2519铝合金热压缩变形流变应力行为

在 Gleeble- 15 0 0热模拟机上对 2 5 19铝合金进行等温热压缩实验 ,变形温度为 30 0～ 5 0 0℃ ,应变速率为0 .0 5～ 2 5 s- 1 ,研究其热压缩变形的流变应力行为。结果表明 :2 5 19铝合金真应力 -应变曲线在低应变速率 (ε<2 5 s- 1 )条件下 ,流变应力开始随应变增加而增大 ,达到峰值后趋于平稳 ,表现出动态回复特征 ;而在高应变速率 (ε≥ 2 5 s- 1 )条件下 ,应力出现锯齿波动达到峰值后逐渐下降 ,表现出不连续再结晶特征。在用 Arrhenius方程描述 2 5 19铝合金热变形行为时 ,其变形激活能 Q为 16 7.81k J/ mol     

TC4钛合金的热变形行为及其影响因素

利用Gleeble1500热模拟机测试了Ti6Al4V合金在不同温度和不同应变速率下的真应力真应变曲线,观察热变形前后的组织,分析变形温度、应变速率、原始组织和热处理工艺对合金的热变形行为的作用及影响规律。结果表明,在应变速率为8.3×10-3s条件下,合金在600℃热变形时软化机制以动态回复为主,800℃至900℃热变形时软化机制以动态再结晶为主;700℃热变形时动态回复和动态再结晶可同时发生。淬火和时效可提高合金的热变形抗力。合金在600℃变形时,热变形抗力对在8.3×10-2s-8.3×100s范围变化的应变速率敏感性较差;当应变速率降至8.3×10-3s-1时,热变形抗力有较大幅度的降低。在相同的变形条件情况下,魏氏组织的流变应力高于等轴组织。     

2519铝合金热变形流变行为

采用Gleeble-1500热模拟机进行高温等温压缩实验,研究了2519铝合金在变形温度为300～450℃、应变速率为0.01～10 s-1条件下的流变变形行为.结果表明:应变速率和变形温度对合金流变应力的大小有显著影响,流变应力随温度升高而降低,随应变速率的提高而增大,在应变速率ε＜10 s-1条件下,流变应力开始随应变增加而增大,达到峰值后趋于平稳,表现出动态回复的特征;而在ε=10 s-1,t≥350℃的变形条件下,合金发生了局部动态再结晶.可用包含Arrhenius项的Zener-Hollomon参数描述2519铝合金高温塑性变形时的流变行为.     

Ti-46Al-2Cr-4Nb-Y合金的高温变形及加工图

采用Gleeble-1500 热压缩模拟试验机进行压缩实验,在变形温度为1 100～1 250 ℃、应变速率为10-2～ 1 s-1的范围内,研究Ti-46Al-2Cr-4Nb-Y合金的高温变形行为,并基于动态材料模型,建立Ti-46Al-2Cr-4Nb-Y合金的加工图.结果表明:Ti-46Al-2Cr-4Nb-Y合金的高温变形流变应力对温度及应变速率敏感;流变应力随应变速率的增大而增大,随温度的升高而减小;动态再结晶是导致流变软化及稳态流变的主要原因;Ti-46Al-2Cr-4Nb-Y合金的安全热加工区域为温度1 200～1 230 ℃,应变速率10-2～10-1 s-1.     

铝青铜合金热变形流变应力特征

采用Gleeble-3500热模拟机进行圆柱体压缩试验,研究了新型铝青铜合金在变形温度为650～950℃、应变速率为0.01～5s-1、真应变为0～0.8条件下的流变应力特征。结果表明:应变速率为0.01和5s-1时,铝青铜合金首先出现加工硬化,流变应力达到峰值后趋于平稳,表现出动态回复的特征;应变速率为0.1和1s-1时,合金发生了局部动态再结晶;可用Zener-Hollomon参数的双曲正弦形式来描述新型铝青铜合金热压缩变形时的流变应力行为。     

