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红树莓叶片中黄酮类物质提取及抗氧化性的研究 总被引:20,自引:0,他引:20
以小浆果果树红树毒叶片为实验材料,利用分光光度法测定其总黄酮含量,并采用烘箱贮存法研究了不同添加量红树毒叶片提取物粗黄酮在猪油中的抗氧化性。结果表明:鲜样中红树毒叶片总黄酮含量是278.73mg/100g,干样中是533.71mg/100g;红树毒叶片提取物粗黄酮对猪油有一定的抗氧化作用,并随添加量的增加而增强;增效剂以(柠檬酸)对红树毒叶片提取物粗黄酮无增效作用,而Vc具有一定的增效作用。抗氧化活性顺序为:0.02%槲皮素>0.02%PG>0.02%BHT>0.4%粗黄酮>0.05%粗黄酮 0.05%Vc>0.2%粗黄酮>0.1%粗黄酮>0.05%粗黄酮>0.02%粗黄酮>0.05%粗黄酮 0.05%CA>对照。 相似文献
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以高效液相色谱法测定了桂林地区兴安县采集的银杏雌雄植株青叶及其落地黄叶的黄酮含量。结果表明,银杏叶总提取物黄酮含量在2.0%~3.0%之间,雌树青叶总提取物黄酮含量高,雄树青叶次之,落地黄叶最少,但三者相差甚小。 相似文献
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介绍了以苦瓜植株各部分为原料用微波法提取黄酮,通过正交试验对该方法进行了最佳条件的探讨。实验结果表明:以体积分数50%乙醇水溶液作提取溶剂,固液比1:30(g/mL),微波照射2min,浸提时间1h,提取温度80℃,苦瓜叶中黄酮提取率最高。并用该最佳条件分别提取苦瓜叶、茎、果、根的黄酮类化合物,测其质量分数分别为1.616%、0.453%、1.535%、0.875%。 相似文献
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玫瑰茄细胞红色素中总黄酮的分离及含量测定 总被引:10,自引:0,他引:10
用1%HCl—甲醇溶液或1%HCl—乙醇溶液提取的玫瑰茄细胞红色素中含有黄酮物质。用纸层析方法(流动相BHW)分离黄酮时,花青素的移迁率为0.34,黄酮为0.71;采用硅胶薄层层析时,迁移率分别为0.14和0.32,经测定,玫瑰茄细胞色素中总黄酮含量为15.30~21.50mg/g。 相似文献
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选用乙醇作为提取溶剂,对高粱中总黄酮进行提取,研究乙醇浓度、浸提温度、浸提时间、料液比对高梁黄酮提取率的影响.并通过单因素及正交试验,确定了高梁黄酮的最佳提取工艺:乙醇浓度为65%,80oC下浸提2h,料液比为6:100.此工艺下提取的高粱黄酮含量为0.54%. 相似文献
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蛋白质水解度测定方法综述 总被引:27,自引:0,他引:27
对目前国内外常用的蛋白质水解度测定方法进行了综述,其中pH—state方法是通过滴定水解过程中释放的质子测定DH;OPA、TNBS及国内常用的水合茚三酮和甲醛等测定方法是利用游离氨基的反应测定DH。 相似文献
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研究了聚多元羧酸盐的合成方法及反应机理,将其应用于洗涤剂和PVC制品中分别代替三聚磷酸钠和邻苯二甲酸二丁酯,证明有良好效果。 相似文献
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SUMMARY: A partially purified immunoglobulin G (lgG) solution prepared from the serum of species to be tested was heated to the specifications for sausages. The resulting supernatant fluid was decanted and the precipitate washed with saline and used to immunize rabbits. The supernatant fluid was used to sensitize tanned sheep red blood cells. The immune serum was rendered monospecific by absorptions with heterologous, heated lgG precipitates. A sample of monospecific immune serum was absorbed with a washed homogenate of sausage. Aliquots of the monospecific immune serum, both untreated and sausage absorbed, were tested with cells sensitized with the homologous heated lgG supematant fluid. A significant reduction of titer by sausage absorption indicated that the sausages contained the meat homologous to the immune serum. 相似文献
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SUMMARY— The mechanism and generality of the known stabilization against autoxidation conferred on linoleic acid by certain basic amino acids, such as lysine and arginine, was investigated. Basic amino acids were the only class of compounds found to confer the effect. However, the smallest basic amino acid, 2,3-diaminopropionic acid, was not effective, nor was αβω-diaminc acid, 3,6-diaminohexanoic acid, although a simple isomer of lysine. The stabilization was observed only in the solid phase. Inclusion of sodium chloride in the solid matrix was deleterious to the effect. A large number of physical and chemical observations were made and correlated but it has not been possible to draw detailed conclusions about the mechanism of stabilization, nor can a detailed structure of the stabilized complex be suggested. The cause of the phenomenon appears to be closely associated with the physical arrangement of the ions in the crystal lattice. 相似文献
