| 金丝桃素的合成工艺改进 |
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| 引用本文： | 汤媛,刘明星,苏江涛,王贤文,向极钎.金丝桃素的合成工艺改进[J].合成化学,2009,17(4). |
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| 作者姓名： | 汤媛 刘明星 苏江涛 王贤文 向极钎 |
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| 作者单位： | 1. 湖北工业大学,生物工程学院,湖北,武汉,430068
2. 恩施州科学院,湖北,恩施,445002 |
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| 摘 要： | 以大黄素为原料,经还原,Aldol缩合和光照反应合成了金丝桃素,总收率58.6%,其结构经1H NMR, IR和MS表征.
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| 关 键 词： | 金丝桃素 大黄素 合成 工艺改进 |
Process Improvement on the Synthesis of Hypericin |
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| TANG Yuan,LIU Ming-xing,SU Jiang-tao,WANG Xian-wen,XIANG Ji-qian.Process Improvement on the Synthesis of Hypericin[J].Chinese Journal of Synthetic Chemistry,2009,17(4). |
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| Authors: | TANG Yuan LIU Ming-xing SU Jiang-tao WANG Xian-wen XIANG Ji-qian |
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| Affiliation: | 1.Institute of Bioengineering;Hubei University of Technology;Wuhan 430068;China;2.Enshi Institute of Agricultural Sciences;Enshi 445002;China |
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| Abstract: | Hypericin in total yield of 58.6% was synthesized by a three-step reaction of reduction,Aldol condensation and photocyclization from emodin.The structure was confirmed by 1H NMR,IR and MS. |
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| Keywords: | Hypericin emodin synthesis process improvement |
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