| 5-[5-(4-硝基苄基)-2H-四唑亚甲基]-2-芳酰氨基-1,3,4-噻二唑的合成 |
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| 引用本文： | 孙乐,范晓东,张自义.5-[5-(4-硝基苄基)-2H-四唑亚甲基]-2-芳酰氨基-1,3,4-噻二唑的合成[J].合成化学,2004,12(4):365-368,380,J003. |
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| 作者姓名： | 孙乐 范晓东 张自义 |
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| 作者单位： | 西北工业大学化工系,陕西,西安,710072;兰州大学化学系,甘肃,兰州,730000 |
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| 摘 要： | 1-5-(4-硝基苄基)-2H-四唑乙酰基]4-芳酰氨基硫脲(自制)在冰醋酸的存在下，经脱水、环化制备了5-5-(4-硝基苄基)-2H-四唑亚甲基]-2-芳酰氨基-1，3，4-噻二唑。其结构经元素分析，IR，^1H NMR和MS确认。
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| 关 键 词： | 1 3 4-噻二唑 芳酰氨基硫脲 合成 |
Synthesis of 5-[5-(4-Nitrobenzyl)-2H-tetrazol-2-methylene]-2-aroylamino-1,3,4-thiadiazoles |
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| Abstract.Synthesis of 5-[5-(4-Nitrobenzyl)-2H-tetrazol-2-methylene]-2-aroylamino-1,3,4-thiadiazoles[J].Chinese Journal of Synthetic Chemistry,2004,12(4):365-368,380,J003. |
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| Authors: | Abstract |
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| Abstract: | Nitrobenzyl)-2H-tetrazol-2-methylene]-2-aroylamino-1,3,4-thiadiazoles were synthesized by dehydration of 1-5-(4-nitrobenzyl)-2H-tetrazol-2-acetyl]-4-aroylthiosemicarbazides under glacial acetic acid and their structures were determined by elemental analysis, IR, 1H NMR and MS. |
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| Keywords: | thiadiazole aroylthiosemicarbazide synthesis |
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