钒微合金化非调质钢48MnVS的奥氏体动态再结晶行为

实验用非调质钢48MnVS（/%:0.48C,0.60Si,1.50Mn,0.35Cr,0.14V,0.05S,0.020Al,0.0150N）由100t EAF冶炼,连铸成280 mm×360 mm坯,轧成Φ100 mm棒材。通过Gleeble-3800热模拟实验机研究了变形温度950~1150℃,变形速率0.1~10 s^-1,变形量60%的单道次压缩钒微合金非调质钢48MnVS的奥氏体再结晶过程得出真应力-应变曲线,计算得出实验钢的动态再结晶晶粒尺寸模型和动态再结晶状态图。结果表明,钒微合金化非调质钢48MnVS变形温度越高,变形速率越低,则发生动态再结晶的形变储能越小,越容易发生动态再结晶。实验钢48MnVS的动态再结晶激活能为Q_d=343.202 kJ/mol。     

微合金化非调质钢C38N2动态再结晶行为

针对微合金化非调质钢热轧过程的变形特征,通过Gleeble-3800热模拟试验机研究了Nb-Ti-V非调质钢C38N2(/%:0.40C、0.52Si、1.42Mn、0.010P、0.047S、0.028V、0.025 Ti、0.022Nb)在950～1 150℃,变形速率0.1～10 s-1变形量60%,单道次压缩时的奥氏体动态再结晶过程,计算得出C38N2钢的动态再结晶晶粒尺寸模型和动态再结晶状态图。结果表明,C38N2钢变形温度越高,变形速率越低,则发生动态再结晶的储蓄能越小,动态再结晶越易发生。C38N2钢的动态再结晶激活能Q_d=294.905 kJ/mol。     

0.03Nb-0.15Ti微合金化低碳高强度钢的动态再结晶

通过Gleeble 1500热模拟试验机试验研究了Nb-Ti微合金化低碳钢（/%:0.06C,0.22Si,1.80Mn,0.03Nb,0.15Ti,≤0.007N,≤0.002S）10mm带钢在850~1100℃,以应变速率0.1~20.0 s^-1,总变形量75%单道次压缩变形时动态再结晶,由真应力-真应变曲线,结合加工硬化率曲线,得出动态再结晶临界应变0.4~0.7和完全再结晶应变量1.1~1.4。该钢的热变形激活能为618.225 kJ/mol。根据试验结果得到Zener-Hollomon方程和动态再结晶状态图,利用Johnson-Mehl-Avrami（JMA）方程法得到再结晶体积分数实际值,采用Epsilon-P模型对实验数据进行回归,得到试验钢的再结晶动力学模型。     

40Mn2V非调质钢热变形再结晶的研究

采用Gleeble-1500热模拟机测得40Mn2V微合金化非调质钢(%:0.38C、1.48Mn、0.12V)Φ90 mm管坯在800～1 000℃、变形速率0.5～2.0 s^-1时的真应力-应变曲线,并研究了该钢的动态再结晶行为。结果表明,40Mn2V钢的动态再结晶激活能Q_d为382.21 kJ/mol,通过动态再结晶图得出,因子Z＞2.621×10¹⁵时,40Mn2V钢动态再结晶难以完成,当因子Z＞2.014×10¹⁷时,该钢动态再结晶难以发生。     

铌、钒对高强钢筋再结晶影响及轧制工艺设计

 为了研究和设计高强钢筋添加铌、钒后轧制过程中对奥氏体区再结晶行为的量化管控,采用Gleeble-3500热模拟机对铌、钒微合金化高强螺纹钢进行单轴热压缩试验,基于再结晶临界条件的热力学原理,通过对不同形变条件下应力-应变曲线分析,采用Avrami方程得到了不同变形条件下的再结晶动力学曲线,并根据再结晶动力学曲线,量化对比分析了铌、钒微合金化对高强螺纹钢再结晶开始、转变及终了过程的影响。结果表明,铌、钒微合金化螺纹钢的热压缩过程均呈现了明显的动态再结晶特征,由于微合金元素Nb/Nb+V的添加,阻碍了20MnSi钢的动态再结晶,变形温度的提高或应变速率的增加可促进再结晶。针对生产中利用动态再结晶而组织调控进行了工艺设计,精轧机组中成品机架前进行冷却和回复,确保830 ℃左右有利再结晶分数达到95%。     

