| 程序升温溶剂热法制备ZrO2及结构表征 |
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| 引用本文： | 佟淑琴,计远,李莉.程序升温溶剂热法制备ZrO2及结构表征[J].齐齐哈尔轻工业学院学报,2009(5):72-74. |
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| 作者姓名： | 佟淑琴 计远 李莉 |
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| 作者单位： | 齐齐哈尔大学化学与化学工程学院,黑龙江齐齐哈尔161006 |
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| 摘 要： | 采用溶胶—凝胶结合程序升温溶剂热法制备了光催化材料ZrO2，通过XRD、N2吸附-脱附、TPD、SEM等检测手段对其组成、结构及其表面物理化学性质进行了表征。结果表明．合成材料的品型结构良好，孔径分机较均匀．为纳米孔结构（3．7nm）．且比表面积显著增大（130．4m^2／g）。
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| 关 键 词： | 溶胶-凝胶法 程序升温溶剂热法 氧化锆 孔材料 |
Preparation of photocatalytic material ZrO2 by hydrothermal treatment |
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| Authors: | TONG Shu-qin JI Yuan LI Li |
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| Affiliation: | (Department of Chemistry and Chemical Engineering, Qiqihar University, Heilongjiang Qiqihar 161006, China ) |
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| Abstract: | The solid material ZrO2 was prepared temperature method. XRD, N2 adsorption, SEM by the methods of the Sol-gel and hydrothermal treatment at a lower and TPD were used to characterize the composition, structure and surface physicochemical properties of the as-prepared photocatalytic material. The results indicated that the composite exhibited nanoporous structures （ the average pore diameter was ca. 3.7 nm ）, and that of large surface area was 130.4 m^2/g. |
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| Keywords: | Sol-gel method hydrothermal treatment ZrO2 nanoporous material |
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