Al-Zn-Mg-Sc-Zr合金的热变形行为及加工图

在Gleeble-1500热模拟试验机上对Al-5.5Zn-1.5Mg-0.2Sc-0.1Zr铝合金进行高温等温压缩实验,研究该合金在变形温度为300～500℃、应变速率为0.01～10s-1条件下的流变行为,建立合金高温变形的本构方程和加工图,采用电子背散射衍射(EBSD)分析变形过程中合金的组织特征.结果表明流变应力随变形温度的升高而降低;当应变速率ε=10s-1,变形温度为300～500℃时,合金发生了动态再结晶.Al-5.5Zn-1.5Mg-0.2Sc-0.1Zr合金的高温流变行为可用Zener-Hollomon参数描述.在热变形过程中,随着真应变增加,合金的变形失稳区域增大.该合金适宜的变形条件如下变形温度300～360℃、应变速率0.01～0.32s-1,或变形温度380～500℃、应变速率0.56～10s-1.     

高强可焊2195铝-锂合金热压缩变形的流变应力

在Gleeble-1500热模拟实验机上,采用高温等温压缩,0.001～10 s-1,变形温度为360～520℃,对2195铝-锂合金在高温压缩变形中的流变应力行为进行了研究,分析了其高温变形的物理本质.结果表明:在应变速率为1 s-1(变形温度为520℃)和应变速率为0.1、0.01、0.001 s-1(变形温度为360～520℃)时,2195铝-锂合金热压缩变形流变应力出现了明显的峰值应力,表现为连续动态再结晶特征;在其它变形条件下存在较为明显的稳态流变特征;可采用Zener-Hollomon参数的双曲正弦函数来描述2195铝-锂合金高温变形时的流变应力行为;在获得的流变应力σ解析表达式中,A、α和n值分别为2.569×1017 s-1、0.012 48 MPa-1和5.94;热变形激活能Q为250.45 kJ/mol.     

Al—Cu—Mg—Ag合金热变形本构方程模型

在Gleeble-1500热模拟机上进行高温等温压缩试验,研究了Al-Cu-Mg-Ag合金在变形温度为300～500 ℃、应变速率为0.01～10.00 s-1条件下的流变变形行为,建立了Al-Cu-Mg-Ag合金热变形本构方程.结果表明,流变应力随温度的降低、应变速率的提高而增大,在应变速率小于10.00 s-1的条件下,流变应力随应变增加而迅速增大,达到峰值后趋于平稳,表现出动态回复的特征;在应变速率为10.00 s-1,温度大于300 ℃的条件下,应力达到峰值后逐渐下降,并出现锯齿波动现象,表明合金发生了局部动态再结晶;Al-Cu-Mg-Ag合金高温变形时的流变行为可用Zener-Hollomon参数来描述,其变形激活能为160.08 kJ/mol.     

铸态ZnAl10Cu2合金热变形本构方程

在Gleeble-3500热模拟机上采用等温压缩实验研究了ZnAl10Cu2合金在温度为210～300℃、应变速率为10-2～10 s-1条件下的热变形行为,获得了该合金热变形过程中的真应力-应变曲线.结果表明:ZnAl10Cu2合金的峰值流变应力随温度升高而降低,随应变速率的提高而增大.通过双曲正弦模型确定了该合金的...     

GH4199合金的热变形行为与微观组织演变

在变形温度为1050～1180℃、应变速率为0.1～10s-1、最大真应变为0.7的条件下,采用Gleeble-3500热模拟试验机研究GH4199合金的热压缩变形行为,得到该合金的热变形激活能及热变形方程式,建立合金的热加工图,并通过组织观察对其热加工图进行解释。结果表明:在实验条件下,GH4199合金均表现出动态再结晶特征;变形温度和应变速率对合金流变应力及相应峰值应变大小的影响显著,流变应力及峰值应变均随着变形温度的降低和应变速率的增加而增大;在真应变为0.1～0.7时合金的热加工图相似,随着变形温度的升高及应变速率的降低,能量消耗效率逐渐升高;在应变速率为0.01s-1时,能量消耗效率达到峰值,约为41%。     

Effects of Post-weld Heat Treatment on Microstructure,Mechanical Properties and the Role of Weld Reinforcement in 2219 Aluminum Alloy TIG-Welded Joints

