| 脱氧胆酸裂口分子的微波合成 |
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| 引用本文： | 陈静,赵志刚,刘兴利,石云.脱氧胆酸裂口分子的微波合成[J].合成化学,2008,16(1):28-32. |
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| 作者姓名： | 陈静 赵志刚 刘兴利 石云 |
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| 作者单位： | 西南民族大学,化学与环境保护工程学院,四川,成都,610041 |
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| 摘 要： | 以固体K2CO3为载体,在微波辐射无溶剂条件下,脱氧胆酸甲酯与芳酰氯反应合成了9个新的脱氧胆酸裂口分子人工受体,其结构经1H NMR,IR,MS及元素分析表征.
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| 关 键 词： | 脱氧胆酸 裂口分子 微波合成 分子识别 |
| 文章编号： | 1005-1511（2008）01-0028-05 |
| 收稿时间： | 2007-10-29 |
| 修稿时间： | 2007年10月29 |
Synthesis of Molecular Clefts Based on Deoxycholic Acid under Microwave Irradiation |
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| CHEN Jing,ZHAO Zhi-gang,LIU Xing-li,SHI Yun.Synthesis of Molecular Clefts Based on Deoxycholic Acid under Microwave Irradiation[J].Chinese Journal of Synthetic Chemistry,2008,16(1):28-32. |
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| Authors: | CHEN Jing ZHAO Zhi-gang LIU Xing-li SHI Yun |
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| Abstract: | Nine new molecular clefts based on deoxycholic acid were synthesized by the reaction of methyl deoxycholate with aroyl chloride using solid K2CO3 as a supporter in solvent-free under microwave irradiation. The structures were characterized by ^1H NMR, IR, MS and elemental analysis. |
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| Keywords: | deoxycholic acid molecular clefts microwave synthesis molecular recognition |
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