Hydrothermal synthesis and characterization of CsNiP and 2(LiZnHP2O7) crystals |
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| Authors: | G S Gopalakrshna M J Mahesh S P Madhu K G Ashamanjari M A Shridhara S Prasad |
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| Affiliation: | (1) Department of Studies in Geology, University of Mysore, Manasagangotri, Mysore, 570 006, India;(2) Department of Studies in Physics, University of Mysore, Manasagangotri, Mysore, 570 006, India |
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| Abstract: | CsNiP and 2(LiZnHP2O7) crystals were synthesized by hydrothermal technique at moderate P-T conditions. Solubility results of both the compound
shown positive thermal coefficient and single crystal X-ray studies revealed, CsNiP crystallized in hexagonal system with
cell parameters; a = 7.173(2), c = 5.944(9) Å, V = 264.87(7) Å3 and space group P63/mmc and 2(LiZnHP2O7) crystallized in orthorhombic system with cell parameters; a = 12.3636 Å, b = 27.5330 Å, c = 6.8647 Å and space group, Pca21 exhibiting ring type of cavities with open aperture in the structure. CsNiP is a frequency
dependent paramagnetic and 2(LiZnHP2O7) is a diamagnetic. |
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