In as-welded state, each region of 2219 aluminum alloy TIG-welded joint shows diff erent microstructure and microhardness due to the diff erent welding heat cycles and the resulting evolution of second phases. After the post-weld heat treatment, both the amount and the size of the eutectic structure or θ phases decreased. Correspondingly, both the Cu content in α-Al matrix and the microhardness increased to a similar level in each region of the joint, and the tensile strength of the entire joint was greatly improved. Post-weld heat treatment played the role of solid solution strengthening and aging strengthening. After the post-weld heat treatment, the weld performance became similar to other regions, but weld reinforcements lost their reinforcing eff ect on the weld and their existence was more of an adverse eff ect. The joint without weld reinforcements after the post-weld heat treatment had the optimal tensile properties, and the specimens randomly crack in the weld zone.     

The First Phase of the SRIF Industrialized Base in ＂West Area＂ Has Been Put into Operation

After nearly two years＇ tense construction, the first phase of industrialized base of Shenyang Research Institute of Foundry （SRIF）, located at the Tiexi Casting and Forging Industrial Park in the west of Tiexi District, has now been completed and formally put into operation.     

新型的治疗阿尔茨海默氏症药物(1-二甲基磷酰基-2,2,2-三氯)-乙基-1-醇烟酸醋对体外神经细胞的作用

目的: 观察本实验室合成的一种治疗阿尔茨海默氏症(AD)的药物(1-二甲基磷酰基-2, 2, 2 -三氯)-乙基^-1-醇烟酸醋(NMF),对体外培养的皮层神经细胞活性的影响以及对海人藻酸(KA)所致的神经损伤的保护作用。方法: 采用体外培养皮层神经元的方法,解剖分离 15 d胚胎小鼠皮层神经细胞, 接种于 96孔板,48 h 后加药并培养 72 h,以 MIT 法 观察 NMF 对小鼠皮层神经细胞活性的影响;同时将接种于 24 孔板的细胞预先给予 NMF,d 3 时加或不加KA处理后,以台盼蓝染色鉴别并计数死、活细胞,可得出细胞的存活率。结果: NMF 明显促进胎鼠皮层神经元活性,其中 NMF1、0. 1、10nmol·L^-1促进神经元活性增殖率分别高达 34.7%、37.4%、36. 7%, NMF 明显促进正常胎鼠皮层神经元存活卒,与对照组比较,10nmol·L^-1 NMF 对皮层神经元的存活率分别提高 39.3%、73.5%。 NMF能显著 对抗 KA 所致的神经元损伤,与 KA 损伤组相比, NMF0.1、10、10nmol·L^-1对损伤皮层神经元的保护率分别为 77.30%、80.10%、84.15%。结论: NMF 明 显促进胎鼠皮层神经元的洁性、提高正常皮层神经元,的存活卒,并能有效地保护KA所致的神经元损伤,提示 NMF 是一种很有潜力的治疗 AD 的药物。     

Theoretical Analysis for the Motion and Temperature of Melt Droplets in Spray Degassing Process

The motion of melt droplets in spray degassing process was analyzed theoretically. The height of the treatment tank in spray degassing process could be determined by the results of theoretical calculation of motion of melt droplets. To know whether the melt droplets would solidify during spraying process, the balance temperature of melt droplets was also theoretically analyzed. Then proof experiments for theoretical results about temperature of melt droplets were carried. In comparison, the experimental results were nearly similar to the calculation results.     

Growth Kinetics of Single Inclusion Particle in Molten Melts

On the basis of the single-particle framework, a new theory on inclusion growth in metallurgical melts is developed to study the kinetics of inclusion growth on account of reaction and collision. The studies show that the early growth of inclusion depends on reaction growth and Brawnian motion collision, and where the former is decisive, the late growth depends on turbulence collision and Stokes＇ collision, and where the former is dominant; collision growth is very quick during the smelting process, lessened in the refining process, but nearly negligible in the continuous casting process.     

