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V型直链淀粉-正己醇复合物制备工艺的研究
引用本文:刘延奇,肖欣欣,李红,李学红,杨留枝.V型直链淀粉-正己醇复合物制备工艺的研究[J].食品科技,2012(5):254-257.
作者姓名:刘延奇  肖欣欣  李红  李学红  杨留枝
作者单位:郑州轻工业学院食品与生物工程学院
基金项目:国家自然科学基金项目(21076201);河南省重点科技攻关项目(102102110103)
摘    要:以B型微晶淀粉为原料、正己醇为配体,采用非水溶剂法制备得到了V型直链淀粉-正己醇复合物。研究了反应温度、滴加时间和冷却温度等对V型复合物结晶度的影响。通过单因素及正交试验得到最佳工艺条件为:反应温度为70℃、滴加速率为2mL/min、室温冷却制备条件,此时所得到的V型复合物的结晶度为70.7%,且具有优异的结晶性。

关 键 词:B型微晶淀粉  正己醇  V型直链淀粉-正己醇复合物  结晶度

Analysis of preparation of V-type amylose-hexanol complex
LIU Yan-qi, XIAO Xin-xin, LI Hong, LI Xue-hong, YANG Liu-zhi.Analysis of preparation of V-type amylose-hexanol complex[J].Food Science and Technology,2012(5):254-257.
Authors:LIU Yan-qi  XIAO Xin-xin  LI Hong  LI Xue-hong  YANG Liu-zhi
Affiliation:(School of Food and Biological Engineering,Zhengzhou University of Light Industry,Zhengzhou 450002)
Abstract:By means of non-aqueous solvent,V-type amylose-hexanol complex which B-type microcrystalline starch made a combination with hexanol was prepared.Study the influence of the reaction temperature,dropping time and cooling temperature on the V-type complexes’ crystallinity.The optimal synthetic conditions were found through the single and orthogonal experiment as follows:reaction temperature at 70 ℃,dropping rate 2 mL/min,cooling to room temperature.V-type complex was prepared under optimum conditions,the crystallinity reached 72.07%.
Keywords:B-type microcrystalline starch  hexanol  V-type amylose-hexanol complex  crystallinity
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