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水热法KTP晶体生长与宏观缺陷研究
引用本文:阮青锋,霍汉德,覃西杰,卢福华,周卫宁,张昌龙,邱志惠,雷威,张良钜.水热法KTP晶体生长与宏观缺陷研究[J].人工晶体学报,2006,35(3):608-611.
作者姓名:阮青锋  霍汉德  覃西杰  卢福华  周卫宁  张昌龙  邱志惠  雷威  张良钜
作者单位:桂林工学院资源与环境工程系,桂林,541004;桂林地质矿产研究院,桂林,541004;广西师范大学化学化工学院,桂林,541004
基金项目:国家自然科学基金;广西青年科学基金;广西科技能力建设基金;广西科学基金
摘    要:本文报道了水热法KTP晶体的生长工艺及晶体生长形态,系统研究了水热法KTP晶体的宏观缺陷,其宏观缺陷主要为添晶、生长脊线、裂隙和包裹体.提出了晶体生长工艺的改进措施,如提高原材料和试剂的纯度、调整籽晶的悬挂方式、减少籽晶的尺寸等,都可以减少晶体的宏观缺陷,提高晶体的质量.//(011)切向的籽晶生长的晶体质量较高,且能很好地应用于激光器件中.

关 键 词:磷酸钛氧钾  KTP晶体  水热法  晶体形态  宏观缺陷  
文章编号:1000-985X(2006)03-0608-04
收稿时间:09 7 2005 12:00AM
修稿时间:2005-09-07

Study on the Growth and Defects of Hydrothermal KTP Crystal
RUAN Qing-feng,HUO Han-de,QIN Xi-jie,LU Fu-hua,ZHOU Wei-ning,ZHANG Chang-long,QIU Zhi-hui,LEI Wei,ZHANG Liang-ju.Study on the Growth and Defects of Hydrothermal KTP Crystal[J].Journal of Synthetic Crystals,2006,35(3):608-611.
Authors:RUAN Qing-feng  HUO Han-de  QIN Xi-jie  LU Fu-hua  ZHOU Wei-ning  ZHANG Chang-long  QIU Zhi-hui  LEI Wei  ZHANG Liang-ju
Affiliation:1. Department of Resources and Environmental Engineering, Guilin University of Technology, Guilin 541004, China; 2. Guilin Research Institute of Geology for Mineral Resources, Gnilin 541004, China; 3. School of Chemistry and Chemical Engineering, Guangxi Normal University, Guilin 541004, China
Abstract:The growth procedure and crystal form of hydrothermal KTP are reported in this article.Some defects in the hydrothermally grown KTP crystal were researched.The macroscopic defects of hydrothermal KTP crystal are mainly twin and coalescence crystal,growth spine,cracks and inclusions.The causes were also discussed. Some suggestions on improving the techniques of the crystal growth of KTP crystal are given at the end of this article to improve the quality of the grown crystals,such as promoting the purity of materials and reagents,minimizing the dimensions of seed crystals and choosing the hang direction of seed crystals,and so on.Parallel to(011) seed crystals can grow pure KTP crystals,and these crystals have a high efficient in the laser device.
Keywords:potassium titanium phosphate  KTP crystal  hydrothermal method  crystal morphology  macroscopic defect
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