BeO陶瓷干压成型工艺参数的优化

采用干压成型制备BeO陶瓷,通过分析BeO陶瓷的坯体密度和断口形貌,研究加压压力、加压速度、保压时间、粘结剂等工艺参数对BeO陶瓷成型工艺的影响.研究结果表明:干压成型制备BeO陶瓷过程中,加压压力、加压速度、保压时间、粘结剂等工艺参数可以明显影响BeO陶瓷的坯体密度:为得到致密度高、热力学性能优异的BeO陶瓷,必须对加压压力、加压速度、保压时间、粘结剂等工艺参数进行优化;当压力为120 MPa,保压60 S,加入质量分数为1%的PVA作为成型剂压制时能得到致密度较高的BeO陶瓷坯体.     

烧结压力对铜粉放电等离子烧结的影响规律

研究了平均粉末粒度为1μm的铜粉在不同压力条件下的放电等离子烧结过程,系统分析了压坯的密度和微观组织与烧结升温阶段的初始压力和保压压力之间的关系. 结果表明:烧结温度为800℃,初始压力为1MPa,保压压力为50MPa的烧结工艺,可以制备相对密度大于98%,平均晶粒度小于10μm的烧结铜. 同时发现,采用SPS工艺制备的烧结铜沿厚度方向存在不同于传统双向压制的密度分布,SPS烧结铜的表面密度低于心部密度.     

高速压制制备高密度纯铁软磁材料

以退火纯铁粉末为原料,采用粉末退火结合高速压制技术的方法制得高密度压坯(7.70 g·cm-3),经烧结后获得高密度高性能的纯铁软磁材料.研究退火粉末的高速压制行为,以及烧结时间和烧结温度对材料磁性能和晶粒大小的影响.结果显示：退火粉末的压坯密度随压制速度的增加而增加,压坯密度最高可达到7.70 g·cm-3,相对密度可达到98.10%.烧结温度为1450益,烧结时间为4 h时,材料密度达到7.85 g·cm-3,相对密度为99.96%,最大磁导率达到13.60 mH·m-1,饱和磁感应强度为1.87 T,矫顽力为56.50 A·m-1.     

超高压处理对橙汁中过氧化物酶活性的影响

为了推进超高压钝酶技术的工业化进程,以橙汁中的过氧化物酶(POD)为研究对象,通过实验对影响超高压钝酶效果的处理条件(压力、保压时间、pH、温度)进行了考察与评价.在处理温度为室温、保压时间分别为5和20min的条件下,200MPa以下压力范围内POD被激活,其活性随压力的增加出现上升趋势,当压力大于200MPa,随着处理压力增加酶活性下降;压力较高时(500MPa)酶的活性随着保压时间的增加而降低,而在较低的压力(200MPa),其活性随着保压时间的增加而升高;酶活性随pH的增大先上升后下降;随着温度的上升,酶活性降低.实验结果表明,压力、保压时间、pH值、温度是影响超高压钝酶效果的重要因素.     

Al2O3k/Al材料的反重力渗流铸造制备

采用氧化铝空心球作为造孔材料,通过反重力渗流铸造技术制备出基本无宏观铸造缺陷的氧化铝/铝基轻质复合材料(即Al2O3k/Al材料).研究结果表明:渗流长度随熔体温度和空心球预热温度的提高以及空心球粒径的增大而增加,空隙度随着空心球粒径的增大而降低;增加充型与保压压力、延长保压时间以及添加金属Mg等均是改善渗流效果的有效手段.     

Fe_(73.5)Cu_1Nb_3Si_(13.5)B_9非晶合金粉体的SPS烧结特性研究

利用机械合金化和放电等离子烧结技术制备了Fe73.5Cu1Nb3Si13.5B9非晶纳米晶合金块体磁性材料。采用XRD、SEM和DSC分析了Fe73.5Cu1Nb3Si13.5B9合金粉体的相组成、微观形貌和热物性参数;利用Gleeble3500、SEM和VSM分析了烧结温度、升温速率、烧结压力、保温时间和冷却方式等烧结工艺参数对烧结块体抗压强度、压缩断口形貌和磁性的影响。结果表明,烧结温度的升高、烧结压力的增大和冷却速率的增加有利于提高烧结块体的抗压强度;升温速率的增加和保温时间的延长使烧结块体的抗压强度先增高后降低;同时,烧结温度的升高和保温时间的延长使烧结块体的饱和磁化强度增大,矫顽力先降低后增加。     

超细晶粒W-40%Cu合金的烧结和力学性能

以纳米W,Cu粉末为原料,通过测定H2中热压烧结和无压烧结的收缩动力学曲线,研究了纳米W-40%Cu化学混合粉末的致密化过程.对比了纳米W粉与常规Cu粉(-44μm)的机械混合粉和纳米W-Cu化学混合粉的热压烧结致密化过程.测定了烧结合金在300℃和500℃下高温应力一应变曲线.实验结果表明:采用纳米W-40%Cu化学混合粉末在H2中无压烧结时最大收缩速率对应温度为980℃;1 200℃烧结平均晶粒小于2μm,相对密度为97%.纳米W-Cu化学混合粉在H2热压烧结时最大收缩速率对应温度为930℃;1 200℃烧结合金的平均晶粒为0.5 μm,相对密度为98%.纳米W-Cu化学混合粉热压合金高温抗压强度比纳米W与常规Cu粉的热压合金高.     

