纳米涂层的研究现状与展望

简述了纳米表面涂层制备工艺的研究现状，分析了气相沉积、热喷涂、电刷镀、化学镀和电沉积等不同工艺在制备纳米表面层中的应用情况。介绍了纳米涂层在超硬耐磨、耐腐蚀、耐高温热稳定性等方面研究的新进展，并对纳米涂层的应用范围和领域作了展望。     

变频调速技术在济钢焦化厂高压氨水泵上的应用

济钢焦化厂高压氨水泵变频调速系统采用变频器和PLC相结合的方式 ,具有调速精度高、节能等多种功能 ,保证氨水泵正常工作。全年可增加经济效益 77.3万元。     

碎煤齿环堆焊材料与工艺研究

通过对碎煤齿环的失效分析 ,找出了影响齿环寿命的因素及薄弱环节 ,并研制成功了最优成分的耐磨材料和堆焊工艺 ,显著提高了生产率和企业的经济效益     

化学镀SiCp／Ni－P复合镀层与基体结合强度及其影响因素

论述了ＳｉＣｐ／Ｎｉ－Ｐ复合镀层与钢基体的结合强度及其影响因素。复合镀层中离界面５μｍ厚度以内区域的组成及应力状态对镀层／基体的界面结合有决定性作用，在该区域以外ＳｉＣ粒径变化不影响镀层的结合强度。适当的热处理可提高界面结合力。     

Overexpression, purification, and characterization of SHPTP1, a Src homology 2-containing protein-tyrosine-phosphatase

A protein-tyrosine-phosphatase (PTPase; EC 3.1.3.48) containing two Src homology 2 (SH2) domains, SHPTP1, was previously identified in hematopoietic and epithelial cells. By placing the coding sequence of the PTPase behind a bacteriophage T7 promoter, we have overexpressed both the full-length enzyme and a truncated PTPase domain in Escherichia coli. In each case, the soluble enzyme was expressed at levels of 3-4% of total soluble E. coli protein. The recombinant proteins had molecular weights of 63,000 and 45,000 for the full-length protein and the truncated PTPase domain, respectively, as determined by SDS/PAGE. The recombinant enzymes dephosphorylated p-nitrophenyl phosphate, phosphotyrosine, and phosphotyrosyl peptides but not phosphoserine, phosphothreonine, or phosphoseryl peptides. The enzymes showed a strong dependence on pH and ionic strength for their activity, with pH optima of 5.5 and 6.3 for the full-length enzyme and the catalytic domain, respectively, and an optimal NaCl concentration of 250-300 mM. The recombinant PTPases had high Km values for p-nitrophenyl phosphate and exhibited non-Michaelis-Menten kinetics for phosphotyrosyl peptides.     

n-Al2O3/Ni复合镀层的组织与滑动磨损性能研究

用电刷镀技术制得了镍基n-Al2O3复合镀层，并对镀层的滑动磨损性能进行了试验研究。纳米复合镀层的表面形貌比较细腻，镀层中纳米粒子分布均匀，与基质金属结合紧密。镀层显微硬度达到HV700，比快速镍镀层提高约40％。滑动磨损试验结果表明，随着纳米粒子含量的增大，镀层的耐磨性提高，摩擦系数也呈增大趋势；但当镀层中n-Al2O3粒子的超过2.56%(质量分数）时，镀层的耐磨性显著下降。纳米复合镀层的磨损机制以疲劳磨损为主，而快速镍底层以粘着磨损为主。     

轴齿轮断齿失效分析

通过对轴齿轮断口形貌、硬度测试及金相组织等试验进行分析表明，齿根处没有进行硬化处理造成齿根处抗疲劳性能不足是导致轴齿轮疲劳断裂的主要原因，另外齿根过渡处倒角过小，且存在纵向刀痕引起了较大应力集中也是导致轴齿轮疲劳断裂的原因。     

波节管当量壁厚研究

应用ANSYS对波节管和对应光管轴向刚度进行了分析,用数学软件Origin对有限元分析结果进行了拟合,归纳了将波节管的壁厚转换成对应光管壁厚的当量关联式,通过该关联式可将波节管换热器的管板按光管换热器管板来设计,为波节管换热器的管板设计提供了一种有效方法。     

On the coherent interference suppression using a spatiallysmoothing adaptive array

The behavior of a spatially smoothing adaptive array is examined. An expression for the weight vector is first derived. Using the array gain on the desired signal and the coherent interference is obtained. Then the expression for output signal-to-noise (SNR) is derived. It shows that the performance of the spatially smoothing array depends on the number of the subarrays, the angle separation, relative power and initial phase difference between the desired signal and the coherent interference. For good interference suppression it is found that the magnitude of the phase difference of the incident and interference signals must be greater than the beamwidths of both the subarray and the equivalent array. There is also a tradeoff between increasing the groups of subarrays and decreasing the number of elements in the subarrays. Computer simulation results are given that validate the analysis     

131I-epidepride的制备与SD大鼠体内分布特性研究

采用双氧水标记法和氯胺 -T法进行13 1I -epidepride标记 ,考察标记物的纯度及稳定性 ,并进行SD大鼠体内分布特性研究。实验结果表明 ,双氧水法和氯胺 -T法标记率分别为 97.4 %和 5 2 .9%。标记物的生理盐水溶液室温放置 4h ,放化纯大于 90 %。大鼠静脉注射13 1I -epide pride的生理盐水溶液后 ,纹状体与小脑比值在注射后 32 0min时高达 2 37:1。13 1I -epidepride进入血液后很快被组织摄取 ,其中以肺的早期摄取最高 (2 .11± 1.0 5 ) %ID·g- 1,各脏器的清除均较快 (T1/2 <4h) ,甲状腺的摄取率随时间的延长而增加。