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微波消化在磷矿石样品制备中的应用
引用本文:曹槐, 尹建国. 微波消化在磷矿石样品制备中的应用[J]. 岩矿测试, 1996, (1): 58-60.
作者姓名:曹槐 尹建国
作者单位:云南大学化学系
基金项目:云南省教委科学研究基金
摘    要:以微波HNO_3消化分解磷矿石试样,用ICP-AES进行多元素同时测定。该方法经磷矿石标准样品验证后,用于云南省九个地区磷矿中Ca、P、Fe、Al、Mg和K六种元素的分析,结果与经典酸分解方法制备样品的分析结果相符;同一样品平行测定9次,其各元素的相对标准偏差(RSD)在1.58%~4.41%。

关 键 词:磷矿石,微波消化,样品制备

Application of Microwave Digestion for Sample Preparation of Phosphorous Ore
Application of Microwave Digestion for Sample Preparation of Phosphorous Ore[J]. Rock and Mineral Analysis, 1996, (1): 58-60.
Authors:Cao Huai  Yin Jianguo
Abstract:The sample was dissolved in HNO_3 by microwave digestion and the solution obtained was analyzed by ICP-AES. The method has been tested on standard reference materials.Phosphorus ores collected from nine regions of Yunnan were analyzed for Ca,P,Fe,Al,Mg and K contents and the results were consistent with those obtained by traditional acid decomposition.
Keywords:phosphorous ore   microwave digestion  sample preparation  
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