Preconcentration of Polycyclic Aromatic Hydrocarbons on Polyurethane Foams and Their Determination in Waters with the Use of Luminescence and High-Performance Liquid Chromatography |
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Authors: | S. G. Dmitrienko E. N. Shapovalova E. Ya. Gurarii M. V. Kochetova O. A. Shpigun Yu. A. Zolotov |
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Affiliation: | (1) Department of Chemistry, Moscow State University, Vorob'evy gory, Moscow, 119992, Russia |
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Abstract: | A technique was developed for the sorption preconcentration of polycyclic aromatic hydrocarbons on polyurethane foams in the batch and dynamic modes providing their simultaneous quantitative extraction. A procedure was proposed for screening waters for polycyclic aromatic hydrocarbons based on the preconcentration of these compounds with polyurethane foam, determination of their total amount by the luminescence method, desorption of adsorbed compounds with acetonitrile, and determination of individual compounds in the eluate by high-performance liquid chromatography with fluorescence detection. The procedure was tested with model and real samples of water. |
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