| SnO_2-SBA-15介孔分子筛的制备与表征 |
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| 作者单位： | ;1.平顶山学院化学与环境工程学院;2.叶县教育体育局教育技术装备站 |
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| 摘 要： | 首先以P123、正硅酸乙酯为原料合成了SBA-15介孔分子筛,然后利用氯化亚锡的水解反应在SBA-15介孔分子筛表面及孔道内部沉积纳米SnO_2,对其进一步功能化,成功制备出了SnO_2-SBA-15介孔分子筛.采用多晶X射线衍射(XRD)、傅里叶变换红外光谱分析、同步热分析、氮气吸脱附等技术手段对材料的结构组成进行了表征,结果表明纳米二氧化锡成功负载到了SBA-15介孔分子筛表面和孔道内部.
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| 关 键 词： | SBA-15 SnO_2-SBA-15 介孔分子筛 功能化 |
Preparation and Characterization of SnO_2-SBA-15 Mesoporous Molecular Sieves |
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| Affiliation: | ,School of Chemistry and Environmental Engineering,Pingdingshan University,Educational Technology and Equipment Station,Yexian Education and Sports Bureau |
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| Abstract: | In this study,SBA-15 mesoporous molecular sieves are prepared by using P123 and tetraethyl orthosilicate as raw materials. Then,nano-SnO_2 is deposited on the surface and pore canal of SBA-15 mesoporous molecular sieve by in-situ synthesis from the hydrolysis of stannous chloride. The synthesized materials are characterized by XRD,FTIR,TG,BET and N_2-adsorption-desorption. The results show that nano-SnO_2 is successfully loaded onto the surface and inside the hole of the SBA-15 mesoporous molecular sieve. |
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| Keywords: | SBA-15 SnO_2-SBA-15 mesoporous molecular sieve functionalize |
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