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| 刺状鱼栖苔化学成分研究 | |
| 引用本文： | 史大永,韩丽君,孙杰,袁兆慧,杨永春,石建功,范 晓. 刺状鱼栖苔化学成分研究[J]. 中国中药杂志, 2007, 32(11): 1035-1037 |
| 作者姓名： | 史大永 韩丽君 孙杰 袁兆慧 杨永春 石建功 范 晓 |
| 作者单位： | 1. 中国科学院,海洋研究所,山东,青岛,266071;中国科学院,研究生院,北京,100039 2. 中国科学院,海洋研究所,山东,青岛,266071 3. 中国医学科学院,中国协和医科大学,药物研究所,北京,100050 |
| 基金项目： | 国家高技术研究发展计划(863计划);中国科学院知识创新工程项目 |
| 摘 要： | 目的：研究红藻刺状鱼栖苔Acantophora spicifera化学成分。方法：利用正相和反相色谱,Sephadex LH-20色谱以及反相HPLC等手段进行分离纯化,应用MS,IR和1D,2D-NMR等方法鉴定结构。结果：从穗状鱼栖苔中分离鉴定了6个化合物,分别为aplysin(1),loloilide(2),(R)-(-)-dehydrovomifoliol(3),尿嘧啶(4),胸腺嘧啶(5),1-methoxy-4-(1-propenyl)benzene(6)。结论：所有化合物均为首次从本属海藻中分离得到,其中化合物6为首次从海洋生物中分离得到。 |
| 关 键 词： | 红藻 刺状鱼栖苔 化学成分 |
| 文章编号： | 1001-5302（2007）11-1035-03 |
| 收稿时间： | 2006-11-07 |
| 修稿时间： | 2006-11-07 |
Studies on chemical constitutes of Acantophora spicifera |
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| SHI Da-yong;; HAN Li-jun; SUN Jie;; YUAN Zhao-hui;; YANG Yong-chun; SHI Jian-gong; FAN Xiao. Studies on chemical constitutes of Acantophora spicifera[J]. China Journal of Chinese Materia Medica, 2007, 32(11): 1035-1037 | |
| Authors: | SHI Da-yong HAN Li-jun SUN Jie YUAN Zhao-hui YANG Yong-chun SHI Jian-gong FAN Xiao |
| Affiliation: | 1. Institute of Oceanology, Chinese Academy of Sciences, Qingdao 266071, China;2. Institute of Materia Medica, Chinese Academy of Medical Sciences and Peking Union Medical College, Beijing 100050, China; 3. Graduate School of the Chinese Academy of Sciences, Beijing 100039, China |
| Abstract: | Objective: To study the chemical constitutes of Acantophora spicifera. Method: Compounds were isolated by normal phase silica gel and Sephadex LH-20 gel column chromatography, and reverse-phase HPLC, as well as recrystallization. Their structures were elucidated by spectroscopic methods. Result: Seven compounds were isolated from A. spicifera and their structures were identified as aplysin (1), loloilide (2), (R)-(-)-dehydrovomifoliol (3), uracil (4), thymine (5), 1-methoxy-4-(1-propenyl)benzene (6). Conclusion: The compounds were obtained from this genus for the first time. Compound 6 was firstly obtained from marine organisms. |
| Keywords: | red alga Acantophora spicifera chemical constitutes |
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