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Al_2O_3/MoS_2复合涂层的制备及摩擦磨损性能
引用本文:邓雯,赵晓琴,李双建,安宇龙,周惠娣,陈建敏.Al_2O_3/MoS_2复合涂层的制备及摩擦磨损性能[J].中国表面工程,2017,30(5):110-118.
作者姓名:邓雯  赵晓琴  李双建  安宇龙  周惠娣  陈建敏
作者单位:中国科学院兰州化学物理研究所 固体润滑国家重点实验室, 兰州 730000;中国科学院 研究生院, 北京 100049,中国科学院兰州化学物理研究所 固体润滑国家重点实验室, 兰州 730000,中国科学院兰州化学物理研究所 固体润滑国家重点实验室, 兰州 730000;中国科学院 研究生院, 北京 100049,中国科学院兰州化学物理研究所 固体润滑国家重点实验室, 兰州 730000,中国科学院兰州化学物理研究所 固体润滑国家重点实验室, 兰州 730000,中国科学院兰州化学物理研究所 固体润滑国家重点实验室, 兰州 730000
基金项目:中国科学院西部之光青年创新促进会项目(2014378)
摘    要:以大气等离子喷涂工艺制备的Al_2O_3陶瓷涂层为模板,利用陶瓷涂层中存在的孔隙和微裂纹,采用水热反应在其内部原位合成具有润滑特性的MoS_2,制备出Al_2O_3/MoS_2的复合涂层。结果表明,通过水热反应在陶瓷涂层原有的微观缺陷中成功合成了MoS_2,合成的MoS_2固体粉末呈类球形状,并且这球状的粉末是由纳米片层状的MoS_2搭建组成的。摩擦试验结果表明,与纯Al_2O_3涂层相比,复合涂层中由于MoS_2润滑膜的形成,其摩擦因数和磨损率都显著降低,且载荷越大,复合涂层的摩擦性能越好。

关 键 词:热喷涂  原位合成  Al2O3/MoS2  复合涂层  摩擦磨损
收稿时间:2017/3/24 0:00:00
修稿时间:2017/5/31 0:00:00

Preparation and Tribological Properties of Al2O3/MoS2 Composite Coating
DENG Wen,ZHAO Xiao-qin,LI Shuang-jian,AN Yu-long,ZHOU Hui-di and CHEN Jian-min.Preparation and Tribological Properties of Al2O3/MoS2 Composite Coating[J].China Surface Engineering,2017,30(5):110-118.
Authors:DENG Wen  ZHAO Xiao-qin  LI Shuang-jian  AN Yu-long  ZHOU Hui-di and CHEN Jian-min
Affiliation:State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000;Graduate School, Chinese Academy of Sciences, Beijing 100049,State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000,State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000;Graduate School, Chinese Academy of Sciences, Beijing 100049,State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000,State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000 and State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000
Abstract:Taking thermal sprayed Al2O3 coatings as templets, MoS2 was in-situ synthesized in the pores and micro-cracks of ceramic coatings using a hydrothermal method coupled with vacuum impregnation to prepare Al2O3/MoS2 composite coatings. The result show that MoS2 is successfully synthesized in the pores and micro-cracks of ceramic coatings through hydrothermal reaction, and the MoS2 powders appear flowerlike, and are constructed with many ultrathin nano-sheets. The results of tribological test show that the composite coatings have lower friction coefficient and wear rates due to the formation of MoS2 lubricating film on frictional surfaces compared with pure Al2O3 coatings. The tribological property of composite coatings is better with the increase of the load.
Keywords:plasma spraying  in-suit synthesis  Al2O3/MoS2  composite coatings  friction and wear
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