| SnO2-Cu2O/CNTs复合催化剂的制备及对FOX-12热分解的催化性能 |
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| 引用本文： | 张金霞,洪伟良,赵凤起,刘剑洪,田德余,朱秀英,马永强. SnO2-Cu2O/CNTs复合催化剂的制备及对FOX-12热分解的催化性能[J]. 火炸药学报, 2011, 34(2): 47-51 |
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| 作者姓名： | 张金霞 洪伟良 赵凤起 刘剑洪 田德余 朱秀英 马永强 |
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| 作者单位： | 1. 深圳大学化学与化工学院,广东,深圳,518060
2. 西安近代化学研究所,陕西,西安,710065 |
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| 基金项目： | 国防重点实验室基金项目(9140C3503020605) |
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| 摘 要： | 以氯化铜、四氯化锡和碳纳米管为原料,采用浸渍法和液相化学沉积法相结合制得SnO2-Cu2O/CNTs复合催化剂,采用XRD、SEM、TEM、EDS等对催化剂进行表征,并用DsC研究催化剂对FOX-12热分解特性的影响.结果表明,纳米金属氧化物以5～10nm的球形颗粒形态附着在碳纳米管表面,分散较均匀.催化剂使N-脒基脲...
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| 关 键 词： | 分析化学 复合催化剂 碳纳米管 二氧化锡 FOX-12 热分解 |
Synthesis of SnO_2-Cu_2O/CNTs Catalyst and Its Catalytic Effect on Thermal Decomposition of FOX-12 |
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| ZHANG Jin-xia,HONG Wei-liang,ZHAO Feng-qi,LIU Jian-hong,TIAN De-yu,ZHU Xiu-ying,MA Yong-qiang. Synthesis of SnO_2-Cu_2O/CNTs Catalyst and Its Catalytic Effect on Thermal Decomposition of FOX-12[J]. Chinese Journal of Explosives & Propellants, 2011, 34(2): 47-51 |
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| Authors: | ZHANG Jin-xia HONG Wei-liang ZHAO Feng-qi LIU Jian-hong TIAN De-yu ZHU Xiu-ying MA Yong-qiang |
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| Affiliation: | 1(1.College of Chemistry and Chemical Engineering,Shenzhen University,Shenzhen 518060,China;2.Xi′an Modern Chemistry Research Institute,Xi′an 710065,China) |
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| Abstract: | SnO2-Cu2O/CNTs composite catalyst was prepared by integrate infusioning method with liquid phase deposition method under normal temperature and normal pressure using copper chloride dihydrate,stannic tetrachloride pentahydrate,and carbon nanotubes as the reactant.The catalyst was characterized with XRD,SEM,TEM and EDS.The catalytic effects of catalyst on the thermal decomposition of FOX-12 were investigated by DSC.The test result showed that SnO2 and Cu2O nanoparticles were attached on carbon nanotubes thro... |
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| Keywords: | analytical chemistry composite catalyst carbon nanotubes cuprous oxide FOX-12 thermal decomposition |
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