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Porous and dense Ni hollow fibre membranes
Authors:Bo Meng   Xiaoyao Tan   Xiuxia Meng   Shizhang Qiao  Shaomin Liu  
Affiliation:aSchool of Chemical Engineering, Shandong University of Technology, Zibo 255049, PR China;bARC Centre of Excellence for Functional Nanomaterials, School of Engineering, The University of Queensland, QLD 4072, Australia
Abstract:Nickel hollow fibre membranes were prepared by extruding a polymer solution containing suspended nickel (Ni) powder to green hollow fibres, which were then sintered at elevated temperature under an argon atmosphere. The hollow fibres were characterized by a scanning electron microscope (SEM), X-ray diffractometer (XRD), mercury porosimeter, gas permeation test and conductance measurements. Porous Ni hollow fibres with micron-sized pore structures can be obtained directly by sintering the green fibre at relatively lower temperatures. Heated at a higher temperature (i.e., 950 °C), the Ni hollow fibres became gas-tight membranes which are of great interest for hydrogen separation.
Keywords:Inorganic Materials   X-ray diffraction   Microstructure
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