| 活血舒筋贴膏剂的质量标准研究 |
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| 引用本文： | 张丽芬,刘志承,索娟,刘纪青,李曙光.活血舒筋贴膏剂的质量标准研究[J].中国药房,2011(11):1012-1014. |
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| 作者姓名： | 张丽芬 刘志承 索娟 刘纪青 李曙光 |
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| 作者单位： | 深圳市中医院; |
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| 基金项目： | 深圳市科技计划立项项目(201003186) |
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| 摘 要： | 目的:建立活血舒筋贴膏剂的质量标准。方法:采用薄层色谱(TLC)法对没药挥发油进行鉴别;采用高效液相色谱法对制剂中紫丁香苷进行含量测定。结果:TLC斑点清晰,分离度好;紫丁香苷进样量在0.138～0.690μg范围内与峰面积积分值呈良好线性关系(r=0.9999),平均回收率为98.50%,RSD=3.04%(n=6)。结论:所建标准可用于活血舒筋贴膏剂的质量控制。
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| 关 键 词： | 活血舒筋贴膏剂 质量标准 薄层色谱法 高效液相色谱法 |
Quality Standard of Huoxue Shujin Plaster |
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| ZHANG Li-fen,LIU Zhi-cheng,SUO Juan,LIU Ji-qing,LI Shu-guang.Quality Standard of Huoxue Shujin Plaster[J].China Pharmacy,2011(11):1012-1014. |
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| Authors: | ZHANG Li-fen LIU Zhi-cheng SUO Juan LIU Ji-qing LI Shu-guang |
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| Affiliation: | ZHANG Li-fen,LIU Zhi-cheng,SUO Juan,LIU Ji-qing,LI Shu-guang(Shenzhen Hospital of Traditional Chinese Medicine,Shenzhen 518033,China) |
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| Abstract: | OBJECTIVE： To establish the quality standard for Huoxue shujin plaster. METHODS： The volatile oil of Commiphora Myrrha was identified by TLC and the content syringin was determined by HPLC. RESULTS： The TLC spots were clear and well-separated. The linear range of syringin in Huoxue shujita plaster was 0,138-0.690 mg （r=0.999 9） with an average recovery of 98.50 % （RSD = 3.04 %, n = 6）. CONCLUSION： The method was reproducible for the quality control of Huoxue shujin plaster. |
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| Keywords: | Huoxue shujin plaster Quality standard TLC HPLC |
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