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FINEMET-type thin films deposited by HiPIMS: Influence of growth and annealing conditions on the magnetic behaviour
Authors:Ioana-Laura Velicu  Maciej Kowalczyk  Maria Neagu  Vasile Tiron  Horia Chiriac  Jarosław Ferenc
Affiliation:1. Faculty of Physics, Alexandru Ioan Cuza University, 700506 Iasi, Romania;2. Faculty of Materials Science and Engineering, Warsaw University of Technology, 05-507 Warszawa, Poland;3. National Institute of Research & Development for Technical Physics, 700050 Iasi, Romania
Abstract:Results concerning the influence of deposition conditions (effective power, Peff, pulse length, τ, and working gas pressure, p) as well as of thermal treatments on the properties of Fe73.5Cu1Nb3Si15.5B7 thin films, deposited by high power impulse magnetron sputtering (HiPIMS) technique, are presented. The Peff, τ and p values were varied in the range of 30–90 W, 4–20 μs and 8–60 mTorr respectively. According to the XRD analysis, in as-deposited state, all the prepared samples are amorphous. For Peff constant the coercive magnetic field, Hc, increases whit τ, while for τ constant Hc decreases when Peff increases. The lowest Hc values have been obtained after the samples were annealed at temperatures between 450 °C and 480 °C, when the average size of the α-Fe(Si) grains and the crystalline volume fraction increase about 45% and 20% respectively.
Keywords:Amorphous   Coercive magnetic field   Nanocrystallization   Sputtering   Thin films
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