| 洁阴灵洗液质量标准研究 |
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| 引用本文： | 高淑丽,王明霞,侯娟,李伟.洁阴灵洗液质量标准研究[J].中国药房,2007,18(15):1157-1158. |
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| 作者姓名： | 高淑丽 王明霞 侯娟 李伟 |
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| 作者单位： | 1. 河北医科大学第四医院,石家庄市,050011;石家庄市第四医院,石家庄市,050011
2. 河北医科大学第四医院,石家庄市,050011 |
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| 摘 要： | 目的:建立洁阴灵洗液的质量标准。方法:采用TLC法鉴别黄柏和淫羊藿,以HPLC法测定淫羊藿苷的含量。结果:薄层斑点清晰,重现性好。淫羊藿苷进样量为2.0~10.0μg时与峰面积积分值呈良好线性关系(r=0.9996);平均回收率为100.1%,RSD=1.92%。结论:所建标准准确、可靠,可用于本品的质量控制。
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| 关 键 词： | 薄层色谱法 高效液相色谱法 淫羊藿苷 洁阴灵洗液 |
| 文章编号： | 1001-0408(2007)15-1157-02 |
| 收稿时间： | 10 28 2006 12:00AM |
| 修稿时间： | 02 25 2007 12:00AM |
Quality Standard Study on Jieyinling Lotion |
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| GAO Shuli,WANG Mingxia,HOU Juan,LI Wei.Quality Standard Study on Jieyinling Lotion[J].China Pharmacy,2007,18(15):1157-1158. |
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| Authors: | GAO Shuli WANG Mingxia HOU Juan LI Wei |
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| Affiliation: | 1.The Fourth Hospital of Hebei Medical University, azhuang 050011, China;2.Shijiazhuang Municipal No. 4 Hospital, Shijiazhuang 050011, China |
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| Abstract: | OBJECTIVE: To establish a quality standard for Jieyinling lotion. METHODS: Cortex Phellodendri and Epimedium Herb were identified by TLC, and the content of Icariin was determined by HPLC. RESULTS: The TLC spots were fairly clear and a good reproducibility was obtained. The linear range of Icariin was 2.0 ～10.0μg(r=0.999 6),with average recovery at 100.1%,RSD =1.92%. CONCLUSION: The established method is reliable and accurate, and suitable for the quality control of Jieyinling lotion. |
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| Keywords: | TLC HPLC Icariin Jieyinling lotion |
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