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1.
采用XD法原位合成TiCp/Al预制块, 并通过XRD、 SEM、 EDAX和DTA等手段研究了预制块的组织和性能, 探讨了TiCp/Al预制块在镁液中的熔化行为. 结果表明: TiCp/Al预制块中, 基体Al的熔点约为635.7.℃, 略低于纯铝的熔点, 但TiC粒子之间存在较强的结合力, 使其在高温加热时仍能保持原有形状; 未搅拌时, TiCp/Al预制块在800.℃的镁液中保温60.min后仍不熔化, 采用搅拌工艺有利于促进TiCp/Al预制块的熔化, 并且使TiC粒子在熔体中均匀分布. TiCp/Al预制块在镁液中熔化时, 基体Al通过熔化和对流扩散进入到镁液中, TiC粒子间的较强的结合力需通过搅拌产生的剪切力才能破坏, 并随镁液流动进入到镁液中. 机械搅拌可使TiC粒子在镁液中均匀分布. 相似文献
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TiCp对Zn—10Al合金凝固行为的影响 总被引:3,自引:0,他引:3
利用XD^TM法与搅拌铸造技术相结合的工艺制备了TiCp/Zn-10Al(%)复合材料,采用定向凝固技术研究究增强粒子TiCp在凝固界面的行为及对复合材料凝因速度的影响,结果表明:TiC颗粒被凝固的界面前沿所排斥,造成界面前沿TiC颗粒富集,但当TiC颗粒含量超过6%后,富集现象已不显著。同时发现随着TiC颗粒含量的增加,复合材料的凝固速度降低。 相似文献
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工艺参数对SHS-铸造钢基表面TiC-Fe梯度复合涂层结构的影响 总被引:16,自引:1,他引:16
将自蔓延高温合成(SHS)技术与铸造工艺结合起来,制备了铸造钢基表面TiC—Fe梯度复合材料,研究了钢液的浇注温度、TiC—Fe预制块的组成及其相对密实度等工艺参数对梯度复合涂层结构的影响。结果表明:在保证预制块能被浇注的钢液直接点燃的条件下,适当提高钢液的浇注温度、降低预制块的密实度均有利于梯度复合涂层的形成;而且在预制块中掺加适量的低熔点金属稀释剂不仅可降低合成TiC颗粒的尺寸,而且也有利于梯度复合涂层的形成。梯度复合涂层的形成与钢液向预制块中的渗透、预制块中Fe和低熔点稀释剂的熔化以及合成的TiC颗粒向钢液中的扩散等作用有关。 相似文献
4.
利用XDTM法与搅拌铸造技术相结合的工艺 制备了TiCp/Zn10Al(%)复合材料, 采用定向凝固技术研究增强粒子TiCp在凝固界面的行为及对复合材料凝固速度的影响。结果表明:TiC颗粒被凝固的界面前沿所排斥,造成界面前沿TiC颗粒富集, 但当TiC颗粒含量超过6% 后, 富集现象已不显著。同时发现随着TiC颗粒含量的增加, 复合材料的凝固速度降低。 相似文献
5.