高强钢筋热压缩过程的本构分析及有限元模拟

为了研究Nb/V微合金化钢筋的热变形行为,采用 Gleeble-3500热模拟机对Nb和Nb/V微合金化的20MnSi钢进行单轴热压缩试验。通过对其不同形变条件(变形温度和应变速率)下的真应力-应变曲线进行分析,建立可以表征20MnSiNb和20MnSiNbV钢应力、应变、应变速率和温度四者关系的本构方程,并将该本构方程应用于有限元分析软件DEFORM 3D的材料模块中,对试验钢的热压缩过程进行数值模拟。结果表明,2种试验钢的热压缩过程均呈现了明显的动态再结晶特征,Nb或Nb/V微合金化均导致20MnSi钢的热变形激活能增加;有限元模拟表明压缩试样存在应变场和温度场分布不均匀现象,其中试样芯部相对于其他区域始终处于高应变、高应变速率和高形变温度的状态。在实际生产和研究中,对试样不同区域组织和性能的预测可参考模拟结果,分别进行探究。     

微合金元素铌对钢动态再结晶的影响

本文研究了A3及18MnNb钢形变奥氏体动态再结晶。在900～1100℃区间进行恒温恒应变压缩形变、在应变速率为3×10~(-3)S~(-1)的条件下,测定了钢的动态再结晶开始时间,绘制A3和18MnNb钢的动态再结晶曲线。文中讨论了铌对动态再结晶的影响。结果表明,微合金元素铌显著推迟钢的动态再结晶。在高温区,这种推迟作用主要是Nb(C,N)的固溶阻滞所至,在较低温度区,则主要是Nb(C,N)的动态析出造成的。     

非调质钢38MnVS奥氏体动态再结晶的研究

研究了V-Ti微合金非调质钢38MnVS（/%:0.42C、0.76Si、1.33Mn、0.011S、0.013P、0.10V、0.02Ti）的奥氏体动态再结晶过程。通过Gleeble-3800热模拟试验机,研究了变形温度（950～1150℃）和变形速率(0.1～10s^-1)对38MnVS钢奥氏体动态再结晶过程的影响,并建立了Zener-Hollomon参数为变量的方程、动态再结晶尺寸模型和动态再结晶状态图。结果表明,变形温度越高,变形速率越低,发生动态再结晶的临界驱动力越小,动态再结晶越易进行;微合金非调质钢38MnVS动态再结晶激活能为Q_d=275.453 kJ/mol。     

含硼微合金钢奥氏体热变形行为

采用单道次压缩实验方法，通过Gleebe-1500热模拟试验机对成分(％)为：0．05C，1．57Mn，0。50Cu，0.05Nb，0．014H，0．0012B微合金化钢进行800～1100℃应力．应变曲线和再结晶组织演变的试验研究，建立了动态再结晶临界应变和晶粒尺寸模型。得出降低变形温度或提高变形速率可明显细化该微合金化钢的晶粒。     

氮含量对1Cr17Mn6Ni5N奥氏体不锈钢高温变形行为的影响

试验用1Cr17Mn6Ni5N钢(/%:0.09~0.11C,0.19~0.29Si,7.33~7.42Mn,0.011~0.015P,0.004~0.007S,16.87~17.24Cr,,5.06~5.19Ni,0.21~0.40N)由10kg真空感应炉熔炼,通过氮气气氛加氮化铬进行N合金化。通过Gleeble-1500D热模拟试验机将实验钢在真空下1150~1 000℃,以应变速率10^-2s^-1和1 s^-1进行压缩60%试验。结果表明,在高温下,以低应变速率压缩时钢的动态再结晶是主要的软化机制;以高应变速率压缩时钢的动态回复是主要的软化机制;与0.21%N和0.29%N试验钢相比,含0.40%N的试验钢具有较高的峰值应力,根据Zener-Hollomon参数的计算得出0.40%N的试验钢再结晶激活能最高,在高温下不易发生动态再结晶。     

