the hydrolysate. Xylose consumption was more effective for peanut cake hydrolyzate compared to DDGS.     

Fire behaviour of hollow structural section steel columns filled with high strength concrete

The use of hollow structural section (HSS) steel columns filled with high strength concrete (HSC) is becoming popular due to many advantages they offer. However, whereas the design rules for HSS columns filled with normal strength concrete are well established, there are many uncertainties for HSS columns filled with HSC. Results from numerical studies on the behaviour of HSS columns filled with HSC are presented. The studies were carried out based on both North American and European material properties for HSC and steel. Results show that required fire resistance in HSS columns can be obtained through the use of bar- or steel fibre-reinforcement in HSC.     

Development of epoxy-cyanate ester-clay nanocomposites offering enhanced thermally stability

The preparation and characterization of blends of a series of dicyanate monomers such as 2,2′-bis(4-cyanatophenyl) propane (DCDPP), bis-4-cyanato-biphenyl (DCBP), bis-4-cyanatonaphthalene (DCN), 3,3′-bis(4-cyanatophenyl)sulphide (DCTDP), 3,3′-bis(4-cyanatophenyl)sulphone (DCDPS), and the diglycidyl ether of bisphenol A are reported. These copolymers are combined with a montmorillionite nanoclay and both epoxy-cyanate blends and epoxy-cyanate blends-nanoclay composites are all analyzed for thermal stability, thermal degradation kinetics, flame retardancy, and impact strength. The nanocomposites are further characterized by X-ray diffraction and SEM to determine morphological features, from which structure–property relationships are determined. Dispersion of the nanoclay is of paramount importance, but its inclusion serves to improve char yield and impact strength, when this is achieved. © 2019 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2019 , 136, 47754.     

Experimental evaluation of machinability performance of CNT coated HSS tool during turning of titanium alloy

Journal of Mechanical Science and Technology - The present research deals with the deposition of carbon nanotubes (CNT) over the HSS tool, and to evaluate the machining performance of the coated...     

Development of docetaxel nanocapsules for improving in vitro cytotoxicity and cellular uptake in MCF-7 cells

The aim of this study was to fabricate docetaxel loaded nanocapsules (DTX-NCs) with a high payload using Layer-by-Layer (LbL) technique by successive coating with alternate layers of oppositely charged polyelectrolytes. Developed nanocapsules (NCs) were characterized in terms of morphology, particle size distribution, zeta potential (ζ-potential), entrapment efficiency and in vitro release. The morphological characteristics of the NCs were assessed using transmission electron microscopy (TEM) that revealed coating of polyelectrolytes around the surface of particles. The developed NCs successfully attained a submicron particle size while the ζ-potential of optimized NCs alternated between (+) 34.64?±?1.5 mV to (?) 33.25?±?2.1 mV with each coating step. The non-hemolytic potential of the NCs indicated the suitability of the developed formulation for intravenous administration. A comparative study indicated that the cytotoxicity of positively charged NCs (F4) was significant higher (p?in vitro on MCF-7 cells. Furthermore, cell uptake studies evidenced a higher uptake of positive NCs (≥1.2 fold) in comparison to negative NCs. In conclusion, formulated NCs are an ideal vehicle for passive targeting of drugs to tumor cells that may result in improved efficacy and reduced toxicity of encapsulated drug moiety.     

Test methods for characterizing concrete properties at elevated temperature

Fire resistance of structural members is dependent on the thermal and mechanical properties of constituent materials and these properties vary as a function of temperature. Currently, there are limited standardized test procedures for evaluating thermal and mechanical properties of construction materials at elevated temperatures. This paper provides a review and assessment of test methods and procedures for evaluating high temperature thermal and mechanical properties of concrete. The drawbacks and variations in currently available test procedures and methods in standards are discussed. Recommendations on the most suitable methods and procedures for measuring thermal and mechanical properties at elevated temperature is presented. In addition, applicability of the proposed high temperature test methods and procedures is illustrated through a case study on conventional concrete specimens. Further, the need for developing standards by organizations such as American Society for Testing and Materials (ASTM), with standardized specifications and test procedures for measuring high temperature properties of construction materials, is laid out.     

Dufour and Soret influence on MHD boundary layer flow of a Maxwell fluid over a stretching sheet with nanoparticles

An analysis has been carried out to examine the heat and mass transfer properties of a two-dimensional incompressible electrically conducting Maxwell fluid over a stretching sheet in the existence of Soret, Dufour, and nanoparticles. In many practical scenarios, such as the polymer extrusion process, the problem presented here is crucial. The flow is examined in terms of the impacts of magnetohydrodynamics and elasticity. Brownian motion and thermophoresis are incorporated into the transport equations. Using adequate similarity variables, the governing partial differential equations and related boundary conditions are non-dimensionalized. The fourth–fifth-order Runge–Kutta–Fehlberg procedure is utilized to solve the consequent transformed ordinary differential equations. The effects of various embedded thermo-physical parameters on the fluid velocity, temperature, concentration, Nusselt number, and Sherwood number have been determined and discussed quantitatively. A comparison of a special case of our results with the one previously reported in the literature shows a very good agreement. An increase in the values of Du and Sr leads to an increase in the temperature and concentration distribution. Nusselt number estimates decrease as Nb estimations increase. Furthermore, this study leads to the study of different flows of electrically conducting fluid over a stretching sheet problem that includes the two-dimensional nonlinear boundary equations.