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甲基苯基硅树脂及其复合材料的性能研究
引用本文:马悦欣,刘坤,周楠.甲基苯基硅树脂及其复合材料的性能研究[J].化学与粘合,2007,29(6):390-394,407.
作者姓名:马悦欣  刘坤  周楠
作者单位:哈尔滨工业大学,哈尔滨工业大学,哈尔滨工业大学 黑龙江 哈尔滨150001,黑龙江 哈尔滨150001,黑龙江 哈尔滨150001
摘    要:以甲基和苯基氯硅烷为单体,采用水解缩聚的方法合成有机硅树脂.对有机硅树脂的凝胶特性及黏度特征等物理性能进行了研究,结果表明甲基苯基硅树脂可以用作复合材料基体树脂使用.通过热失重法、热失重微分曲线法及恒温热失重法对硅树脂的热性能进行研究,发现甲基苯基硅树脂具有优异的耐热性能.对以甲基苯基硅树脂为基体,制备的玻璃纤维复合材料进行弯曲强度测试和层间剪切强度测试,结果表明,玻璃纤维/甲基苯基硅树脂复合材料具有较好的力学性能.

关 键 词:甲基苯基硅树脂  有机硅树脂  耐热性  复合材料  甲基苯基硅树脂  树脂复合材料  力学性能  研究  Composite  Material  Silicone  Methyl  Performance  玻璃纤维  层间剪切  强度测试  弯曲  纤维复合材料  基体树脂  耐热性能  发现  恒温  曲线法  微分  热失重法
文章编号:1001-0017(2007)06-0390-06
收稿时间:2007-08-13
修稿时间:2007-08-13

Research on the Performance of Methyl Phenyl Silicone and Its Composite Material
MA Yue-xin,LIU Kun,ZHOU Nan.Research on the Performance of Methyl Phenyl Silicone and Its Composite Material[J].Chemistry and Adhesion,2007,29(6):390-394,407.
Authors:MA Yue-xin  LIU Kun  ZHOU Nan
Affiliation:Harbin Institute of Technology, Harbin 150001, China
Abstract:The silicone resin is synthesized with hydrolysis-polycondensation method from phenyl and methyl ehlorosilane,and the studies on the gel properties and viscosity of silicone resin are carried out.The result shows that the methyl phenyl silicone can be used as matrix resins for composite ma- terial.It is found that the silicone resin has excellent thermal stability by using thermo-gravimetrie analysis (TG),differential thermo-gravimetric anal- ysis (DTG)and isothermal TG.The shear and bending tests of glass fiber composite material prepared with methyl phenyl silicone as matrix are carried out,and the result shows that the glass fiber/methyl phenyl silicone composite materials have better mechanical properties.
Keywords:Methyl phenyl silicone  silicone resin  heat resistance  composite material
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