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Sol-Gel法玻璃颜色涂层的研制
引用本文:滕立东,张梅梅,王春龙.Sol-Gel法玻璃颜色涂层的研制[J].山东轻工业学院学报,1994(1).
作者姓名:滕立东  张梅梅  王春龙
作者单位:山东轻工业学院无机材料系
摘    要:本文论述了溶胶──凝胶法制备Fe_2O_3-CoO-SiO_2系统玻璃涂层的工艺过程;研究了热处理过程中涂层由凝胶向玻璃态的转化过程;探讨了影响成膜过程的各种因素及工艺参数。结果表明;在热处理过程中凝胶发生缩聚反应逐渐转化为非晶态固体薄膜,基质玻璃表面与膜层之间产生牢固的化学键结合,形成连续的无界面玻璃结构;适当选择涂液的成分、提升速度和热处理制度,可制备出性能优良的非晶态颜色涂层。

关 键 词:溶胶-凝胶工艺,浸涂技术,颜色涂层,薄膜结构

Preparation of Glass Colour Coatings by Sol-Gel Process
Teng Lidong,Zhang Meimei,Wang Chunlong.Preparation of Glass Colour Coatings by Sol-Gel Process[J].Journal of Shandong Institute of Light Industry(Natural Science Edition),1994(1).
Authors:Teng Lidong  Zhang Meimei  Wang Chunlong
Abstract:The preparing process of Fe_2O_3-CoO-SiO_2 system glass coatings by sol-gelmethod has been discussed.The structure evolution of gels as a function of heat treatmenttemperature has been studied by means of infrared reflection spectroscopy(IRRS ),X-raydiffraction(XRD)and differential thermal analysis (DTA).The gels of coatings have beengradually changed into non-crystal solid thin film,followed by the condensation reactionwhen heated. The high quality coloured coatings can be obtained on soda-lime-silica glasssubstrates with the dip-coating techniques if the proper processing parameters are chosen.
Keywords:Sol-gel process  dip-coating technique  coloured coatings  film microstructure
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