| 微波促进下无溶剂一锅法合成含氟喹唑啉-4(3H)-酮类化合物 |
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| 引用本文： | 商文丽,章建民,金见安,陈晓蕾.微波促进下无溶剂一锅法合成含氟喹唑啉-4(3H)-酮类化合物[J].有机化学,2011,31(8). |
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| 作者姓名： | 商文丽 章建民 金见安 陈晓蕾 |
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| 作者单位： | 上海大学理学院化学系 上海200444 |
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| 基金项目： | 国家自然科学基金(No.20972092)资助项目 |
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| 摘 要： | 采用邻胺基苯甲酸、原甲酸三乙酯及含氟苯胺为原料,在微波促进下,无溶剂一锅法高效合成了系列3-氟苯基-喹唑啉-4(3H)-酮类化合物,同时测试了新化合物的荧光性能,并与不含氟同类化合物的荧光发射光谱进行了比较.
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| 关 键 词： | 含氟喹唑啉酮 微波促进 一锅法 无溶剂法 荧光发射光谱 |
One-Pot Preparation of Fluorinated 4(3H)-Quinazolinones under Microwave Irradiation and Solvent-Free Conditions |
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| Shang Wenli,Zhang Jianmin,Jin Jianan,Chen Xiaolei.One-Pot Preparation of Fluorinated 4(3H)-Quinazolinones under Microwave Irradiation and Solvent-Free Conditions[J].Chinese Journal of Organic Chemistry,2011,31(8). |
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| Authors: | Shang Wenli Zhang Jianmin Jin Jianan Chen Xiaolei |
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| Affiliation: | Shang,Wenli Zhang,Jianmin* Jin,Jianan Chen,Xiaolei(Department of Chemistry,School of Science,Shanghai University,Shanghai 200444) |
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| Abstract: | A facile one-pot method has been developed for the synthesis of fluorine-containing 4(3H)-quinazolinones by a three-component coupling of anthranilic acid,triethyl orthoformate and fluorinated anilines under microwave irradiation and solvent-free conditions.All new compounds are fully characterized by spectral methods,especially,fluorescence. |
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| Keywords: | fluorinated 4(3H)-quinazolinones microwave one-pot reaction solvent free fluorescence emission spectrum |
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