超声塑化工艺参数对聚合物熔体流动性能的影响

为了测试超声塑化的聚合物熔体流动性能,采用自行研制的阿基米德螺旋模具进行超声塑化微注射成型充填实验,通过充填长度表征聚合物的流动性能。以聚甲基丙烯酸甲酯(PMMA,无定型)、聚丙烯(PP,半结晶型)、聚酰胺66(PA66,结晶型)这3种不同类型的聚合物为对象,采用单因素实验法分别研究超声振幅、塑化时间、塑化压力、保压时间、保压压力、模芯温度等关键工艺参数对聚合物充填长度的影响规律。研究结果表明:提高超声振幅、延长塑化时间、增大塑化压力、提高模芯温度均能显著提高聚合物的流动性能,在相同条件下,这3种聚合物的充填长度L关系为LPA66LPPLPMMA;当保压时间从2s提高到6s时,这3种聚合物充填长度分别提高24.3%,21.1%和24.1%;充填长度与保压压力呈线性增长关系。研究结果可为建立超声塑化的聚合物流动性测试标准提供参考。     

无管式按摩泵泵体注塑成型工艺的稳健设计

为减少无管式按摩泵的翘曲变形量,引入稳健设计方法,使用模流分析软件Moldflow6.1对注塑成型的泵体进行模拟分析.将注塑成型过程中的模具温度(A)、熔体温度(B)、保压压力(C)、保压时间(D)、冷却时间(E)等5个因素作为影响因子,设计了L16(45)正交试验矩阵.通过信噪比分析,得到各工艺参数对泵体翘曲变形的影响程度,获得了最佳工艺参数组合.结果表明:保压压力和保压时间是影响泵体翘曲变形的主要因素,优化后的工艺参数组合为模具温度80℃、熔体温度275℃、保压压力90 MPa、保压时间6 s、冷却时间10 s.优化后泵体的最大翘曲变形量为1.098 mm,变形量减小了12.87%,泵体质量得到了较大的提高.     

退火对表面纳米化纯钛热稳定性的影响

采用表面机械研磨技术实现纯钛材料表面纳米化,并研究了纳米化处理后的材料表层组织结构,详细分析了样品表层纳米晶组织在不同温度、不同时间退火后的热稳定性.结果表明:纯钛TA2经过表面机械研磨处理后可以在表面形成等轴且取向随机的纳米晶层,晶粒尺寸约为12nm.对表面纳米化样品退火后发现,表层纳米晶组织在773 K以下温度退火后具有良好的热稳定性,晶粒尺寸没有明显增大;在773 K温度退火150min后晶粒尺寸稍有增大,而在773 K温度退火240min后晶粒尺寸明显增大,且横截面显微硬度也比表面纳米化后未退火样品显著下降,良好的热稳定性消失.     

Markedness and its Interpretation in Language Use

Language markedness is a common phenomenon in languages, and is reflected from hearing, vision and sense, i.e. the variation in the three aspects such as phonology, morphology and semantics. This paper focuses on the interpretation of markedness in language use following the three perspectives, i.e. pragmatic interpretation, psychological interpretation and cognitive interpretation, with an aim to define the function of markedness.     

Characterization of Ordovician carbonate reservoirs, southeastern Saskatchewan, Canada

The discovery of the prolific Ordovician Red River reservoirs in 1995 in southeastern Saskatchewan was the catalyst for extensive exploration activity which resulted in the discovery of more than 15 new Red River pools. The best yields of Red River production to date have been from dolomite reservoirs. Understanding the processes of dolomitization is, therefore, crucial for the prediction of the connectivity, spatial distribution and heterogeneity of dolomite reservoirs.The Red River reservoirs in the Midale area consist of 3～4 thin dolomitized zones, with a total thickness of about 20 m, which occur at the top of the Yeoman Formation. Two types of replacement dolomite were recognized in the Red River reservoir: dolomitized burrow infills and dolomitized host matrix. The spatial distribution of dolomite suggests that burrowing organisms played an important role in facilitating the fluid flow in the backfilled sediments. This resulted in penecontemporaneous dolomitization of burrow infills by normal seawater. The dolomite in the host matrix is interpreted as having occurred at shallow burial by evaporitic seawater during precipitation of Lake Almar anhydrite that immediately overlies the Yeoman Formation. However, the low δ18O values of dolomited burrow infills (-5.9‰～ -7.8‰, PDB) and matrix dolomites (-6.6‰～ -8.1‰, avg. -7.4‰ PDB) compared to the estimated values for the late Ordovician marine dolomite could be attributed to modification and alteration of dolomite at higher temperatures during deeper burial, which could also be responsible for its 87Sr/86Sr ratios (0.7084～0.7088) that are higher than suggested for the late Ordovician seawaters (0.7078～0.7080). The trace amounts of saddle dolomite cement in the Red River carbonates are probably related to "cannibalization" of earlier replacement dolomite during the chemical compaction.     

