| 4-溴甲基-5-甲基-1,3-二氧杂环戊烯-2-酮的合成研究 |
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| 引用本文： | 何人宝,王莺妹,金逸中,俞传明.4-溴甲基-5-甲基-1,3-二氧杂环戊烯-2-酮的合成研究[J].浙江化工,2011,42(7):5-7. |
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| 作者姓名： | 何人宝 王莺妹 金逸中 俞传明 |
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| 作者单位： | 1. 浙江永太科技股份有限公司,浙江临海,317016
2. 浙江工业大学,浙江杭州,310014 |
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| 基金项目： | 浙江省科技厅科技计划项目 |
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| 摘 要： | 以4,5-二甲基-1,3-二氧杂环戊烯-2-酮（DMDO）为原料,经溴化反应得4-溴甲基-5-甲基-1,3-二氧杂环戊烯-2-酮（DMDO-Br）,对反应的条件做了研究。对目标产物的结构进行核磁及质谱的表征。
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| 关 键 词： | 4-溴甲基-5-甲基-1 3-二氧杂环戊烯-2-酮 中间体 合成 |
Synthesis of 4-Bromomethyl-5-methyl-1,3-dioxol-2-one |
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| HE Ren-bao,WANG Ying-mei,JIN Yi-zhong,YU Chuan-ming.Synthesis of 4-Bromomethyl-5-methyl-1,3-dioxol-2-one[J].Zhejiang Chemical Industry,2011,42(7):5-7. |
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| Authors: | HE Ren-bao WANG Ying-mei JIN Yi-zhong YU Chuan-ming |
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| Affiliation: | HE Ren-bao1,WANG Ying-mei1,JIN Yi-zhong1,YU Chuan-ming2(1.Zhejiang Yongtai Technology Co.,Ltd.,Linhai,Zhejiang 317016,China,2.Zhejiang University of Technology,Hangzhou,Zhejiang 310014,China) |
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| Abstract: | The reaction of DMDO with bromine under UV irradiation condition to form DMDO-Br was investigated,some reaction conditions were studied,and target compound was confirmed by 1HMNR and MS. |
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| Keywords: | synthesis DMDO-Br intermediate |
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