利用XDTM 法与搅拌铸造技术相结合的工艺制备了TiCp/Zn 10Al(% )复合材料 ,采用定向凝固技术研究增强粒子TiCp 在凝固界面的行为及对复合材料凝固速度的影响。结果表明 :TiC颗粒被凝固的界面前沿所排斥 ,造成界面前沿TiC颗粒富集 ,但当TiC颗粒含量超过 6 %后 ,富集现象已不显著。同时发现随着TiC颗粒含量的增加 ,复合材料的凝固速度降低。 相似文献
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通过预制块在铸造Al-4.5%Cu合金熔体中的自蔓延反应,制备了TiCp/Al-4.5%Cu原位复合材料,分析了TiC形成的热力学及其原位生成过程。试验结果表明,TiCp/Al-4.5%Cu原位复合材料的拉伸性能比基体合金有大幅度地提高;原位反应生成的TiC颗粒呈小圆片状,平均直径0.15μm,与基体结合良好,无界面有害相。提出了一种新的TiC颗粒合成机制:Al依次与Ti、C发生反应生成Al3Ti和Al4C3,同时放出大量的热引发了TiC的生成;Al3Ti和Al4C3作为中间反应产物,由于热力学上的不稳定,最终被TiC取代。 相似文献
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热处理对TiCp/Fe复合材料基体组织与力学性能的影响 总被引:1,自引:0,他引:1
通过不同的热处理工艺改变原位TiCp/Fe复合材料的基体组织,探讨了原位TiCp/Fe复合材料不同基体组织与性能的关系。试验结果表明:在热处理过程中基体组织明显改变,TiC增强相不发生变化。退火处理降低材料的硬度,提高材料的韧性。淬火 低温回火处理使材料的强度和硬度提高,而韧性没有明显的下降。采用等温淬火工艺,可使TiCp/Fe复合材料具有最好的综合力学性能。 相似文献
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Deng-Kui Zhang Guo-Qing Wang Ai-Ping Wu Ji-Guo Shan Yue Zhao Tian-Yi Zhao Dan-Yang Meng Jian-Ling Song Zhong-Ping Zhang 《金属学报(英文版)》2019,32(6):684-694
In as-welded state, each region of 2219 aluminum alloy TIG-welded joint shows diff erent microstructure and microhardness due to the diff erent welding heat cycles and the resulting evolution of second phases. After the post-weld heat treatment, both the amount and the size of the eutectic structure or θ phases decreased. Correspondingly, both the Cu content in α-Al matrix and the microhardness increased to a similar level in each region of the joint, and the tensile strength of the entire joint was greatly improved. Post-weld heat treatment played the role of solid solution strengthening and aging strengthening. After the post-weld heat treatment, the weld performance became similar to other regions, but weld reinforcements lost their reinforcing eff ect on the weld and their existence was more of an adverse eff ect. The joint without weld reinforcements after the post-weld heat treatment had the optimal tensile properties, and the specimens randomly crack in the weld zone. 相似文献
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After nearly two years'tense construction the first phase of industrialized base of Shenyang Research Institute of Foundry 《中国铸造》2008,5(1):63-64
After nearly two years' tense construction, the first phase of industrialized base of Shenyang Research Institute of Foundry (SRIF), located at the Tiexi Casting and Forging Industrial Park in the west of Tiexi District, has now been completed and formally put into operation. 相似文献
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Z. Sun S.L. Zheng Y. Zhang 《金属学报(英文版)》2007,20(3):187-192
Institute of Process Engineering, Chinese Academy of Sciences, China, has proposed a method for oxidative leaching of chromite with potassium hydroxide. Understanding the mechanism of chromite decomposition, especially in the potassium hydroxide fusion, is important for the optimization of the operating parameters of the oxidative leaching process. A traditional thermodynamic method is proposed and the thermal decomposition and the reaction decomposition during the oxidative leaching of chromite with KOH and oxygen is discussed, which suggests that chromite is mainly destroyed by reactions with KOH and oxygen. Meanwhile, equilibrium of the main reactions of the above process was calculated at different temperatures and oxygen partial pressures. The stable zones of productions, namely, K2CrO4 and Fe2O3, increase with the decrease of temperature, which indicates that higher temperature is not beneficial to thermodynamic reactions. In addition, a comparison of the general alkali methods is carried out, and it is concluded that the KOH leaching process is thermodynamically superior to the conventional chromate production process. 相似文献
14.
R. González-Martínez 《金属学报(英文版)》2007,20(4):235-240
The effect of isochronal heat treatments for 1h on variation of damping, hardness and microstructural change of the magnesium wrought alloy AZ61 was investigated. Damping and hardness behaviour could be attributed to the evolution of precipitation process. The influence of precipitation on damping behaviour was explained in the framework of the dislocation string model of Granato and Lücke. 相似文献
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R.Z. Wu Z.K. Qu B.D. Sun D. Shu J. Wang 《金属学报(英文版)》2007,20(3):193-198
The motion of melt droplets in spray degassing process was analyzed theoretically. The height of the treatment tank in spray degassing process could be determined by the results of theoretical calculation of motion of melt droplets. To know whether the melt droplets would solidify during spraying process, the balance temperature of melt droplets was also theoretically analyzed. Then proof experiments for theoretical results about temperature of melt droplets were carried. In comparison, the experimental results were nearly similar to the calculation results. 相似文献
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B.W. Zhang B.W. Li 《金属学报(英文版)》2007,20(2):129-138
On the basis of the single-particle framework, a new theory on inclusion growth in metallurgical melts is developed to study the kinetics of inclusion growth on account of reaction and collision. The studies show that the early growth of inclusion depends on reaction growth and Brawnian motion collision, and where the former is decisive, the late growth depends on turbulence collision and Stokes' collision, and where the former is dominant; collision growth is very quick during the smelting process, lessened in the refining process, but nearly negligible in the continuous casting process. 相似文献
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An approach based on film buckling under simple uniaxial tensile testing was utilized in this paper to quantitatively estimate the interfacial energy of the nanostructured multilayer films(NMFs) adherent to flexible substrates. The interfacial energies of polyimide-supported NMFs are determined to be *5.0 J/m2 for Cu/Cr, *4.1 J/m2 for Cu/Ta,*2.8 J/m2 for Cu/Mo, *1.1 J/m2 for Cu/Nb, and *1.2 J/m2 for Cu/Zr NMFs. Furthermore, a linear relationship between the adhesion energy and the interfacial shear strength is clearly demonstrated for the Cu-based NMFs, which is highly indicative of the applicability and reliability of the modified models. 相似文献
18.
