Keggin Heteropolyacid Catalyzed Synthesis of Isoxazolo[5,4-d]pyrimidine-4,6(5H,7H)-diones at Room Temperature |
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Authors: | Bamoharram Fatemeh F Roshani Mina Heravi Majid M Mahdavi Masoumeh Javid Ali Emampour Jalal Sh |
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Affiliation: | Bamoharram1 Fatemeh F,Roshani Mina,Heravi Majid M,Mahdavi Masoumeh,Javid Ali,Emampour Jalal Sh |
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Abstract: | Isoxazolo[5,4‐d]pyrimidine‐4,6(5H,7H)diones 2a – 2f have been synthesized from the reaction of ethyl 5‐amino‐3‐methyl‐4‐isoxazole carboxylate ( 1 ) with aryl isocyanates in the presence of Keggin heteropolyacid H3[PW12O40] as a green solid acid catalyst at room temperature in a one‐pot process in good yields. |
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Keywords: | isoxazolopyrimidine cyclization heteropolyacid Keggin catalyst |
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