Features of Women's language

Language is a means of verbal communication. People use language to communicate with each other. In the society, no two speakers are exactly alike in the way of speaking. Some differences are due to age, gender, statue and personality. Above all, gender is one of the obvious reasons. The writer of this paper tries to describe the features of women＇s language from these perspectives： pronunciation, intonation, diction, subjects, grammar and discourse. From the discussion of the features of women＇s language, more attention should be paid to language use in social context. What＇s more, the linguistic phenomena in a speaking community can be understood more thoroughly.     

A computer generator for randomly layered structures

AcomputergeneratorforrandomlylayeredstructuresYUJia shun1,2,HEZhen hua2(1.TheInstituteofGeologicalandNuclearSciences,NewZealand;2.StateKeyLaboratoryofOilandGasReservoirGeologyandExploitation,ChengduUniversityofTechnology,China)Abstract:Analgorithmisintrod…     

低渗透非均质砂岩油藏启动压力梯度研究

理论推导与室内实验相结合,建立了低渗透非均质砂岩油藏启动压力梯度确定方法。首先借助油藏流场与电场相似的原理,推导了非均质砂岩油藏启动压力梯度计算公式。其次基于稳定流实验方法,建立了非均质砂岩油藏启动压力梯度测试方法。结果表明:低渗透非均质砂岩油藏的启动压力梯度确定遵循两个等效原则。平面非均质油藏的启动压力梯度等于各级渗透率段的启动压力梯度关于长度的加权平均;纵向非均质油藏的启动压力梯度等于各渗透率层的启动压力梯度关于渗透率与渗流面积乘积的加权平均。研究成果可用于有效指导低渗透非均质砂岩油藏的合理井距确定,促进该类油藏的高效开发。     

On Tragic Consciousness In The Works By Ernest Hemingway

As an American modern novelist who were famous in the literary world, Hemingway was not a person who always followed the trend but a sharp observer. At the same time, he was a tragedy maestro, he paid great attention on existence, fate and end-result. The dramatis personae's tragedy of his works was an extreme limit by all means tragedy on the meaning of fearless challenge that failed. The beauty of tragedy was not produced on the destruction of life, but now this kind of value was in the impact activity. They performed for the reader about the tragedy on challenging for the limit and the death.     

海南岛地体及其毗邻陆缘晚中生代—新生代古地磁研究和构造演化

本文叙述了对海南岛及其毗邻大陆边缘白垩纪到第四纪地层岩石进行古地磁研究的全部工作过程。通过分析岩石中剩余磁矢量的磁偏角及磁倾角的变化,提出海南岛白垩纪以来经历的构造演化模式如下:早期伴随顺时针旋转而向南迁移,后期伴随逆时针转动并向北运移。联系该地区及邻区的地质、地球物理资料,对海南岛上述的构造地体运动提出以下认识:北部湾内早期有一拉张作用,主要是该作用使湾内地壳显著伸长减薄,形成北部湾盆地。从而导致了海南岛的早期构造运动,而海南岛后期的构造运动则主要是受南海海底扩张的影响。海南地体运动规律的阐明对于了解北部湾油气盆地的形成演化有重要的理论和实际意义。     

An Index mechanism for multi-scale view in spatial databases

There are numerous geometric objects stored in the spatial databases. An importance function in a spatial database is that users can browse the geometric objects as a map efficiently. Thus the spatial database should display the geometric objects users concern about swiftly onto the display window. This process includes two operations:retrieve data from database and then draw them onto screen. Accordingly, to improve the efficiency, we should try to reduce time of both retrieving object and displaying them. The former can be achieved with the aid of spatial index such as R-tree, the latter require to simplify the objects. Simplification means that objects are shown with sufficient but not with unnecessary detail which depend on the scale of browse. So the major problem is how to retrieve data at different detail level efficiently. This paper introduces the implementation of a multi-scale index in the spatial database SISP (Spatial Information Shared Platform) which is generalized from R-tree. The difference between the generalization and the R-tree lies on two facets: One is that every node and geometric object in the generalization is assigned with a importance value which denote the importance of them, and every vertex in the objects are assigned with a importance value,too. The importance value can be use to decide which data should be retrieve from disk in a query. The other difference is that geometric objects in the generalization are divided into one or more sub-blocks, and vertexes are total ordered by their importance value. With the help of the generalized R-tree, one can easily retrieve data at different detail levels.Some experiments are performed on real-life data to evaluate the performance of solutions that separately use normal spatial index and multi-scale spatial index. The results show that the solution using multi-scale index in SISP is satisfying.     

Jane Eyre——A Feminist In The 19th Century

In the 19th century the society was controlled by men, and women were just appendants of them, they had not any rights and freedom. But Jane was an exception, she showed some characteristics of early feminist. Jane showed her characteristics of feminism in three aspects: rebellion, equality, and independence. These characteristics were helpful to her success, and feminism is the only way out for women of that time.     

《Chinese Science Bulletin》SUBJECT INDEX TO VOLUME 59(2014)

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