| 高效液相色谱法测定护肝颗粒中芍药甙的含量 |
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| 引用本文： | 何勤 张志荣. 高效液相色谱法测定护肝颗粒中芍药甙的含量[J]. 华西药学杂志, 1996, 11(4): 243-245 |
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| 作者姓名： | 何勤 张志荣 |
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| 作者单位： | 华西医科大学药学院 |
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| 摘 要： | 用ＨＰＬＣ法测定了护肝颗粒中芍药甙的含量，其分析柱为ＯＤＳ－Ｃ_(１８)，流动相为甲醇－异丙醇－醋酸（３６％）－水（２５：２：２：７１），检测波长为２３０ｎｍ，样品提取溶剂为水，提取方法和时间为超声振荡１０ｍｉｎ。芍药甙的平均回收率为９７．４４％，ＲＳＤ＝０．６１％（ｎ＝６）．线性范围０．２０８～０．８５２μｇ。方法简便、快速，精密度和稳定性良好，适于护肝颗粒生产的质量控制。
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| 关 键 词： | 芍药甙 高效液相色谱 肝颗粒 |
DETERMINATION OF PAEONILORIN IN HUGAN PARTICLES BY HPLC |
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| He Qin,Zhang Zhirong. DETERMINATION OF PAEONILORIN IN HUGAN PARTICLES BY HPLC[J]. West China Journal of Pharmaceutical Sciences, 1996, 11(4): 243-245 |
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| Authors: | He Qin Zhang Zhirong |
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| Abstract: | The paeonilorin in Hugan particles was determined by HPLC,the mobile phase consisted of ethanol-isopropnolacetic acid-water(25:2:2:71)), the ODS-C18 column was used as analytical column.The standard curve of paeonilorin was A=5653 +563270X(r=0.9997),recovery was 97. 94%(RSD =0.61%,n =6),The HPLC to be adopted in this paper could be used for quality control in the production of Hugan preparations. |
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| Keywords: | HPLC Paeonilorin |
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