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11.
Nanocrystalline Gd2O3:A (A=Eu3+, Dy3+, Sm3+, Er3+) phosphor films and their patterning were fabricated by a Pechini sol–gel process combined with a soft lithography. X-ray diffraction (XRD), atomic force microscopy (AFM), scanning electron microscopy (SEM) and optical microscopy, UV/vis transmission and photoluminescence (PL) spectra as well as lifetimes were used to characterize the resulting films. The results of XRD indicated that the films began to crystallize at 500 °C and that the crystallinity increased with the elevation of annealing temperatures. Uniform and crack free non-patterned phosphor films were obtained by optimizing the composition of the coating sol, which mainly consisted of grains with an average size of 70 nm and a thickness of 550 nm. Using micro-molding in capillaries technique, we obtained homogeneous and defects-free patterned gel and crystalline phosphor films with different stripe widths (5, 10, 20 and 50 μm). Significant shrinkage (50%) was observed in the patterned films during the heat treatment process. The doped rare earth ions (A) showed their characteristic emission in crystalline Gd2O3 phosphor films due to an efficient energy transfer from Gd2O3 host to them. Both the lifetimes and PL intensity of the rare earth ions increased with increasing the annealing temperature from 500 to 900 °C, and the optimum concentrations for Eu3+, Dy3+, Sm3+, Er3+ were determined to be 5, 0.25, 1 and 1.5 mol% of Gd3+ in Gd2O3 films, respectively. 相似文献
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分析了我国典型炼油厂FCC汽油硫含量和烯烃含量的变化情况,将MIP汽油[采用多产异构烷烃FCC工艺(Maximizing Iso-Paraffins)生产的汽油],与常规FCC汽油的性质进行了比较,介绍了用OCT-M技术(FCC汽油选择性加氢脱硫技术)对MIP汽油进行深度加氢脱硫的研究情况,包括加工方案的比较、反应压力的影响.结果表明,OCT-M FCC汽油选择性加氢脱硫技术可以将烯烃体积分数为31%的MIP汽油的硫质量分数由664 μg/g降低到50 μg/g以下,研究法辛烷值损失0.7~1.7,OCT-M技术能够为我国炼油厂由MIP汽油生产符合欧Ⅳ标准的清洁汽油提供灵活、经济的技术解决方案. 相似文献
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The kinetics of substrate removal by the liver and the resulting nonlinear changes in unbound fraction along the flow path at varying input drug concentrations were examined by a model simulation study. Specifically, we varied the binding association constant, KA, and the Michaelis-Menten constants (Km and Vmax) to examine the steady state drug removal (expressed as hepatic extraction ratio E) and changes in drug binding for (i) unienzyme systems and (ii) simple, parallel metabolic pathways; zonal metabolic heterogeneity was also added as a variable. At low KA, E declined with increasing input drug concentration, due primarily to saturation of enzymes; only small differences in binding were present across the liver. At high KA, a parabolic profile for E with concentration was observed; changes in unbound fraction between the inlet and the outlet of the liver followed in parallel fashion. Protein binding was the rate-determining step at low input drug concentrations, whereas enzyme saturation was the rate-controlling factor at high input drug concentration. Heterogeneous enzymic distribution modulated changes in unbound fraction within the liver and at the outlet. Despite marked changes in unbound fraction occurring within the liver for different enzymic distributions, the overall transhepatic differences were relatively small. We then investigated the logarithmic average unbound concentration and the length averaged concentration as estimates of substrate concentration in liver in the presence of nonlinear drug binding. Fitting of simulated data, with and without assigned random error (10%), to the Michaelis-Menten equation was performed; fitting was repeated for simulated data obtained with presence of a specific inhibitor of the high-affinity, anteriorly distributed pathway. Results were similar for both concentration terms: accurate estimates were obtained for anterior, high affinity pathways; an overestimation of parameters was observed for the lower affinity posteriorly distributed pathways. Improved estimations were found for posteriorly distributed pathways upon inhibition with specific inhibitors; with added random error, however, the improvement was much decreased. We applied the method for fitting of several sets of metabolic data obtained from rat liver perfusion studies performed with salicylamide (SAM) (i) without and (ii) with the presence of 2,6-dichloro-4-nitrophenol (DCNP), a SAM sulfation inhibitor. The fitted results showed that SAM sulfation was a high-affinity high-capacity pathway; SAM glucuronidation was of lower affinity but comparable capacity as the sulfation pathway, whereas SAM hydroxylation was of lower affinity and lower capacity. 相似文献
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考虑变质量湍流影响的水平井流入动态分析 总被引:1,自引:0,他引:1
在水平井生产过程中,井筒内管流与地层渗流互相制约、互相影响、互为边界条件,从而构成了一个完整的水动力学体系。根据水平井生产时井筒内管流与油藏的相互作用关系,建立了水平井筒存在压力梯度的变质量湍流与地层渗流的耦合计算新方法。关于井筒内流的计算;应用了经典的kεM湍流模型,关于地层的渗流计算,采用了有限元法。通过耦合模拟获得了井筒内湍流场流速分布及总压能损耗的规律,根据耦合模拟计算结果绘出了较为准确的水平井流入动态曲线。该计算方法为描述水平井流入动态、评价水平井产能、确定合理生产制度提供了可靠的手段. 相似文献
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挤压力对晶体生长速度及枝晶间距的影响 总被引:4,自引:4,他引:0
研究了挤压铸造时挤压力对宏观晶体生长速度的影响,给出了晶体生长速度表达式。结果表明:挤压力对合金宏观晶体生长速度的影响除与合金成分有关外,在某些挤压条件下,当形核率的增加幅度超过长大速度时,则挤压力可使宏观晶粒细化;反之,会使宏观晶粒变粗。随着挤压力的提高,合金凝固速度加快,一次枝晶间距和二次枝晶间距都随之减小,从而细化了树枝晶。 相似文献
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