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辐照食品分析检测技术的研究进展 总被引:8,自引:0,他引:8
本文介绍了国内外辐照食品检测技术的研究进展,着重对化学分析法、电子自旋共振(ESR)法及热释光分析(TL)法进行了阐述,并对今后辐照食品检测技术的研究提出了建议。 相似文献
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Ihab Tewfik 《International Journal of Food Science & Technology》2008,43(1):108-113
2‐Alkylcyclobutanones (cyclobutanones) are accepted as radiolytic markers in lipid‐containing foods (LCF). To date, cyclobutanones have not been detected in non‐irradiated foods. Their identification is the basis of a standardised detection test for irradiated LCF (BS EN 1785, 2003). This paper reports work to develop and refine a new rapid method for the analysis of cyclobutanones in irradiated LCF (e.g. chicken meat and liquid whole egg). Direct solvent extraction (DSE) enables the efficient screening of large numbers of food samples and is not as resource intensive as the BS EN 1785 (2003) method. The new DSE appears to be a promising, rapid, simple and robust method for the analysis of irradiated lipid‐containing foods. 相似文献
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Consumer awareness and acceptance, and influence of benefit statements and price on acceptance of irradiated foods were investigated in Turkey. Consumer awareness of food irradiation was very low (29%). Majority of consumers (80%) were uncertain about the safety of irradiated foods. Only 11% expressed irradiated foods are safe. Level of positive attitude towards irradiated foods increased substantially (62%) upon hearing a benefit statement of food irradiation. Purchase intent of irradiated foods was highest (44%) when price is same as unirradiated foods, but significant proportion of consumers indicated to pay 5% premium price for irradiated foods. A successful market for irradiated foods can be achieved by educating consumers with the benefit and uses of irradiation process. 相似文献
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Sulaxana Kumari Chauhan R. Kumar S. Nadanasabapathy A.S. Bawa 《Comprehensive Reviews in Food Science and Food Safety》2009,8(1):4-16
ABSTRACT: Proper control of irradiation processing of food is very critical to facilitate international trade of irradiated foods and to enhance consumer confidence, consumer choice, and safety. Analytical detection of radiation‐processing of food is very important to implement quality control at all levels. An ideal detection method should measure a specific radiation effect, which is proportional to the dose and should not be affected by processing parameters and storage conditions or the length of time between irradiation processing and analysis. The detection of irradiated foods is mainly based on radiolysis of lipids, modification of amino acids, modification of DNA, modification of carbohydrates, formation of free radicals, release of hydrogen gas, alterations in microbial load, measurement of biological difference, and other physical methods. 相似文献
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Minimal change in irradiated foods with low dose treatment makes the identification process a difficult task. Two independent physical methods, electron paramagnetic resonance (EPR) spectroscopy and thermoluminescence (TL) detection were employed for detection of irradiation treatment on Basmati rice. EPR investigation of 0.5–2.0 kGy irradiated rice samples showed a short lived, asymmetric, dose dependent spectrum (g = 2.005), characterised by the radicals of irradiated starch. However, this signal disappears with time. The present work explores the possibility to identify irradiated rice by the relaxation characteristics and thermal behaviour of the radicals. This study reports for the first time that the different microwave saturation behaviours of the signal (g = 2.004) in irradiated and non-irradiated rice samples provide an important clue to identify radiation treatment beyond the period when the radiation specific EPR spectral lines have disappeared. TL investigation involving scanning electron microscopy/energy dispersive X-ray analysis (SEM/EDX) of the poly-minerals isolated from the rice samples allowed to discriminate clearly between irradiated and non-irradiated samples even after a prolonged period of storage. 相似文献
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Anne V J Crone Mark V Hand John T G Hamilton Narain D Sharma Derek R Boyd Mary H Stevenson 《Journal of the science of food and agriculture》1993,62(4):361-367
The synthesis and characterisation of 2-tetradecylcyclobutanone (TCB) is described. Both 2-dodecykyclobutanone and TCB were shown to be present in liquid whole egg irradiated at doses of 2.5 and 10.0 kGy. These compounds were absent from the unirradiated pasteurised samples. Using gas chromatography and infrared spectroscopy, there was also evidence for the presence in irradiated egg of 2-tetradeccnyl- and 2-tetradecadienylyclobutanone which are formed from oleic and linoleic acids, respectively. Authentic standards for these unsaturated cyclobutanones were not available commercially but the presence of 2-tetra-decenylcyclobutanone was substantiated by hydrogenating the egg extracts so converting this unsaturated cyclobutanone to TCB. Saturated and unsaturated cyclobutanones appear to be specific products of irradiation and are potential markers for detection of irradiated liquid egg and probably other fat-containing foods. 相似文献
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MARC DESROSIERS DEBRA BENSEN DEANNA YACZKO 《International Journal of Food Science & Technology》1995,30(5):675-680
After many interlaboratory trials, several EPR methods for the detection of irradiated foods are being prepared as standard protocols. The works of Goodman et al. (1994) and Raffi et al. (1992) present conflicting general recommendations for optimum parameter sets in the EPR protocols. Here we demonstrate the shortcomings of recommending general parameter sets for the varying types of food samples and the different spectrometer configurations employed to examine them. 相似文献
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Hydrocarbons, which are produced by irradiation of lipid-containing foods, were analyzed in irradiated soybeans, which were roasted, powdered and stored, to determine whether these treatments affect hydrocarbon detection for identifying post-irradiation of soybeans. Soybeans were irradiated (Irr), irradiated and roasted (Irr–Rst), roasted and irradiated (Rst–Irr), irradiated, roasted and powdered (Irr–Rst–Pwd), and roasted, powdered and irradiated (Rst–Pwd–Irr). They were stored at refrigerated or room temperature for 30 weeks. Oils were extracted using hexane and Na2SO4. Hydrocarbon fraction was separated through a Florisil column and analyzed using GC. Hydrocarbons 17:2, 16:3, 17:1 and 16:2 were not detected in non-irradiated soybeans and soybean powder, but they were detected in those irradiated at 0.5 kGy or higher. The levels of the hydrocarbons increased with dose. The hydrocarbon levels in the Irr–Rst, Rst–Irr, and Irr–Rst–Pwd soybeans were little different from those in the Irr soybeans. Hydrocarbon detection in the Rst–Pwd–Irr soybean powder showed a slightly different pattern from those in the other treatments. Hydrocarbon levels in the soybean and soybean powder samples stored at refrigerated temperature for 30 weeks changed little, compared to initial samples. The hydrocarbon detection patterns in the samples stored at room temperature for 30 weeks were similar to the initial and refrigerated samples with slightly lower detection levels in the room-stored samples. 相似文献