| 电喷制备多孔二氧化钛微球及其结构表征 |
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| 引用本文： | 赵一阳,汤玉峰,柳文敏,赵巧娜.电喷制备多孔二氧化钛微球及其结构表征[J].光谱实验室,2010,27(4):1663-1666. |
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| 作者姓名： | 赵一阳 汤玉峰 柳文敏 赵巧娜 |
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| 作者单位： | 南阳师范学院化学与制药工程学院,河南省南阳市卧龙路1638号,473061 |
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| 基金项目： | 河南省教育厅自然科学研究计划项目，南阳师范学院科研基金项目 |
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| 摘 要： | 采用电喷离子化技术结合溶胶-凝胶技术制备多孔二氧化钛微球,并利用扫描电镜、红外光谱和X射线衍射等对所得微球的形貌和结构进行了初步的表征。结果表明,该法制备的微球表面不平滑,平均直径范围为350—600nm左右,主要呈锐钛矿晶相。小角X射线衍射的结果表明微球中可能存在有序的孔结构。
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| 关 键 词： | 电喷离子化技术 二氧化钛 多孔 微球 |
Fabrication and Characterization of Porous Titanium Dioxide Microparticles by Electrospray Ionization Technique |
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| ZHAO Yi-Yang,TANG Yu-Feng,LIU Wen-Min,ZHAO Qiao-Na.Fabrication and Characterization of Porous Titanium Dioxide Microparticles by Electrospray Ionization Technique[J].Chinese Journal of Spectroscopy Laboratory,2010,27(4):1663-1666. |
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| Authors: | ZHAO Yi-Yang TANG Yu-Feng LIU Wen-Min ZHAO Qiao-Na |
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| Affiliation: | ZHAO Yi-Yang TANG Yu-Feng LIU Wen-Min ZHAO Qiao-Na(College of Chemistry and Pharmacy Engineering,Nanyang Normal University,Nanyang,Henan 473061,P.R.China) |
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| Abstract: | Porous titanium dioxide microparticles were prepared by electrospray ionization （ESI） technique and sol-gel method.The particles were examined by SEM,FTIR and XRD.Results indicated that the TiO2 particles had rough surface,were not uniform and mostly showed crystalloid phase of anataase with diameter of 350—600nm.The obvious peak in LAXRD spectra also showed there may be potential porous structures in the TiO2 particles. |
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| Keywords: | Electrospray Ionization Technique Titanium Dioxide Porous Microparticle |
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