| 2,6-二甲基-4-氨基吡啶的合成研究和表征 |
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| 引用本文： | 刘世普,张婷,赵明,刘骏腾. 2,6-二甲基-4-氨基吡啶的合成研究和表征[J]. 河北化工, 2011, 34(2): 22-23,49 |
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| 作者姓名： | 刘世普 张婷 赵明 刘骏腾 |
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| 作者单位： | 1. 冀州市宏泰医药科技有限公司,河北,衡水,053200
2. 河北省混凝土外加剂厂,河北,石家庄,050031 |
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| 摘 要： | 2,6-二甲基吡啶为重要的吡啶类起始原料。以2,6-二甲基吡啶为起始原料,经双氧水氧化、混酸硝化、Pd/C-H2还原的方法制备2,6-二甲基-4-氨基吡啶,该合成工艺适合工业化生产。
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| 关 键 词： | 2,6-二甲基吡啶 2,6-二甲基-4-氨基吡啶 氧化 硝化 还原 |
Synthesis and Characterization of 2,6-Dimethyl-4-aminopyridine |
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| LIU Shi-pu,ZHANG Ting,ZHAO Ming,LIU Jun-teng. Synthesis and Characterization of 2,6-Dimethyl-4-aminopyridine[J]. Hebei Chemical Engineering and Industry, 2011, 34(2): 22-23,49 |
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| Authors: | LIU Shi-pu ZHANG Ting ZHAO Ming LIU Jun-teng |
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| Affiliation: | 1(1.Jizhou Hongtai Pharmaceutical Technology Co.,Ltd,Hengshui 053200,China;2.Concrete Admixture Plant of Hebei Province,Shijiazhuang 050031,China) |
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| Abstract: | 2,6-Dimethylpyridine is an important starting material.To prepare 2,6-dimethyl-4-aminopyridine with 2,6-dimethylpyridine as the starting material and by the hydrogen peroxide oxidation,mixed acid nitration,Pd/C-H2 reduction.The synthetic process is suitable for industrial production. |
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| Keywords: | 2,6-dimethylpyridine 2,6-dimethyl-4-aminopyridine oxidation nitration reduction |
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