Chen Wang Bei-Bei Wang Dong Wang Peng Xue Quan-Zhao Wang Bo-Lv Xiao Li-Qing Chen Zong-Yi Ma 《金属学报(英文版)》2019,32(6):677-683
A 17 vol% SiCp/Al–Mg–Si–Cu composite plate with a thickness of 3 mm was successfully friction stir welded(FSWed) at a very high welding speed of 2000 mm/min for the first time. Microstructural observation indicated that the coarsening of the precipitates was greatly inhibited in the heat-affected zone of the FSW joint at high welding speed, due to the significantly reduced peak temperature and duration at high temperature. Therefore, prominent enhancement of the hardness was achieved at the lowest hardness zone of the FSW joint at this high welding speed, which was similar to that of the nugget zone. Furthermore, the ultimate tensile strength of the joint was as high as 369 MPa, which was much higher than that obtained at low welding speed of 100 mm/min(298 MPa). This study provides an effective method to weld aluminum matrix composite with superior quality and high welding efficiency. 相似文献
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目的: 观察本实验室合成的一种治疗阿尔茨海默氏症(AD)的药物(1-二甲基磷酰基-2, 2, 2 -三氯)-乙基-1-醇烟酸醋(NMF),对体外培养的皮层神经细胞活性的影响以及对海人藻酸(KA)所致的神经损伤的保护作用。方法: 采用体外培养皮层神经元的方法,解剖分离 15 d胚胎小鼠皮层神经细胞, 接种于 96孔板,48 h 后加药并培养 72 h,以 MIT 法 观察 NMF 对小鼠皮层神经细胞活性的影响;同时将接种于 24 孔板的细胞预先给予 NMF,d 3 时加或不加KA处理后,以台盼蓝染色鉴别并计数死、活细胞,可得出细胞的存活率。结果: NMF 明显促进胎鼠皮层神经元活性,其中 NMF1、0. 1、10nmol·L-1促进神经元活性增殖率分别高达 34.7%、37.4%、36. 7%, NMF 明显促进正常胎鼠皮层神经元存活卒,与对照组比较,10nmol·L-1 NMF 对皮层神经元的存活率分别提高 39.3%、73.5%。 NMF能显著 对抗 KA 所致的神经元损伤,与 KA 损伤组相比, NMF0.1、10、10nmol·L-1对损伤皮层神经元的保护率分别为 77.30%、80.10%、84.15%。结论: NMF 明 显促进胎鼠皮层神经元的洁性、提高正常皮层神经元,的存活卒,并能有效地保护KA所致的神经元损伤,提示 NMF 是一种很有潜力的治疗 AD 的药物。 相似文献
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X.B. Li Y.Q. Xie Y.Z. Nie H.J. Peng H.J. Tao F.X. Yu 《金属学报(英文版)》2007,20(1):27-34
On the basis of energy and shape method for the determination of the valence bond (VB) structures of crystal, the valence bond structure of titanium is redetermined at room temperature and calculated in the whole temperature range of 0-1943K. The outer shell electronic distribution of Ti is e_c~(2.9907) · (s_c~(0.4980) d_c~(2.4927)) ef1.0093 in crystal. The temperature dependences of the VB structures of hcp and bcc phases are the same. The VB structures of hcp and bcc phases monotonically increase or decrease with the increase in temperature, but show discontinuous changes at the phase-transformation temperature 1155K. 相似文献