Dynamic and Static Recrystallization Behaviour of Coarse-grained Austenite in a Nb-V-Ti Microalloyed Steel简

The dynamic recrystallization （DRX） and static recrystallization （SRX） behaviour of coarse-grained aus- tenite in a Nb-V-Ti microalloyed steel were studied by using a Gleeble thermomechanical simulator. Continuous and interrupted compression tests of coarse-grained austenite were performed in the temperature range of 1000-1 150 ℃ at a strain rate of 0. 1- 5 s 1. The peak and critical strains for the onset of DRX were identified with strain hardening rate analysis, and the ratio of critical strain to peak strain was found to be consistent with the one reported for fine- grained austenite. An equation of the time for 50% softening was proposed by considering the activation energy of steel without microalloying elements and the solute drag effect of microalloying elements. Strain-induced precipitation may not take place at the deformation temperature above 1000 ℃, which indicates that SRX of coarse-grained aus- tenite is mainly retarded by coarse grain size and Nb in solution during rough rolling.     

Recrystailization Behavior of Deformed Austenite in High Strength Microalloyed Pipeline Steel

Using methods of single-hit hot compression and stress relaxation after deformation on a Gleeble 1500D thermomechanical simulator,the curves of flow stress and stress relaxation,the microstructure and the recrystallization behavior of Nb-V-Ti high strength microalloyed low carbon pipeline steel were studied,and the influence of the thermomechanical treatment parameters on dynamic and static recrystallization of the steel was investigated.It was found that microalloying elements improved the deformation activation energy and produced a retardation of the recrystallization due to the solid solution and precipitation pinning.The deformation conditions such as deformation temperature,strain,and strain rate influenced the recrystallization kinetics and the microstructure respectively.Equations obtained can be used to valuate and predict the dynamic and static recrystallizations.     

Recrystallization Behavior of Deformed Austenite in High Strength Microailoyed Pipeline Steel

Using methods of single-hit hot compression and stress relaxation after deformation on a Gleeble 1500D thermomechanical simulator, the curves of flow stress and stress relaxation, the microstructure and the recrystallization behavior of Nb-V-Ti high strength microalloyed low carbon pipeline steel were studied, and the influence of the thermomechanical treatment parameters on dynamic and static recrystallization of the steel was investigated. It was found that microalloying elements improved the deformation activation energy and produced a retardation of the recrystallization due to the solid solution and precipitation pinning. The deformation conditions such as deformation temperature, strain, and strain rate influenced the recrystallization kinetics and the microstructure respectively. Equations obtained can be used to valuate and predict the dynamic and static recrystallizations.     

321奥氏体不锈钢动态再结晶的研究

通过Gleeble-1500热模拟试验机研究了321钢(/%:0.028C、0.69Si、1.21Mn、0.030P、0.001S、17.33Cr、9.19Ni、0.31Ti)单道次高温(900～1 200℃)压缩(0.01～1 s^-1)时的动态再结晶。结果表明,变形温度越高,应变速率越低,321钢的软化作用越强,热变形条件下的真应力-真应变曲线一般没有明显的应力峰值,在应变速率0.01、0.1、1 s^-1时321钢动态再结晶开始发生的温度分别为1 050、1 150、1 150℃;在1 200℃变形时,仍然只发生部分动态再结晶。321钢热变形激活能Q=422.72 kJ/mol,动态再结晶Z参数Z=εexp[422 720/(RT)],临界应变ε_c=0.035 67Z^{0.066 04}。     

Q345GJC高层建筑钢热变形行为及流变应力数学模型研究

利用Gleeble-2000热模拟试验机对Q345GJC钢（/%:0.16C,0.36Si,1.37Mn,0.026Nb）进行了单道次压缩试验,实测了试验钢900～1 150℃、真应变0.8～1.2、应变速率0.1～1 s^-1的变形抗力,分析了各工艺变形参数对试验钢动态再结晶和变形抗力的影响。确定了试验钢的动态再结晶激活能为245.448 kJ/mol（峰态时）和166.994 kJ/mol（稳态时）,并建立了试验钢高温变形抗力的数学模型。该模型具有良好的曲线拟合特性,用该模型计算的结果与实测值吻合较好。