An Easy Way to Quantify the Adhesion Energy of Nanostructured Cu/X(X=Cr,Ta,Mo,Nb,Zr) Multilayer Films Adherent to Polyimide Substrates

An approach based on film buckling under simple uniaxial tensile testing was utilized in this paper to quantitatively estimate the interfacial energy of the nanostructured multilayer films(NMFs) adherent to flexible substrates. The interfacial energies of polyimide-supported NMFs are determined to be *5.0 J/m2 for Cu/Cr, *4.1 J/m2 for Cu/Ta,*2.8 J/m2 for Cu/Mo, *1.1 J/m2 for Cu/Nb, and *1.2 J/m2 for Cu/Zr NMFs. Furthermore, a linear relationship between the adhesion energy and the interfacial shear strength is clearly demonstrated for the Cu-based NMFs, which is highly indicative of the applicability and reliability of the modified models.     

High-Speed Friction Stir Welding of SiC_p/Al–Mg–Si–Cu Composite

A 17 vol% SiCp/Al–Mg–Si–Cu composite plate with a thickness of 3 mm was successfully friction stir welded(FSWed) at a very high welding speed of 2000 mm/min for the first time. Microstructural observation indicated that the coarsening of the precipitates was greatly inhibited in the heat-affected zone of the FSW joint at high welding speed, due to the significantly reduced peak temperature and duration at high temperature. Therefore, prominent enhancement of the hardness was achieved at the lowest hardness zone of the FSW joint at this high welding speed, which was similar to that of the nugget zone. Furthermore, the ultimate tensile strength of the joint was as high as 369 MPa, which was much higher than that obtained at low welding speed of 100 mm/min(298 MPa). This study provides an effective method to weld aluminum matrix composite with superior quality and high welding efficiency.     

Three-Dimensional Growth of Coherent Ferrite in Austenite: A Molecular Dynamics Study

Coherent second phase often exhibits anisotropic morphology with specifi c orientations with respect to both the second and the matrix phases. As a key feature of microstructure, the morphology of the coherent particles is essential for understanding the second-phase strengthening eff ect in various industrial alloys. This letter reports anisotropic growth of coherent ferrite from austenite matrix in pure iron based on molecular dynamics simulation. We found that the ferrite grain tends to grow into an elongated plate-like shape, independent of its initial confi guration. The fi nal shape of the ferrite is closely related to the misfi t between the two phases, with the longest direction and the broad facet of the plate being, respectively, consistent with the best matching direction and the best matching plane calculated via the Burgers vector content(BVC) method. The strain energy calculation in the framework of Eshelby's inclusion theory verifi es that the simulated orientation of the coherent ferrite is energetically favorable. It is anticipated that the BVC method will be applicable in analysis of anisotropic growth and morphology of coherent second phase in other phase transformation systems.     

A STUDY OF TEMPERATURE-DEPENDENT VALENCE BOND STRUCTURE OF TITANIUM

On the basis of energy and shape method for the determination of the valence bond (VB) structures of crystal, the valence bond structure of titanium is redetermined at room temperature and calculated in the whole temperature range of 0-1943K. The outer shell electronic distribution of Ti is e_c~(2.9907) · (s_c~(0.4980) d_c~(2.4927)) ef1.0093 in crystal. The temperature dependences of the VB structures of hcp and bcc phases are the same. The VB structures of hcp and bcc phases monotonically increase or decrease with the increase in temperature, but show discontinuous changes at the phase-transformation temperature 1155K.     

Structural Optimization of Electromagnetic Swirling Flow in Nozzle of Slab Continuous Casting

During the slab continuous casting process, the flow field of molten steel in the mold plays a decisive role in the quality of the slab. In this paper, electromagnetic swirling flow in nozzle technology is proposed to control the flow field in mold.This technology can drive molten steel to rotate inside the submerged entry nozzle by electromagnetic force, thereby controlling the flow field. This research shows that it can reduce the impact of molten steel on the bottom of nozzle and partly reduce the negative pressure at the upper part of nozzle outlet which is even eliminated by optimizing the structure and angle of nozzle. The area of heat flux of the mold wall becomes larger, and the crest value of heat flux gets lower than that without swirling in nozzle and any nozzle optimization. The meniscus fluctuates smoothly, and the flow velocity at the top surface is within a reasonable range. The temperature field distribution in the mold is uniform which was beneficial to the growth of equiaxed crystal and decreased element segregation.