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蒸馏-萃取法与溶剂萃取法提取杏果实香气成分的比较
引用本文:陈美霞,陈学森,周杰.蒸馏-萃取法与溶剂萃取法提取杏果实香气成分的比较[J].分析试验室,2005,24(3):65-70.
作者姓名:陈美霞  陈学森  周杰
作者单位:山东农业大学果树生物学实验室,泰安,271018;山东农业大学化学与材料学院,泰安,271018
基金项目:科技部农业科技成果转化基金;山东省农业良种产业化工程项目
摘    要:采用水蒸气蒸馏一萃取法和溶剂萃取法提取杏果香成分,用气相色谱一质谱联用测定其化学成分和质量分数,并对两种提取方法进行了比较。水蒸气蒸馏一萃取法提取的杏果香成分是74种,占总峰面积的73.604%;溶剂萃取法提取的杏果香成分是32种,占总峰面积的44.677%,两者相同的成分有21种。溶剂萃取法提取的主要是烷烃类化合物,水蒸气蒸馏萃取法提取的主要化合物为G醛类、C6醇类、内酯类、萜烯醇类、酮类、烷烃类等。结果表明:水蒸气蒸馏-萃取法能较好地提取杏果实香气成分。

关 键 词:  果实  香气成分  蒸馏-萃取  溶剂萃取  气相色谱-质谱
文章编号:1000-0720(2005)03-0065-06

Comparison of aroma components from apricot fruit obtained by steam distillation-extraction and solvent extraction
CHEN Mei-xia,CHEN Xue-sen,ZHOU jie.Comparison of aroma components from apricot fruit obtained by steam distillation-extraction and solvent extraction[J].Chinese Journal of Analysis Laboratory,2005,24(3):65-70.
Authors:CHEN Mei-xia  CHEN Xue-sen  ZHOU jie
Abstract:The aroma components which present in apricot fruit were focused on, meanwhile two methods for extracting aroma components were compared. The fruit was sampled by steam distillation-extraction and solvent extraction. The concentrated extracts were analyzed by capillary gas chromatography-mass spectrometry. A total of 74 components were identified by steam distillation-extraction, representing 73.604% of the total peak area and 32 components by solvent extraction, representing 44.677% of the total peak area. There were 21 common components in two extracts. C_6 aldehydes, C_6 alcohols, lactones, terpenic alcohols, ketones and hydrocarbons were the major constituents by steam distillation-extraction, meanwhile hydrocarbons were the dominant constituents in the solvent extraction samples. The results indicated that the steam distillation-extraction was a better method for extracting aroma components from apricot fruit.
Keywords:Apricot  Fruit  Aroma component  Steam distillation-extraction  Solvent extraction  Gas chromatography-mass spectrometry
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