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Hop oil emulsions prepared from different varieties of hops have been found to exhibit enhanced physical stability on the addition of blends of the emulsifiers Span 20/Tween 80 or Span 60/Tween 60. Examination of the particle size and volume distributions of an emulsion by use of a Coulter Counter was found to be an excellent method of monitoring its stability. An indication as to the relative efficiency of emulsifiers can be obtained from Coulter Counter measurements on hop oil emulsions after storage for 4 days. The use of an ultracentrifuge provies a rapid means of testing emulsion stability and hence the effectiveness of emulsion stabilizers. 相似文献
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矩阵乘积的行式,列式 总被引:1,自引:0,他引:1
张静 《郑州轻工业学院学报(自然科学版)》1997,12(3):72-74
给出了m×m矩阵与m×n矩阵的行(列)式的表达式.若A=a11a12…a1ma21a22…a2m……am1am2…ammB=b11b12…b1nb21b22…b2n……bm1bm2…bmn分别是m×m,m×n矩阵,则|A||B|=|AB|+∑i1<i2<…<itj1<j2<…<jt1≤t≤mn-t≥mNBi1i2…itj1j2…jtNAB1…m(-1)st+1jt+1…(-1)snjn其中i1,i2,…,it是1,2,…,m中t个数码;j1,j2,…,jt,jt+1,…,jn是1,2,…,n的一个排列;sr=π(j1,j2,…,jt,jr)(r=1,2,…,n)是排列j1,j2,…,jt,jr的反序数. 相似文献
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《中国服装(北京)》2013,(19):130-133
一场流光溢彩、赏心悦目的展览,一段百年风尚演进的传奇旅程,一次东西方文化艺术的完美对话。2013年9月13日,“博萃臻艺一中西方珍宝艺术展”在辽宁省博物馆举行了隆重的开幕仪式,法兰西共和国驻华大使白林女士、辽宁省文物局局长丁辉先生、辽宁省博物馆馆长马宝杰先生、卡地亚全球总裁兼首席执行官邓阁仕先生、卡地亚区域行政总裁(北亚洲)陆慧全先生、卡地亚中国区首席执行官陆意斯先生、辽宁省文物店总经理张春鹰先生,以及众多文化界与文博界的贵宾齐聚一堂,共同见证了这场文化艺术盛事。 相似文献
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ABSTRACT— The effect of time, temperature and rpm of comminution of emulsions was determined on the dispersion of approximately 25% of beef fat, pork fat or cottonseed oil in frankfurters. The numbers of lipid particles 5 μ or less in diameter increased in frankfurters containing either beef or pork fat as comminution was continued to higher temperatures, with pork fat dispersed more thoroughly. Fat tended to separate from frankfurters containing beef fat in particles 200 μ or more in diameter. In contrast, no specific degree of dispersion of particles 5 μ or less in diameter consistently indicated emulsion stability, or its lack. Increased rpm during comminution produced an increased dispersion of beef or pork fat. Under the same conditions pork fat was dispersed more finely than beef fat. Dispersion of cottonseed oil produced finely dispersed particles beyond the resolution of light microscopy, as was confirmed by electron microscopy which showed a substantial number of particles to be less than 1 μ in diameter. 相似文献
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张仲民 《郑州轻工业学院学报(自然科学版)》1993,8(3):21-24
本文基于点的复合运动理论,用球坐标法推导出点的速度及加速度的计算公式,进一步论证了理论力学中点的速度,加速度公式的正确性。 相似文献